Characterization of Column Hold-Up Volume with Static and Dynamic Methods on an Immobilized Polysaccharide-Based Chiral Stationary Phase

2007 ◽  
Vol 67 (1-2) ◽  
pp. 3-7 ◽  
Author(s):  
Wenjian Lao ◽  
Jay Gan
Keyword(s):  
Stationary Phase ◽  
Chiral Stationary Phase ◽  
Dynamic Methods

Characterization of a Chiral Stationary Phase by HR/MAS NMR Spectroscopy and Investigation of Enantioselective Interaction with Chiral Ligates by Transferred NOE

2004 ◽  
Vol 126 (12) ◽  
pp. 3809-3816 ◽  
Author(s):  
Christine Hellriegel ◽  
Urban Skogsberg ◽  
Klaus Albert ◽  
Michael Lämmerhofer ◽  
Norbert M. Maier ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Stationary Phase ◽  
Chiral Stationary Phase ◽  
Mas Nmr ◽  
Transferred Noe

scholarly journals Strategies for Preparation of Chiral Stationary Phases: Progress on Coating and Immobilization Methods

Molecules ◽  
2021 ◽  
Vol 26 (18) ◽  
pp. 5477
Author(s):  
Carla Fernandes ◽  
Joana Teixeira ◽  
Madalena M. M. Pinto ◽  
Maria Elizabeth Tiritan
Keyword(s):  
Stationary Phase ◽  
Chiral Stationary Phase ◽  
Stationary Phases ◽  
Chiral Stationary Phases ◽  
Separation And Purification ◽  
Enantioselective Chromatography ◽  
Synthetic Approaches ◽  
Applied Coating ◽  
Selection Of

Enantioselective chromatography is one of the most used techniques for the separation and purification of enantiomers. The most important issue for a specific successful enantioseparation is the selection of the suitable chiral stationary phase (CSP). Different synthetic approaches have been applied for the preparation of CSPs, which embrace coating and immobilization methods. In addition to the classical and broadly applied coating and immobilization procedures, innovating strategies have been introduced recently. In this review, an overview of different methods for the preparation of coated and immobilized CSPs is described. Updated examples of CSPs associated with the various strategies are presented. Considering that after the preparation of a CSP its characterization is fundamental, the methods used for the characterization of all the described CSPs are emphasized.

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