scholarly journals Coexistence of Grain Boundary Sliding and Solute Drag Creep during High-Temperature Deformation for Fine-Grained Aluminum Solid Solution Alloy

Materia Japan ◽  
2017 ◽  
Vol 56 (5) ◽  
pp. 346-353 ◽  
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi
2018 ◽  
Vol 941 ◽  
pp. 1216-1221
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

It is widely accepted that the dominant deformation mechanism of fine-grained superplasticity is through grain boundary sliding (GBS) that occurs in fine-grained materials. However, it has been reported that in “Class I” solid solution alloys, superplastic-like behavior controlled by trans-granular deformation occurs by solute drag creep. In this study, we have investigated superplastic behavior in a fine-grained aluminum solid solution alloy with a thermally unstable microstructure. To obtain fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum (Al−Mg) alloy. An equiaxial fine-grained microstructure with a grain size of 7.4 μm was obtained after FSP; however, this microstructure was unstable at high temperatures. Generally, for fine-grained superplasticity or GBS to occur or continue, the fine-grained microstructure must be smaller than 10 μm during high-temperature deformation. However, a large elongation of over 200% was observed at high temperatures despite the occurrence of grain growth. From microstructural observations, it was determined that a fine-grained microstructure is maintained in the early stage of deformation, but at strain levels greater than 100%, trans-granular deformation occurs. The microstructural feature of this trans-granular deformation is similar to the deformation microstructure of solute drag creep observed in “Class I” solid solution alloys. This indicates that a change in the deformation mechanism from GBS to solute drag creep takes place during high-temperature deformation. Here, based on our observations on our model system, which is a thermally unstable aluminum solid solution alloy, we discuss the possibility of a superplastic elongation occurring by means of a transition of the deformation mechanism.


2016 ◽  
Vol 723 ◽  
pp. 21-26
Author(s):  
Tsutomu Ito ◽  
Takashi Mizuguchi

In this study, the superplastic behavior on a fine-grained aluminum solid solution alloy consisting of thermally unstable microstructures was investigated. In order to obtain the fine-grained microstructure, friction stir processing (FSP) was applied to a commercial 5083 aluminum alloy. An equiaxial fine-grained microstructure of 7.8 mm was obtained after FSP, but this microstructure was thermally unstable at high temperatures. Commonly, for fine-grained superplasticity to occur (or to continue grain boundary sliding (GBS)), it is necessary to keep the fine-grained microstructure to less than 10 mm during the high-temperature deformation. However, in this study, a large elongation of over 200% was observed at high temperatures in spite of the occurrence of grain growth. From the microstructural observations, it was determined that the fine-grained microstructure was maintained until the early stage of deformation, but the transgranular deformation was observed at a strain of over 100%. The microstructural feature of the abovementioned transgranular deformation is similar to the deformation microstructure of the solute drag creep occurring in "Class I"-type solid solution alloys. This indicates that the deformation mechanism transition from GBS to the solute drag creep occurred during high-temperature deformation. Here, the possibility of occurrence of the superplastic elongation through deformation mechanism transition is discussed as a model of the thermally unstable aluminum solid solution alloy.


2012 ◽  
Vol 735 ◽  
pp. 93-100
Author(s):  
Alexander J. Carpenter ◽  
Anthony J. Barnes ◽  
Eric M. Taleff

Complex sheet metal components can be formed from lightweight aluminum and magnesium sheet alloys using superplastic forming technologies. Superplastic forming typically takes advantage of the high strain-rate sensitivity characteristic of grain-boundary-sliding (GBS) creep to obtain significant ductility at high temperatures. However, GBS creep requires fine-grained materials, which can be expensive and difficult to manufacture. An alternative is provided by materials that exhibit solute-drag (SD) creep, a mechanism that also produces elevated values of strain-rate sensitivity. SD creep typically operates at lower temperatures and faster strain rates than does GBS creep. Unlike GBS creep, solute-drag creep does not require a fine, stable grain size. Previous work by Boissière et al. suggested that the Mg-Y-Nd alloy, essentially WE43, deforms by SD creep at temperatures near 400°C. The present investigation examines both tensile and biaxial deformation behavior of ElektronTM 43 sheet, which has a composition similar to WE43, at temperatures ranging from 400 to 500°C. Data are presented that provide additional evidence for SD creep in Elektron 43 and demonstrate the remarkable degree of biaxial strain possible under this regime (>1000%). These results indicate an excellent potential for producing complex 3-D parts, via superplastic forming, using this particular heat-treatable Mg alloy.


