Flexural and diametral tensile strength of composite resins

Clinical Relevance Irradiance may decrease as the light-emitting diode (LED) is discharged. Therefore, the LED must be charged carefully to prevent the possibility of influencing the chemical, mechanical, and physical properties of composite resin. SUMMARY The aim of this study was to evaluate the influence of different light-emitting diode (LED) curing units and battery levels on the chemical, mechanical, and physical properties of composite resins. The irradiance for each cycle from full to completely discharged battery level was evaluated, for five different new cordless LED units: Optilight Color (Gnatus), Bluephase (Ivoclar), Valo (Ultradent), Radii Plus (SDI), and Radii Xpert (SDI). After the irradiance evaluation, composite resin specimens were prepared and light cured, while varying the battery level for each LED unit: high level (HL, 100%), medium level (ML, 50%), and low level (LL, 10%). The degree of conversion, diametral tensile strength, sorption, and solubility were also evaluated. Data were checked for homoscedasticity and submitted to two-way and three-way analysis of variance, depending on the test performed, followed by the Tukey test with a significance level of 95%. A negative correlation was found between irradiance and cycles of light curing, which was checked by the Pearson correlation test. Valo and Radii Xpert were not influenced by the battery level in any test performed. However, different battery levels for some LED units can influence the degree of conversion, diametral tensile strength, sorption, and solubility of composite resins.

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Effect of Preheating and Fatiguing on Mechanical Properties of Bulk-fill and Conventional Composite Resin

Operative Dentistry ◽

10.2341/19-092-l ◽

2019 ◽

Vol 45 (4) ◽

pp. 387-395

Author(s):

AA Abdulmajeed ◽

TE Donovan ◽

R Cook ◽

TA Sulaiman

Keyword(s):

Mechanical Properties ◽

Fracture Toughness ◽

Tensile Strength ◽

Elastic Modulus ◽

Flexural Strength ◽

Composite Resin ◽

Statistical Significance ◽

Composite Resins ◽

Significant Difference ◽

Diametral Tensile Strength

Clinical Relevance Bulk-fill composite resins may have comparable mechanical properties to conventional composite resin. Preheating does not reduce the mechanical properties of composite resins. SUMMARY Statement of Problem: Bulk-fill composite resins are increasingly used for direct restorations. Preheating high-viscosity versions of these composites has been advocated to increase flowability and adaptability. It is not known what changes preheating may cause on the mechanical properties of these composite resins. Moreover, the mechanical properties of these composites after mastication simulation is lacking. Purpose: The purpose of this study was to evaluate the effect of fatiguing and preheating on the mechanical properties of bulk-fill composite resin in comparison to its conventional counterpart. Methods and Materials: One hundred eighty specimens of Filtek One Bulk Fill Restorative (FOBR; Bulk-Fill, 3M ESPE) and Filtek Supreme Ultra (FSU; Conventional, 3M ESPE) were prepared for each of the following tests: fracture toughness (International Organization for Standardization, ISO 6872), diametral tensile strength (No. 27 of ANSI/ADA), flexural strength, and elastic modulus (ISO Standard 4049). Specimens in the preheated group were heated to 68°C for 10 minutes and in the fatiguing group were cyclically loaded and thermocycled for 600,000 cycles and then tested. Two-/one-way analysis of variance followed by Tukey Honest Significant Difference (HSD) post hoc test was used to analyze data for statistical significance (α=0.05). Results: Preheating and fatiguing had a significant effect on the properties of both FSU and FOBR. Fracture toughness increased for FOBR specimens when preheated and decreased when fatigued (p=0.016). FOBR had higher fracture toughness value than FSU. Diametral tensile strength decreased significantly after fatiguing for FSU (p=0.0001). FOBR had a lower diametral tensile strength baseline value compared with FSU (p=0.004). Fatiguing significantly reduced the flexural strength of both FSU and FOBR (p=0.011). Preheating had no effect on the flexural strength of either FSU or FOBR. Preheating and fatiguing significantly decreased the elastic modulus of both composite resins equally (p>0.05). Conclusions: Preheating and fatiguing influenced the mechanical properties of composite resins. Both composites displayed similar mechanical properties. Preheating did not yield a major negative effect on their mechanical properties; the clinical implications are yet to be determined.

