A Novel Approach to Understanding Asphalt Binder Aging Behavior Using Asphaltene Proportion as a Performance Indicator

2015 ◽  
Vol 44 (1) ◽  
pp. 20140490 ◽  
Author(s):  
Yogesh Shamsunder Kumbargeri ◽  
Krishna Prapoorna Biligiri
2020 ◽  
Vol 13 (6) ◽  
pp. 697-706
Author(s):  
Yuhong Wang ◽  
Kecheng Zhao ◽  
Fangjin Li ◽  
Qi Gao ◽  
King Wai Chiu Lai

AbstractThe microscopic surface features of asphalt binders are extensively reported in existing literature, but relatively fewer studies are performed on the morphology of asphaltene microstructures and cross-examination between the surface features and asphaltenes. This paper reports the findings of investigating six types of asphalt binders at the nanoscale, assisted with atomic force microscopy (AFM) and scanning transmission electron microscopy (STEM). The surface features of the asphalt binders were examined by using AFM before and after being repetitively peeled by a tape. Variations in infrared (IR) absorbance at the wavenumber around 1700 cm−1, which corresponds to ketones, were examined by using an infrared s-SNOM instrument (scattering-type scanning near-field optical microscope). Thin films of asphalt binders were examined by using STEM, and separate asphaltene particles were cross-examined by using both STEM and AFM. In addition, connections between the microstructures and binder’s physicochemical properties were evaluated. The use of both microscopy techniques provide comprehensive and complementary information on the microscopic nature of asphalt binders. It was found that the dynamic viscosities of asphalt binders are predominantly determined by the zero shear viscosity of the corresponding maltenes and asphaltene content. Limited samples also suggest that the unique bee structures are likely related to the growth of asphaltene content during asphalt binder aging process, but more asphalt binders from different crude sources are needed to verify this finding.


2021 ◽  
Vol 1 (1) ◽  
pp. 1
Author(s):  
Yusuke Maeno ◽  
Tatsuo Oyama ◽  
M.L.U.K. Piyasena ◽  
Yuji Kawase

Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1067 ◽  
Author(s):  
Hechuan Li ◽  
Jianying Yu ◽  
Shaopeng Wu ◽  
Quantao Liu ◽  
Yuanyuan Li ◽  
...  

Induction heating is a valuable technology to repair asphalt concrete damage inside. However, in the process of induction heating, induced particles will release a large amount of heat to act on asphalt binder in a short time. The purpose of this paper was to study the effect of induction heating on asphalt binder aging in steel fibers modified asphalt concrete. The experiments were divided into two parts: induction heating of Dramix steel fibers coated with asphalt binder (DA) and steel wool fibers modified asphalt concrete. After induction heating, the asphalt binders in the samples were extracted for testing aging indices with Fourier Transform Infrared (FTIR), Dynamic Shear Rheometer (DSR), and Four-Components Analysis (FCA) tests. The aging of asphalt binder was analyzed identifying the change of chemical structure, the diversification of rheological properties, and the difference of component. The experiments showed that the binder inside asphalt concrete began aging during induction heating due to thermal oxygen reaction and volatilization of light components. However, there was no peak value of the carbonyl index after induction heating of ten cycles, and the carbonyl index of DA was equivalent to that of binder in asphalt concrete after three induction heating cycles, which indicated the relatively closed environment inside asphalt concrete can inhibit the occurrence of the aging reaction.


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