Deproteinization Treatment on Bond Strengths of Primary, Mature and Immature Permanent Tooth Enamel

2013 ◽  
Vol 37 (3) ◽  
pp. 275-280 ◽  
Author(s):  
S Aras ◽  
HC Küçükeçmen ◽  
Sönmez I öaroğlu
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tooth Enamel ◽  
Permanent Tooth ◽  
Permanent Teeth ◽  
Acid Etching ◽  
Control Groups ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Bond Strengths

Objective: The aim of this study was to examine the effect of pre-post deproteinization treatment with 5% sodium hypochloride on shear bond strength (sbs) of adhesive resin to primary, immature and mature permanent teeth enamel. Method: 30 teeth were used for each of primary, immature and mature permanent teeth groups. (totally 90). In control groups, enamel was etched for 60s with 37% phosphoric acid (3M) and rinsed for 10s (Procedure A). In experimental groups, deproteinization was applied with 5% NaOCI solution for 120s before (Procedure D+A) and after acid-etching (Procedure A+D). Gluma Comfort Bond (Heraeus-Kulzer) and Charisma (Heraeus-Kulzer) composite resin were applied to etched enamel surfaces. Data were determined with Two-Way ANOVA and LSD Multiple Comparison Test (p<0.05). Results: SBS was significantly lower in primary and immature permanent teeth than mature permanent teeth (p<0.05). “Procedure A+D” statistically increased sbs values in primary and immature permanent teeth (p<0.05). Conclusion: Deproteinization after acid etching significantly enhanced the shear bond strength values in primary and immature permanent teeth.

scholarly journals In Vitro Shear Bond Strength of Three Self-adhesive Resin Cements and a Resin-Modified Glass Ionomer Cement to Various Prosthodontic Substrates

2013 ◽  
Vol 38 (2) ◽  
pp. 186-196 ◽  
Author(s):  
Camila Sabatini ◽  
Manthan Patel ◽  
Eric D'Silva
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Glass Ionomer Cement ◽  
Glass Ionomer ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Setting Reaction ◽  
Resin Modified Glass Ionomer ◽  
Bond Strengths ◽  
Ionomer Cement

SUMMARY Objective To evaluate the shear bond strength (SBS) of three self-adhesive resin cements and a resin-modified glass ionomer cement (RMGIC) to different prosthodontic substrates. Materials and Methods The substrates base metal, noble metal, zirconia, ceramic, and resin composite were used for bonding with different cements (n=12). Specimens were placed in a bonding jig, which was filled with one of four cements (RelyX Unicem, Multilink Automix, Maxcem Elite, and FujiCEM Automix). Both light-polymerizing (LP) and self-polymerizing (SP) setting reactions were tested. Shear bond strength was measured at 15 minutes and 24 hours in a testing device at a test speed of 1 mm/min and expressed in MPa. A Student t-test and a one-way analysis of variance (ANOVA) were used to evaluate differences between setting reactions, between testing times, and among cements irrespective of other factors. Generalized linear regression model and Tukey tests were used for multifactorial analysis. Results Significantly higher mean SBS were demonstrated for LP mode relative to SP mode (p<0.001) and for 24 hours relative to 15 minutes (p<0.001). Multifactorial analysis revealed that all factors (cement, substrate, and setting reaction) and all their interactions had a significant effect on the bond strength (p<0.001). Resin showed significantly higher SBS than other substrates when bonded to RelyX Unicem and Multilink Automix in LP mode (p<0.05). Overall, FujiCEM demonstrated significantly lower SBS than the three self-adhesive resin cements (p<0.05). Conclusions Overall, higher bond strengths were demonstrated for LP relative to SP mode, 24 hours relative to 15 minutes and self-adhesive resin cements compared to the RMGICs. Bond strengths also varied depending on the substrate, indicating that selection of luting cement should be partially dictated by the substrate and the setting reaction.

scholarly journals Bond strength of modern self-adhesive resin cements to human dentin and different CAD/CAM ceramics

