The Effect of Hydrostatic Pressure on Physical Properties and Microstructure of Spruce and Cherry

Holzforschung ◽  
2000 ◽  
Vol 54 (1) ◽  
pp. 83-92 ◽  
Author(s):  
Voichita Bucur ◽  
Simone Garros ◽  
Claire Y. Barlow

Summary The effect of hydrostatic pressure on the density, the ultrasonic velocities and the microstructure of spruce and cherry wood has been studied. Generally speaking, under hydrostatic pressure wood becomes less heterogeneous and less anisotropic than natural wood. In spruce, crushing and buckling of the thin-walled cells in the earlywood takes place. This also has the effect of disrupting the medullary rays, which assume a zig-zag path through the structure. Cherry has a much more homogeneous structure, and the main effect of the hydrostatic pressure is compaction of the vessels by buckling of the walls. The fibres are scarcely affected by the treatment. The width of the earlywood zone decreased after the application of pressure by 26% in spruce, and by 11% in cherry. The average density was increased by the hydrostatic pressure by 26% for spruce and by 46% for cherry. The densitometric profile of spruce demonstrates significant changes following the pressure treatment, with the minimum density DMin increasing and the maximum density DMax decreasing. For cherry, the densitometric profile is shifted rather uniformly towards higher densities, and the annual ring profile is spatially slightly compacted but otherwise similar to that of untreated wood. The anisotropy of wood (expressed by the ratio of acoustic invariants) decreased by 56% for spruce and by 33% for cherry. The structural damage in spruce is predominantly found in the radial (R) direction, and this corresponds to a reduction of 73% in the velocity of the longitudinal ultrasonic waves in the radial direction, VRR. In cherry, the structural damage is mainly in the transverse, T direction. The velocity of the longitudinal ultrasonic waves in the transverse direction, VTT is reduced by 44%. The medullary rays in cherry seem to be the most important anatomical feature influencing the propagation of ultrasonic waves.

1985 ◽  
Vol 54 (1) ◽  
pp. 334-338 ◽  
Author(s):  
Takeshi Kanomata ◽  
Kiwamu Shirakawa ◽  
Takejiro Kaneko

Author(s):  
R. N. V. C. Virinthorn ◽  
M. Chandrasekaran ◽  
K. Wang ◽  
K. L. Goh

AbstractWe described a technique of a post-process stage to partially remove the poly(vinyl alcohol) (PVA) binder in Poly(lactic-co-glycolic acid) (PLGA) dental scaffolds. The scaffolds were exposed to ultrasonic waves while immersed in an ethanol/acetone solvent mixture that possessed both polar and nonpolar properties. A factorial experiment was conducted in which the scaffolds were treated to three levels of sonication power (pW): 0, 20% (22 W) and 40% (44 W), and soaking duration (t): 5, 15, and 30 min. The treated scaffolds were characterized by FT-IR, optical microscopy, and mechanical (compressive) testing. FT-IR revealed that the amount of PVA decreased with increasing pW and t. Two-way ANOVA revealed that increasing pW and t, respectively, resulted in increasing scaffold surface area to volume (SVR). Sonication and solvent caused structural damage (i.e., unevenness) on the scaffold surface, but the damage was minimal at 20% pW and 30 min. The optimal values of pW and t resulting in enhanced fracture strength, strain and toughness were 20% and 30 min, respectively, which corroborated the findings of minimal structural damage. However, sonication had no significant effects on the scaffold stiffness. Mechanistic analysis of the effects of sonication predicted that the ultrasonic energy absorbed by the scaffold was sufficient to disrupt the van Der Waals bonds between the PVA and PLGA but not high enough to disrupt the covalent bonds within the PLGA. This technique is promising as it can partially remove the PVA from the scaffold, and mitigate problematic issues down the line, such as thermal degradation during sterilization, and undue delay/variability in biodegradation.


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