105 Coexistence of Grain Boundary Sliding and Solute Drag Creep on Thermally Unstable Fine-Grained Aluminum Solid Solution Alloy

2015 ◽  
Vol 2015.23 (0) ◽  
pp. _105-1_-_105-5_
Author(s):  
Tsutomu ITO ◽  
Takashi MIZUGUCHI
2018 ◽  
Vol 941 ◽  
pp. 1216-1221
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

It is widely accepted that the dominant deformation mechanism of fine-grained superplasticity is through grain boundary sliding (GBS) that occurs in fine-grained materials. However, it has been reported that in “Class I” solid solution alloys, superplastic-like behavior controlled by trans-granular deformation occurs by solute drag creep. In this study, we have investigated superplastic behavior in a fine-grained aluminum solid solution alloy with a thermally unstable microstructure. To obtain fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum (Al−Mg) alloy. An equiaxial fine-grained microstructure with a grain size of 7.4 μm was obtained after FSP; however, this microstructure was unstable at high temperatures. Generally, for fine-grained superplasticity or GBS to occur or continue, the fine-grained microstructure must be smaller than 10 μm during high-temperature deformation. However, a large elongation of over 200% was observed at high temperatures despite the occurrence of grain growth. From microstructural observations, it was determined that a fine-grained microstructure is maintained in the early stage of deformation, but at strain levels greater than 100%, trans-granular deformation occurs. The microstructural feature of this trans-granular deformation is similar to the deformation microstructure of solute drag creep observed in “Class I” solid solution alloys. This indicates that a change in the deformation mechanism from GBS to solute drag creep takes place during high-temperature deformation. Here, based on our observations on our model system, which is a thermally unstable aluminum solid solution alloy, we discuss the possibility of a superplastic elongation occurring by means of a transition of the deformation mechanism.


2014 ◽  
Vol 922 ◽  
pp. 360-365 ◽  
Author(s):  
Takashi Mizuguchi ◽  
Tsutomu Ito ◽  
Kota Kimura ◽  
Yasuhiro Tanaka

In this study, the high-temperature ductility of a fine-grained, polycrystalline 5083 solid solution alloy was investigated. The composition of the alloy in mass% was Al–4.5 Mg–0.68 Mn–0.19 Fe–0.13 Si–0.11 Cr. Grain refinement was effectively achieved in the stir zone by a friction stir process, and the grain size could be reduced to 3.7 μm. Tensile tests were performed at temperatures ranging from 643 to 743 K and strain rates ranging from 0.001 to 0.1 /s. The stress–strain curves showed that the flow stress continuously decreased until it reached a maximum value of stress and fractured after the initial strain hardening occurred. The value of elongation-to-failure was more than 100% when temperatures were greater than 693 K. The high ductility observed at this point can be referred to as superplastic-like elongation. This phenomenon has been reported in some Al–Mg alloys. The experimentally determined stress exponent (n value) and activation energy for deformation were about 2.5 and 123 kJ/mol, respectively. These results suggest that the grain boundary sliding, accompanied by solute drag motion of dislocations, was a rate controlling process for deformation.


2016 ◽  
Vol 723 ◽  
pp. 21-26
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

In this study, the superplastic behavior on a fine-grained aluminum solid solution alloy consisting of thermally unstable microstructures was investigated. In order to obtain the fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum alloy. An equiaxial fine-grained microstructure of 7.8 mm was obtained after FSP, but this microstructure was thermally unstable at high temperatures. Commonly, for fine-grained superplasticity to occur (or to continue grain boundary sliding (GBS)), it is necessary to keep the fine-grained microstructure to less than 10 mm during the high-temperature deformation. However, in this study, a large elongation of over 200% was observed at high temperatures in spite of the occurrence of grain growth. From the microstructural observations, it was determined that the fine-grained microstructure was maintained until the early stage of deformation, but the transgranular deformation was observed at a strain of over 100%. The microstructural feature of the abovementioned transgranular deformation is similar to the deformation microstructure of the solute drag creep occurring in "Class I"-type solid solution alloys. This indicates that the deformation mechanism transition from GBS to the solute drag creep occurred during high-temperature deformation. Here, the possibility of occurrence of the superplastic elongation through deformation mechanism transition is discussed as a model of the thermally unstable aluminum solid solution alloy.


2007 ◽  
Vol 39 (1) ◽  
pp. 50-64 ◽  
Author(s):  
Terry R. McNelley ◽  
Keiichiro Oh-Ishi ◽  
Alexander P. Zhilyaev ◽  
Srinivasan Swaminathan ◽  
Paul E. Krajewski ◽  
...  

2012 ◽  
Vol 735 ◽  
pp. 93-100
Author(s):  
Alexander J. Carpenter ◽  
Anthony J. Barnes ◽  
Eric M. Taleff

Complex sheet metal components can be formed from lightweight aluminum and magnesium sheet alloys using superplastic forming technologies. Superplastic forming typically takes advantage of the high strain-rate sensitivity characteristic of grain-boundary-sliding (GBS) creep to obtain significant ductility at high temperatures. However, GBS creep requires fine-grained materials, which can be expensive and difficult to manufacture. An alternative is provided by materials that exhibit solute-drag (SD) creep, a mechanism that also produces elevated values of strain-rate sensitivity. SD creep typically operates at lower temperatures and faster strain rates than does GBS creep. Unlike GBS creep, solute-drag creep does not require a fine, stable grain size. Previous work by Boissière et al. suggested that the Mg-Y-Nd alloy, essentially WE43, deforms by SD creep at temperatures near 400°C. The present investigation examines both tensile and biaxial deformation behavior of ElektronTM 43 sheet, which has a composition similar to WE43, at temperatures ranging from 400 to 500°C. Data are presented that provide additional evidence for SD creep in Elektron 43 and demonstrate the remarkable degree of biaxial strain possible under this regime (>1000%). These results indicate an excellent potential for producing complex 3-D parts, via superplastic forming, using this particular heat-treatable Mg alloy.


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