2020 ◽  
Vol 22 (2) ◽  
Author(s):  
Andrzej Małysa ◽  
Joanna Weżgowiec ◽  
Dariusz Danel ◽  
Klauss Boening ◽  
Katarzyna Walczak ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Shear Strength Test ◽  
Software Failure ◽  
Human Dentin ◽  
Cad Cam ◽  
Bond Strengths

Purpose: The aim of the study was to evaluate the shear bond strength of CAD/CAM ceramics to dentin after cementation with conventional or self-adhesive resin cements. Methods: Three self-adhesive, self-etching cements (Panavia SA, RelyX U200, Maxcem Elite), and one conventional cement (Panavia V5), were selected to lute three CAD/CAM ceramics (IPS Empress CAD, IPS e.max CAD, IPS e.max ZirCAD) onto the dentin. The bond strength was evaluated using a shear strength test according to the PN-EN ISO 29022:2013-10. Evaluation of the differences was performed using the Statistica software. Failure modes were analyzed using a light microscope. Results: All the studied cements differed (regardless of the ceramic type) in the bond strength. The highest bond strength was observed in Panavia V5, lower – in RelyX U200 and Panavia SA, and the lowest – in Maxcem. For IPS e.max ZirCAD, it was observed that compared to Panavia V5, the other cements were characterized by a significantly higher bond strength. For the IPS Empress CAD and the IPS e.max CAD, Panavia V5 displayed the highest bond strength. For all the studied self-adhesive cements, the failure of adhesion between the cement and dentin was predominant mode. Conclusions: Significant differences were found in the shear bond strengths of the CAD/CAM ceramics luted to dentin using tested self-adhesive and conventional cements. The bond strength depended on the combination of ceramic and cement. The IPS e.max ZirCAD had the highest bond strength to dentin after cementation with RelyX U200, while the IPS Empress CAD and IPS e.max CAD – with Panavia V5.

The Effect of Aging and Surface treatments on Micro-shear Bond Strength of Resin Nano-Ceramic Material Using Two Resin Cements

2020 ◽  
Author(s):  
Ayman Mohammed Said
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Surface Treatments ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Mean Values ◽  
Adhesive Resin Cement

Purpose: To evaluate the effect of aging and different surface treatments on micro-shear bond strength of two resin cements to resin nano-ceramic composite blocks using an in-vitro study. Materials and methods: Blocks of resin nano-ceramic (Lava Ultimate, 3M, St Paul, Minnesota, USA) were used to prepare eight plates having the following dimensions: (14mm × 12mm × 2mm). After plates preparation they were assigned to two main groups according to the surface treatment applied, either hydrofluoric acid etching and silane or sandblasting and silane. Scanning electron microscope (SEM) was used to analyze the surface topography of the Lava-Ultimate plates before and after application of surface treatments. Two resin cements were used; dual cured adhesive resin cement (Bifix QM, VOCO, Cuxhafen, Germany) and dual cured self-adhesive resin cement (Bifix SE, VOCO, Cuxhafen, Germany) to create a five resin micro-cylinders received on each lava ultimate plate. Ten specimens from each subgroup were tested after 24 hours and the other ten specimens were tested after aging in saline for 6 months. Micro-shear bond strength test was applied until failure. . Multi-factorial ANOVA test and One-way ANOVA followed by pair-wise Tukey’s post-hoc tests were used to analyze the data. Results: Both resin cements showed statistically significant decrease on bond strength after aging. Before aging, both surface treatments with adhesive resin cement showed statistically significant higher micro-shear bond strength mean values than with self-adhesive resin cement. After aging sandblasting showed a statistically significant higher micro-shear bond strength mean values with adhesive resin cement, while hydrofluoric acid etching revealed a statistically non-significant higher values with adhesive resin cement than self-adhesive resin cement. Conclusion: For both surface treatments and resin cements aging had a detrimental effect on micro- shear bond strength.

scholarly journals Effects of CPP-ACP Paste on the Shear Bond Strength of Orthodontic Brackets

