scholarly journals Altering the properties of the magnetic Co ferrite nanoparticles fabricated by modified inverse coprecipitation for high-frequency applications

2020 ◽  
Author(s):  
Rabea Al-Kershi ◽  
S. H. Aldirham
Keyword(s):  
High Frequency ◽  
Average Crystallite Size ◽  
Ferrite Nanoparticles ◽  
X Ray ◽  
Ft Ir ◽  
Coprecipitation Technique ◽  
Magnetic Ions ◽  
Average Lattice ◽  
Ft Ir Spectroscopy

Abstract Magnetic Co ferrite nanoparticles doped with non-magnetic ions (Zn2+) fabricated by modified inverse coprecipitation technique. X-ray calculations show that the average crystallite size (D) and the average lattice constant (a) of CoZn ferrite nanoparticles increase from 32.33 to 52.87 nm and from 8.39 to 8.41Ǻ respectively with increasing non-magnetic Zn2+ ions from 0.00 to 0.55. Morphological forms and M-O at A and B sites studied by SEM and FT-IR spectroscopy. Measurements of the structural, optical, electrical and magnetic characterization of the CoZn ferrite nanoparticles strongly depend on non-magnetic Zn2+ ions content (y). Non-magnetic ions transform Co ferrite from hard and dielectric nature to soft and semiconductor nature. Values of Coercivity and the remanence decrease as non-magnetic Zn2+ ions increases to the minimum values 955 Oe and 6 emu /g for the sample with Zn = 0.55. Co0.45Zn0.55Fe2O4 is might be suitable for high-frequency applications where it has the smallest value of optical gap, the largest value of resistivity and the lowest value of dielectric loss factor.

Synthesis and Characterization of TMA-A Zeolite Nanocrystals

2007 ◽  
Vol 124-126 ◽  
pp. 563-566
Author(s):  
Young Mi Kim ◽  
Seok Ju Lee ◽  
Ik Jin Kim
Keyword(s):  
Electron Microscopy ◽  
Environmental Scanning Electron Microscopy ◽  
Environmental Scanning ◽  
X Ray ◽  
Transmission Electron ◽  
Bet Analysis ◽  
Ft Ir ◽  
Average Lattice ◽  
Ft Ir Spectroscopy

Well-controlled cubic nanocrystal of TMA-A zeolite with a size of 60~100 nm were synthesized by a hydrothermal method in a solution having a Al(i-pro)3 : 2.2 TEOS : 2.4 TMAOH: 0.3 NaOH : 200H2O composition. The single TMA-A nanocrystals has an average lattice constant of 24.61 Å having a surface area of 742.36 m2/g. Thermal treatment of TMA zeolite crystals results in the formation of an amorphous above 900oC. Environmental scanning electron microscopy (ESEM). high resolution transmission electron microscopy(HRTEM), X-ray powder diffraction(XRD), fourier transform infrared(FT-IR) spectroscopy, DTA/TGA and BET analysis were used to characterize the initial materials and the obtained products after various heat treatments.

scholarly journals Growth and Characterization of Pure and Doped L-Alanine Tartrate Single Crystals

2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
K. Rajesh ◽  
B. Milton Boaz ◽  
P. Praveen Kumar
Keyword(s):  
Single Crystals ◽  
Vickers Microhardness ◽  
Diffraction Method ◽  
Dielectric Studies ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cell Parameters ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

Single crystals of pure and Lanthanum doped L-Alanine Tartrate were grown by slow evaporation method. The cell parameters were determined using single crystal X-ray diffraction method. To improve the physical properties of the LAT crystal, Lanthanum dopant was added by 2 mol%. ICP studies confirm the presence of Lanthanum in the grown LAT crystal. Transparency range of the crystal was determined using UV-VIS-NIR spectrophotometer. The functional groups of pure and doped LAT crystals were analyzed by FT-IR spectroscopy. Using Vickers microhardness tester, mechanical strength of the material was found. Dielectric studies of pure and doped LAT single crystals were carried out. The doped LAT crystal is found to have efficiency higher than that of pure LAT crystal.

Synthesis and Characterization of HgSe Nanostructure Using a Novel Precursor

2013 ◽  
Vol 32 (2) ◽  
pp. 157-162 ◽  
Author(s):  
Mahdiyeh Esmaeili-Zare ◽  
Masoud Salavati-Niasari ◽  
Davood Ghanbari
Keyword(s):  
Electron Microscopy ◽  
Synthesis And Characterization ◽  
Sonochemical Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Mercury Selenide ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

AbstractMercury selenide nanostructures were synthesized from the reaction of N, N′-bis(salicylidene)propane-1,3-diamine mercury complex, (Hg(Salpn)) as a novel precursor, via sonochemical method. The effect of different surfactant on the morphology and particle size of the products was investigated. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy and X-ray energy dispersive spectroscopy (EDS).

scholarly journals Synthesis and Characterization of New Polyimide/Organoclay Nanocomposites Containing Benzophenone Moieties in the Main Chain

2017 ◽  
Vol 57 (2) ◽  
Author(s):  
Khalil Faghihi ◽  
Mostafa Ashouri ◽  
Akram Feyzi
Keyword(s):  
Main Chain ◽  
In Situ Polymerization ◽  
Clay Content ◽  
Nanocomposite Films ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

