Superplastic Elongation through Deformation Mechanism Transition during High-Temperature Deformation in Thermally Unstable Fine-Grained Aluminum Solid Solution Alloy

2016 ◽  
Vol 723 ◽  
pp. 21-26
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

In this study, the superplastic behavior on a fine-grained aluminum solid solution alloy consisting of thermally unstable microstructures was investigated. In order to obtain the fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum alloy. An equiaxial fine-grained microstructure of 7.8 mm was obtained after FSP, but this microstructure was thermally unstable at high temperatures. Commonly, for fine-grained superplasticity to occur (or to continue grain boundary sliding (GBS)), it is necessary to keep the fine-grained microstructure to less than 10 mm during the high-temperature deformation. However, in this study, a large elongation of over 200% was observed at high temperatures in spite of the occurrence of grain growth. From the microstructural observations, it was determined that the fine-grained microstructure was maintained until the early stage of deformation, but the transgranular deformation was observed at a strain of over 100%. The microstructural feature of the abovementioned transgranular deformation is similar to the deformation microstructure of the solute drag creep occurring in "Class I"-type solid solution alloys. This indicates that the deformation mechanism transition from GBS to the solute drag creep occurred during high-temperature deformation. Here, the possibility of occurrence of the superplastic elongation through deformation mechanism transition is discussed as a model of the thermally unstable aluminum solid solution alloy.

2018 ◽  
Vol 941 ◽  
pp. 1216-1221
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

It is widely accepted that the dominant deformation mechanism of fine-grained superplasticity is through grain boundary sliding (GBS) that occurs in fine-grained materials. However, it has been reported that in “Class I” solid solution alloys, superplastic-like behavior controlled by trans-granular deformation occurs by solute drag creep. In this study, we have investigated superplastic behavior in a fine-grained aluminum solid solution alloy with a thermally unstable microstructure. To obtain fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum (Al−Mg) alloy. An equiaxial fine-grained microstructure with a grain size of 7.4 μm was obtained after FSP; however, this microstructure was unstable at high temperatures. Generally, for fine-grained superplasticity or GBS to occur or continue, the fine-grained microstructure must be smaller than 10 μm during high-temperature deformation. However, a large elongation of over 200% was observed at high temperatures despite the occurrence of grain growth. From microstructural observations, it was determined that a fine-grained microstructure is maintained in the early stage of deformation, but at strain levels greater than 100%, trans-granular deformation occurs. The microstructural feature of this trans-granular deformation is similar to the deformation microstructure of solute drag creep observed in “Class I” solid solution alloys. This indicates that a change in the deformation mechanism from GBS to solute drag creep takes place during high-temperature deformation. Here, based on our observations on our model system, which is a thermally unstable aluminum solid solution alloy, we discuss the possibility of a superplastic elongation occurring by means of a transition of the deformation mechanism.


1996 ◽  
Vol 460 ◽  
Author(s):  
P. H. Kitabjian ◽  
A. Garg ◽  
R. Noebe ◽  
W. D. Nix

ABSTRACTWe have investigated the high-temperature deformation behavior of the solid-solution strengthened alloy Ni-47.5Al-2.5Ti. Single crystals were deformed in compression in the “hard” <001> and “soft” <111> orientations, at temperatures between 900°C and 1200°C. The results show that Ti has a very powerful solute strengthening effect in NiAl. The creep rates for the solid-solution alloy were observed to be three to four orders of magnitude lower than for the stoichiometric material. We discuss our efforts to understand this solid-solution strengthening effect. We have studied high-temperature deformation transients in an effort to determine whether solute drag effects contribute to the creep resistance of this solid solution. In addition, we have examined the solute size effect of Ti as it replaces Al on the Al sub-lattice. We discuss the probable mechanism of creep of this alloy in light of TEM observations of the dislocation structures in creep-deformed crystals.


2014 ◽  
Vol 783-786 ◽  
pp. 352-357
Author(s):  
Pierre Lhuissier ◽  
Luc Salvo ◽  
Jean Jacques Blandin

Due to limited deformability at room temperature, high temperature forming of magnesium alloys appears as an interesting alternative. Superplastic properties can be obtained in the case of fine grained magnesium alloys and in this regime, due to significant damage sensitivity, fracture strain is mainly controlled by nucleation, growth and coalescence of cavities. Magnesium alloys with large grained alloys can also exhibit interesting deformabilities at high temperature since dislocation movements can be controlled by a solute drag effect promoting plastic stability. Examples of such situations are presented in the case of wrought magnesium alloys, the associated damage mechanisms being investigated thanks to 3D X-ray micro tomography performed in continuous mode, namely directly during high temperature deformation tests.


2010 ◽  
Vol 433 ◽  
pp. 267-272 ◽  
Author(s):  
R. Boissière ◽  
Jean Jacques Blandin ◽  
Luc Salvo

The deformability of wrought magnesium alloys at room temperature is limited and a way to overcome this limit is to carry out forming operations in warm or hot conditions. In the case of fine grained alloys, superplastic properties can be generally achieved but in this regime, the Mg alloys are sensitive to strain induced cavitation. However, large grained alloys can also exhibit quite large deformabilities when they are deformed at high temperature. This can be due to the fact that on one hand, the Mg alloys may quite easily dynamically recrystallize and on the other hand, that dislocation movements may be controlled by a solute drag effect leading to significant strain rate sensitivity parameters. These various mechanisms of deformation will depend on the composition, the mean grain size and the conditions of deformation (i.e. temperature and strain rate). In this work, the high temperature deformation mechanisms as well as the associated damage mechanisms of two wrought magnesium alloys are discussed.


2015 ◽  
Vol 466 ◽  
pp. 653-657 ◽  
Author(s):  
Yoshito Sugino ◽  
Shigeharu Ukai ◽  
Naoko Oono ◽  
Shigenari Hayashi ◽  
Takeji Kaito ◽  
...  

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