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Influence of Battery Level of a Cordless LED Unit on the Properties of a Nanofilled Composite Resin

Operative Dentistry ◽

10.2341/15-200-l ◽

2016 ◽

Vol 41 (4) ◽

pp. 409-416 ◽

Cited By ~ 2

Author(s):

AG Pereira ◽

LHA Raposo ◽

DNR Teixeira ◽

RCQ Gonzaga ◽

IO Cardoso ◽

...

Keyword(s):

Tensile Strength ◽

Light Intensity ◽

Composite Resin ◽

Light Emitting Diode ◽

Pearson Correlation ◽

Composite Resins ◽

Degree Of Conversion ◽

Battery Voltage ◽

Significant Difference ◽

Diametral Tensile Strength

SUMMARY The properties of composite resins can be influenced by light activation, depending primarily on the performance of the curing unit. The aim of this study was to evaluate how different battery levels of a cordless light-emitting diode (LED) unit influence the properties of a nanofilled composite resin. First, the battery voltage and light intensity of the cordless LED unit were individually checked for all light-curing cycles. Then, composite resin discs were prepared and light-cured at different battery levels: high level (HL, 100%), medium level (ML, 50%), and low level (LL, 10%). The degree of conversion, diametral tensile strength, sorption, and solubility of the specimens were tested. Data were checked for homoscedasticity and submitted to one-way analysis of variance followed by Tukey honestly significant difference and Pearson correlation tests (p<0.05). The battery voltage and light intensity varied significantly among the groups (p<0.001). The LL group presented a lower degree of conversion than the HL and ML groups (p<0.001), which shower similar results (p=0.182). Lower diametral tensile strength was also verified for the LL group when compared with the HL and ML groups (p<0.001), which presented no difference (p=0.052). Positive correlation was observed between the light intensity and the parameters studied, with the exception of sorption and solubility (p<0.001). The ML and LL groups showed higher sorption than the HL group (p <0.001), but no difference was verified between the first two groups (p=0.535). No significant differences were found for solubility between the ML and LL groups (p=0.104), but the HL group presented lower values (p<0.001). The different battery levels of the cordless LED curing unit influenced all the properties of the nanofilled composite resin evaluated.

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Diametral tensile strength of composite resins submitted to different activation techniques

Brazilian Oral Research ◽

10.1590/s1806-83242006000300006 ◽

2006 ◽

Vol 20 (3) ◽

pp. 214-218 ◽

Cited By ~ 9

Author(s):

Denise Sá Maia Casselli ◽

Claudia Cia Worschech ◽

Luis Alexandre Maffei Sartini Paulillo ◽

Carlos Tadeu dos Santos Dias

Keyword(s):

Tensile Strength ◽

Composite Resin ◽

Artificial Saliva ◽

Testing Machine ◽

Composite Resins ◽

Universal Testing ◽

Halogen Light ◽

Indirect Composite ◽

Diametral Tensile Strength ◽

Curing Systems

The aim of this study was to evaluate the diametral tensile strength (DTS) of composite resins submitted to different curing techniques. Four composite resins were tested in this study: Targis (Ivoclar), Solidex (Shofu), Charisma (Heraeus-Kulzer) and Filtek Z250 (3M Espe). Sixty-four cylindrical specimens were prepared and divided into eight groups according to each polymerization technique (n = 8). The indirect composite resins (Targis and Solidex) were polymerized with their respective curing systems (Targis Power and EDG-lux); Charisma and Filtek Z250 were light-cured with conventional polymerization (halogen light) and additionally, with post-curing systems. Specimens were stored in artificial saliva at 37°C for one week. DTS tests were performed in a Universal Testing Machine (0.5 mm/min). The data were statistically analyzed by ANOVA and Duncan tests. The results were (MPa): Z250/EDG-lux: 69.04ª; Z250/Targis Power: 68.57ª; Z250/conventional polymerization: 60.75b; Charisma/Targis Power: 52.34c; Charisma/conventional polymerization: 49.17c; Charisma/EDG-lux: 47.98c; Solidex: 36.62d; Targis: 32.86d. The results reveal that the post-cured Z250 composite resin showed the highest DTS means. Charisma composite presented no significant differences when activation techniques were compared. Direct composite resins presented higher DTS values than indirect resins.

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