<p>A series of nanocomposites consist of organic polyimide and organo-modified clay content varying from 0 to 5 wt%, were successfully prepared by in situ polymerization. Polyimide used as a matrix of nanocomposite was prepared through the reaction of 1,4-bis [4-aminophenoxy] butane (APB) and 3،3΄،4،4΄-benzophenone tetra carboxylic dianhydride (BTDA) in N,N-dimethylacetamide (DMAc). The resulting nanocomposite films were characterized by FT-IR spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM) and thermogravimetric analysis (TGA).</p>

Synthesis and Characterization of Structure of Fe3O4@Graphene Oxide Nanocomposites

2016 ◽  
Vol 25 (6) ◽  
pp. 096369351602500 ◽  
Author(s):  
Ruimin Fu ◽  
Mingfu Zhu
Keyword(s):  
Graphene Oxide ◽  
Drug Carrier ◽  
Precipitation Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Ft Ir ◽  
Co Precipitation ◽  
Ft Ir Spectroscopy

Nowadays, the hummers method for preparation of graphene oxide (GO) was improved. The grapheme oxide @ Fe3O4 magnetic nanocomposites were synthesized by co-precipitation method. After analysing the morphology and structure of obtained nanocomposites by X-ray diffraction (XRD), transmission electron microscope (TEM) and Fourier transform infrared (FT-IR) spectroscopy, the result was shown as follows. The particle size of Fe3O4 in nanocomposites is 30 nm. Many functional groups are found in grapheme oxide, and such groups could be used to bind with the drug. In the test for magnetic properties, the nanocomposites gathered rapidly in the vicinity of the permanent magnet. The nanocomposites, with high superparamagnetism, can be used in the following applications: drug targeting transports, drug carrier, and diagnosis assistant system.

scholarly journals Multicomponent Materials to Improve Solubility: Eutectics of Drug Aminoglutethimide

Crystals ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 40
Author(s):  
Basanta Saikia ◽  
Andreas Seidel-Morgenstern ◽  
Heike Lorenz
Keyword(s):  
Melting Point ◽  
Molar Ratio ◽  
Experimental Characterization ◽  
X Ray ◽  
Eutectic Mixtures ◽  
Ft Ir ◽  
Aqueous Solubilities ◽  
Ft Ir Spectroscopy

Here, we report the synthesis and experimental characterization of three drug-drug eutectic mixtures of drug aminoglutethimide (AMG) with caffeine (CAF), nicotinamide (NIC) and ethenzamide (ZMD). The eutectic mixtures i.e., AMG-CAF (1:0.4, molar ratio), AMG-NIC (1:1.9, molar ratio) and AMG-ZMD (1:1.4, molar ratio) demonstrate significant melting point depressions ranging from 99.2 to 127.2 °C compared to the melting point of the drug AMG (151 °C) and also show moderately higher aqueous solubilities than that of the AMG. The results presented include the determination of the binary melt phase diagrams and accompanying analytical characterization via X-ray powder diffraction, FT-IR spectroscopy and scanning electron microscopy.

scholarly journals Synthesis, characterization of Ag-doped CdS-WO2 nanocomposite and effects of photocatalytic degradation in RhB under visible light irradiation

2022 ◽  
Author(s):  
G. Roshini ◽  
V. Sathish ◽  
S. Manigandan ◽  
A. Tamilarasi ◽  
E. Priyanka
Keyword(s):  
Visible Light ◽  
Visible Light Irradiation ◽  
Photocatalytic Performance ◽  
Irradiation Time ◽  
Light Irradiation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

Abstract In this paper, the highly stable Ag/CdS-WO2 nanocomposite was fabricated by a facile and capping agent-free hydrothermal technique. The fabricated Ag doped CdS-WO2 nanocomposite were characterized by powder X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy and UV-vis diffuse reflectance (DRS) spectroscopy. The photocatalytic performance of synthesized photocatalysts was evaluated for the photodegradation of rhodamine B (Rh B) under visible light irradiation (VLI). The parameters used for the optimization of the photocatalyst were pH, catalyst dose, oxidant dose, and irradiation time. Based on this, a possible reaction mechanism for the enhancement of photocatalytic activity of Ag/CdS-WO2 has been proposed. Hence, we have a tendency to believe it might be a promising material that may be used for the photodegradation of organic pollutants present in wastewater.

Hydrothermal synthesis of a new lead(II) borate (Pb4O)Pb2B6O14-II

2016 ◽  
Vol 71 (12) ◽  
pp. 1233-1243 ◽  
Author(s):  
Sandra Schönegger ◽  
Klaus Wurst ◽  
Gunter Heymann ◽  
Hubert Huppertz
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Reaction ◽  
Rietveld Analysis ◽  
Lead Borate ◽  
X Ray Diffraction ◽  
Major Phase ◽  
X Ray ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

AbstractA new centrosymmetric modification of the lead borate (Pb4O)Pb2B6O14 has been obtained as a side phase through a facile hydrothermal reaction from Pb(BO2)2·H2O, H2O, and KOH as starting materials. The compound (Pb4O)Pb2B6O14-II crystallizes in the space group P1̅ (no. 2) with the lattice parameters a=695.9(3), b=778.0(3), c=1408.3(3) pm, α=97.35(1)°, β=100.39(1)°, and γ=103.02(1)°. The structure consists of anti-parallel arranged B6O14 chains and isolated oxygen-centered OPb4 tetrahedra. The compound Pb6B12O21(OH)6 constitutes the major phase of the synthesis, as verified through a Rietveld analysis. The characterization of (Pb4O)Pb2B6O14-II is based on a Rietveld analysis, single-crystal X-ray diffraction data, and FT-IR spectroscopy.

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