2014 ◽  
Vol 922 ◽  
pp. 360-365 ◽  
Author(s):  
Takashi Mizuguchi ◽  
Tsutomu Ito ◽  
Kota Kimura ◽  
Yasuhiro Tanaka

In this study, the high-temperature ductility of a fine-grained, polycrystalline 5083 solid solution alloy was investigated. The composition of the alloy in mass% was Al–4.5 Mg–0.68 Mn–0.19 Fe–0.13 Si–0.11 Cr. Grain refinement was effectively achieved in the stir zone by a friction stir process, and the grain size could be reduced to 3.7 μm. Tensile tests were performed at temperatures ranging from 643 to 743 K and strain rates ranging from 0.001 to 0.1 /s. The stress–strain curves showed that the flow stress continuously decreased until it reached a maximum value of stress and fractured after the initial strain hardening occurred. The value of elongation-to-failure was more than 100% when temperatures were greater than 693 K. The high ductility observed at this point can be referred to as superplastic-like elongation. This phenomenon has been reported in some Al–Mg alloys. The experimentally determined stress exponent (n value) and activation energy for deformation were about 2.5 and 123 kJ/mol, respectively. These results suggest that the grain boundary sliding, accompanied by solute drag motion of dislocations, was a rate controlling process for deformation.


1996 ◽  
Vol 460 ◽  
Author(s):  
P. H. Kitabjian ◽  
A. Garg ◽  
R. Noebe ◽  
W. D. Nix

ABSTRACTWe have investigated the high-temperature deformation behavior of the solid-solution strengthened alloy Ni-47.5Al-2.5Ti. Single crystals were deformed in compression in the “hard” <001> and “soft” <111> orientations, at temperatures between 900°C and 1200°C. The results show that Ti has a very powerful solute strengthening effect in NiAl. The creep rates for the solid-solution alloy were observed to be three to four orders of magnitude lower than for the stoichiometric material. We discuss our efforts to understand this solid-solution strengthening effect. We have studied high-temperature deformation transients in an effort to determine whether solute drag effects contribute to the creep resistance of this solid solution. In addition, we have examined the solute size effect of Ti as it replaces Al on the Al sub-lattice. We discuss the probable mechanism of creep of this alloy in light of TEM observations of the dislocation structures in creep-deformed crystals.


2014 ◽  
Vol 452 (1-3) ◽  
pp. 628-632 ◽  
Author(s):  
Yoshito Sugino ◽  
Shigeharu Ukai ◽  
Bin Leng ◽  
Naoko Oono ◽  
Shigenari Hayashi ◽  
...  

2005 ◽  
Vol 475-479 ◽  
pp. 393-396 ◽  
Author(s):  
Dong Suk Lee ◽  
Gyu-Sam Shim ◽  
Mok Soon Kim ◽  
Won Yong Kim ◽  
Hiroshi Yamagata

Compressive deformation behavior of pre-sintered Al-10Si-5Fe-1Cu-0.5Mg-1Zr (wt%) alloy containing 15% of porosity was investigated in the temperature range from 753 K to 793 K and at strain rates from 10-4 to 100 s-1. From the microstructural observation, it was revealed that the occurrence of grain boundary sliding accomodated by dynamic recrystallization during the compressive deformation was closely associated with the considerable decrease in the porosity of the pre-sintered alloy. In the specimens deformed at 793 K with 10-4~100 s-1 and at 773 K with 10- 4~10-2 s-1, we have found an evidence of the occurrence of a liquid phase during compressive deformation in the microstructure. The liquid phase was considered to promote particle boundary sliding and hinder the reduction of the pore.


2010 ◽  
Vol 654-656 ◽  
pp. 611-614 ◽  
Author(s):  
Masafumi Noda ◽  
Yoshihito Kawamura

Magnesium alloys are very attractive in such applications as automotive and aerospace. However, the mechanical properties of Mg alloys are inferior to those of Al alloys, and this limits their range of applications. In the present study, effects of annealing on the mechanical properties and the thermal stability of the microstructure in LPSO Mg-Zn-Y extruded alloys were investigated. Even when elongation showed 10% with having maintained high strength to annealing temperature at 573 K for 3.6 ks, and this alloy extended annealing time for 1.0 kh, LPSO phase did bent and was able to confirm kink bands. On the other hand, α-Mg phase was fine structure without pronounced grain growth. In elevated temperature deformation of as extruded and annealed materials, LPSO phase did finely dispersed to α-Mg phase by grain boundary sliding of α-Mg phase, but fracture did not occurred in the interface between LPSO and α-Mg phases. Kink bands introduced in LPSO phase during plastic deformation and fine-grained α-Mg phase were important to obtained of high strength and ductility.


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