Short-Term Oxidation Behavior, Microstructure Evolution and Compression Behavior of Nickel-Based Superalloy GH4037 in Solid and Semi-Solid States

Semi-solid processing combines the advantages of traditional forging and casting methods, so it has received much attention recently. However, the research on semi-solid behaviors of Nickel-based superalloys has been rarely reported. In order to investigate the behaviors of Nickel-based superalloy at solid and semi-solid states, oxidation experiments, isothermal treatment experiments and deformation experiments of GH4037 alloy were studied. Short-term oxidation experiments of GH4037 alloy were carried out at a solid temperature (1200 °C) and a semi-solid temperature (1360 °C). The results indicated that the oxides formed at 1200 °C were mainly composed of TiO2, Cr2O3 and a small amount of spinels NiCr2O4, while the oxides formed at 1360 °C consisted of the spinels of NiCr2O4, NiWO4 and NiMoO4 besides TiO2 and Cr2O3. Microstructure evolution of GH4037 alloy after semi-solid isothermal treatment at 1370 °C and 1380 °C was studied. The results indicated that semi-solid microstructures consisted of equiaxed solid grains and liquid phases. The average grains size and shape factor of solid grains were affected by melting mechanism and grain growth mechanism. Compression behaviors of GH4037 alloy after compressed at 1200 °C and 1360 °C were investigated. The results indicated that the flow stress of 1360 °C decreased significantly compared to that of 1200 °C. The deformation zones in the specimens were divided into three parts: the difficult deformation zone, the large deformation zone, and the free deformation zone. At 1200 °C, the deformation mechanism was plastic deformation mechanism. At 1360 °C, sliding between solid particles (SS), liquid flow (LF), flow of liquid incorporating solid particles (FLS), plastic deformation of solid particles (PDS) coexisted in the compression specimen.

A Compendium of Deformation-Mechanism Maps for Metals

Deformation-mechanism maps represent an invaluable guide to predicting the optimum processing conditions for a material. They are also useful in matching a material to a given engineering application. The present book summarizes recent research results in the field. The book references 106 original resources and includes their direct web link for in-depth reading.

Experimental Study on Fracturing Fracture Deformation Mechanism of Shale Reservoir

After large-scale sand fracturing of horizontal wells in shale gas reservoir, fracturing fractures will deform in the production process. However, fracture deformation will lead to the decrease in fracture conductivity and then cause the decrease of gas well productivity. Therefore, in order to evaluate the fracturing fracture deformation mechanism of shale reservoirs, the shale proppant-supported fracture deformation evaluation experiments were carried out under different proppant types, particle sizes, sanding concentrations, and closure pressure conditions, respectively, and the variation curves of fracture width was calculated by a stereomicroscope under different experimental conditions. Then based on the experimental results, the fracture sensitivity factors and fracture deformation mechanism were analyzed, and the deformation mechanisms of fracturing fractures affected by proppant embedding and crushing were studied emphatically. The analysis results of fracture sensitivity factors indicate that the larger the particle size and hardness of proppant, the lower the sand concentration, proppant embedded on the shale rock surface. Moreover, the deeper the proppant is embedded, the faster the fracture conductivity decreases. In addition, the greater the closure pressure, the more serious is the proppant embedment, and the faster the fracture width decreases. The analysis results of fracture deformation mechanism show that, on the on hand, under variable closure pressure, the proppant with larger hardness and larger particle size is used for fracturing, and the proppant embedded in the fracture surface is the main cause of fracture deformation. However, if only the sand concentration of the proppant in the fracture is changed, the fracture deformation is jointly dominated by the embedding and crushing of the proppant. On the other hand, under constant closure pressure, the main mechanism of fracture deformation is that the proppant is embedded into the fracture surface when the closure pressure is low, but if the closure pressure is high, the main mechanism of fracture deformation is the crushing and compaction of proppant.