2009 ◽  
Vol 79 (5) ◽  
pp. 945-950 ◽  
Author(s):  
Ding Xiaojun ◽  
Lu Jing ◽  
Guo Xuehua ◽  
Ruan Hong ◽  
Yu Youcheng ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Artificial Saliva ◽  
Orthodontic Brackets ◽  
Acid Etching ◽  
Bonding System ◽  
Significant Difference ◽  
Bond Strengths ◽  
Scanning Electron

Abstract Objective: To evaluate the effect of casein phosphopeptide–amorphous calcium phosphate (CPP-ACP) paste on shear bond strength and debonding failure modes of orthodontic brackets. Materials and Methods: Freshly extracted premolars were randomly divided into four groups (n =18) as follows: in groups 1 and 3, the enamel was treated with a solution of CPP-ACP dissolved in artificial saliva; groups 2 and 4 served as controls, and the enamel was treated with artificial saliva. After conventional acid etching, in groups 1 and 2, brackets were bonded using a light-cured bonding system (Blugloo); while in groups 3 and 4, brackets were bonded using a conventional bonding system (Unite Bonding Adhesive). Bonded specimens were subjected to thermal cycling for 1000 cycles before debonding procedures. After debonding, teeth and brackets were examined under a stereomicroscope at 10× magnification to determine whether any adhesive remained, in accordance with the adhesive remnant index. The acid-etched enamel surfaces were also observed using scanning electron microscopy after treatment with and without CPP-ACP paste. Results: The shear bond strengths of group 1 were significantly higher than those seen in group 2 (P < .01). There was no significant difference in the shear bond strengths of groups 3 and 4 (P > .05). Scanning electron microscopic observation showed that the pretreated enamel surface was rougher than that of the control surface after acid etching. Conclusion: The use of CPP-ACP can be considered as an alternative prophylactic application in orthodontic practice since it did not compromise bracket bond strength.

Incremental Layer Shear Bond Strength of Low-shrinkage Resin Composites Under Different Bonding Conditions

2014 ◽  
Vol 39 (6) ◽  
pp. 603-611 ◽  
Author(s):  
AH Al Musa ◽  
HNA Al Nahedh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Resin Composites ◽  
Adhesive Resin ◽  
Aging Conditions ◽  
Bond Strengths

SUMMARY The purpose of this study was to determine the incremental shear bond strength of a silorane-based composite (Filtek Silorane) repaired with silorane or a methacrylate-based composite (Filtek Z250) under various aging conditions. Also, the incremental bond strength of the silorane-based composite was compared with that of another low-shrinkage methacrylate-based composite (Aelite LS Posterior) under fresh and aged conditions, with and without the use of an adhesive resin between successive layers. The two brands of low-shrinkage composites were compared with a microhybrid, Filtek Z250, which served as the control. Substrate discs were fabricated and second layers were adhered to them immediately, after two weeks of aging, or after four weeks of aging and with and without an adhesive resin. Shear bond strengths were measured and failure modes were evaluated. The incremental bond strength of silorane to the silorane-based composite was not significantly different from that of the methacrylate-based composite. However, repairing a silorane-based composite with a methacrylate-based composite significantly reduced the bond strength. Aelite showed a lower incremental bond strength than Z250 and silorane, but the use of an adhesive significantly improved the bond strength. The absence of an oxygen-inhibited layer did not affect the bond strength of the consecutive layers of the silorane-based composite.

The Effect of Sandblasting and Different Primers on Shear Bond Strength Between Yttria-tetragonal Zirconia Polycrystal Ceramic and a Self-adhesive Resin Cement

2015 ◽  
Vol 40 (1) ◽  
pp. 63-71 ◽  
Author(s):  
Y-A Yi ◽  
J-S Ahn ◽  
Y-J Park ◽  
S-H Jun ◽  
I-B Lee ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Xrd Analysis ◽  
Resin Cement ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Adhesive Resin Cement ◽  
Tetragonal Zirconia Polycrystal

