scholarly journals Fast and Efficient Separation and Determination of UV-absorbing Amino Acids, Nucleobases, and Creatinine Using a Carboxy-functionalized Cation-exchange Column

2015 ◽  
Vol 31 (5) ◽  
pp. 371-376 ◽  
Author(s):  
Yukio YOKOYAMA ◽  
Takeru FUJISHIMA ◽  
Kazuki KUROTA
Keyword(s):  
Amino Acids ◽  
Cation Exchange ◽  
Exchange Column ◽  
Efficient Separation ◽  
Cation Exchange Column

Determination of haemoglobin A1c by liquid chromatography using a new cation-exchange column

2003 ◽  
Vol 791 (1-2) ◽  
pp. 73-83 ◽  
Author(s):  
Maria Beatriz de la Calle Guntiñas ◽  
René Wissiack ◽  
Guy Bordin ◽  
Adela Rosa Rodrı́guez
Keyword(s):  
Liquid Chromatography ◽  
Cation Exchange ◽  
Haemoglobin A1c ◽  
Exchange Column ◽  
Cation Exchange Column

ANALYSIS FOR SMALL AMOUNTS OF CALCIUM, MAGNESIUM, BARIUM, AND SULPHATE USING PHTHALEIN PURPLE

1956 ◽  
Vol 34 (7) ◽  
pp. 921-925 ◽  
Author(s):  
J. R. McCallum
Keyword(s):  
Cation Exchange ◽  
Distilled Water ◽  
Complexometric Method ◽  
Exchange Column ◽  
Cation Exchange Column ◽  
Calcium Magnesium

For the determination of sulphate ion in samples containing 3 to 20 mgm., it was found that the standard precipitation techniques did not give sufficiently accurate results, and were time consuming. Reference to the literature showed that with certain modifications a complexometric method proposed by Schwarzenbach etal. for samples containing 20 to 50 mgm. of sulphate was most likely to give accurate results rapidly. In this method the sample is passed through a cation exchange column and washed with distilled water into a flask. This solution is boiled and precipitated with excess standard disodium ethylenediaminetetracetate in the presence of alcohol and ammonia using phthalein purple indicator. Provided that the details of procedure described in this paper are closely adhered to, accuracy is usually within two per cent. Calcium, magnesium, and barium may also be titrated directly using the phthalein purple indicator.

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