SUMMARY Purpose To evaluate the effect of zirconia primers, air-abrasion, and tribochemical surface treatment methods on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramic and self-adhesive resin cement. Methods and Materials Y-TZP ceramic surfaces were ground flat with 600-grit silicon carbide paper and then divided into seven groups of 10 and treated as follows: untreated (control), Monobond Plus, Z-PRIME Plus, ESPE Sil with CoJet, air-abrasion, Monobond Plus with air-abrasion, and Z-PRIME Plus with air-abrasion. Self-adhesive resin cement was placed onto the treated Y-TZP specimens for each group. All specimens were thermocycled and subjected to a shear bond strength test. Scanning electron microscope images of the fractured areas and x-ray diffraction (XRD) analysis of the surface-treated Y-TZP specimens were performed. Data were statistically analyzed using one-way analysis of variance and the Student-Newman-Keuls multiple comparison test (p<0.05). Results The Z-PRIME Plus treatment in combination with air-abrasion produced the highest bond strength (16.50±2.26 MPa), followed by air-abrasion (10.56±3.32 MPa), and then Monobond Plus combined with air-abrasion (8.93±3.13 MPa), ESPE Sil after CoJet application (8.54±3.98 MPa), and the Z-PRIME Plus group (8.27±2.79 MPa). The control (3.91±0.72 MPa) and Monobond Plus (4.86±1.77 MPa) groups indicated the lowest results (p<0.05). The XRD results showed the peaks of the monoclinic phase for the air-abrasion and CoJet treatment groups compared with the Y-TZP control. Conclusion Z-PRIME Plus primer application after air-abrasion presented the best results for improving the bond strength between Y-TZP ceramic and self-adhesive resin cement.

scholarly journals Shear Bond Strength of MDP-Containing Self-Adhesive Resin Cement and Y-TZP Ceramics: Effect of Phosphate Monomer-Containing Primers

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Jin-Soo Ahn ◽  
Young-Ah Yi ◽  
Yoon Lee ◽  
Deog-Gyu Seo
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Control Group ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Ceramic Surfaces ◽  
Adhesive Resin Cement

Purpose. This study was conducted to evaluate the effects of different phosphate monomer-containing primers on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramics and MDP-containing self-adhesive resin cement.Materials and Methods. Y-TZP ceramic surfaces were ground flat with #600-grit SiC paper and divided into six groups (n=10). They were treated as follows: untreated (control), Metal/Zirconia Primer, Z-PRIME Plus, air abrasion, Metal/Zirconia Primer with air abrasion, and Z-PRIME Plus with air abrasion. MDP-containing self-adhesive resin cement was applied to the surface-treated Y-TZP specimens. After thermocycling, a shear bond strength test was performed. The surfaces of the Y-TZP specimens were analyzed under a scanning electron microscope. The bond strength values were statistically analyzed using one-way analysis of variance and the Student–Newman–Keuls multiple comparison test (P<0.05).Results. The Z-PRIME Plus treatment combined with air abrasion produced the highest bond strength, followed by Z-PRIME Plus application, Metal/Zirconia Primer combined with air abrasion, air abrasion alone, and, lastly, Metal/Zirconia Primer application. The control group yielded the lowest results (P<0.05).Conclusion. The application of MDP-containing primer resulted in increased bond strength between Y-TZP ceramics and MDP-containing self-adhesive resin cements.

Shear Bond Strength of Self-etch Adhesives to Enamel with Additional Phosphoric Acid Etching

10.2341/07-63 ◽  
2008 ◽  
Vol 33 (2) ◽  
pp. 155-162 ◽  
Author(s):  
A-K. Lührs ◽  
S. Guhr ◽  
R. Schilke ◽  
L. Borchers ◽  
W. Geurtsen ◽  
...  
Keyword(s):  
Composite Materials ◽  
Phosphoric Acid ◽  
Bond Strength ◽  
Clinical Relevance ◽  
Shear Bond Strength ◽  
Acid Etching ◽  
Etch And Rinse ◽  
Bond Strengths ◽  
Self Etch ◽  
Phosphoric Acid Etching

Clinical Relevance When using self-etch adhesives to bond composite materials to enamel, there is concern about the ability to achieve bond strengths comparable to approved etch-and-rinse systems. An additional phosphoric acid etching can improve the shear bond strength of self-etch adhesives to enamel.

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