scholarly journals Determination of the response of pentaerythritol tetranitrate to static high pressure up to 4.2 GPa by neutron diffraction

1997 ◽  
Author(s):  
J.J. Dick ◽  
R.B. von Dreele
Keyword(s):  
High Pressure ◽  
Neutron Diffraction ◽  
Pentaerythritol Tetranitrate

scholarly journals Determination of hydrogen site and occupancy in hydrous Mg2SiO4 spinel by single-crystal neutron diffraction

2018 ◽  
Vol 74 (1) ◽  
pp. 115-120 ◽  
Author(s):  
Narangoo Purevjav ◽  
Takuo Okuchi ◽  
Xiaoping Wang ◽  
Christina Hoffmann ◽  
Naotaka Tomioka
Keyword(s):  
High Pressure ◽  
Neutron Diffraction ◽  
Single Crystal ◽  
Diffraction Analysis ◽  
Natural Occurrence ◽  
Hydration Mechanism ◽  
Neutron Time ◽  
Important Host ◽  
Pressure Synthesis

Ringwoodite [(Mg,Fe2+)2SiO4 spinel] has been considered as one of the most important host minerals of water in the Earth's deep mantle. Its extensive hydration was observed in high-pressure synthesis experiments and also by its natural occurrence. Water can dissolve into ringwoodite as structurally bound hydrogen cations by substituting other cations, although the hydrogen site and its occupancy remain unclear. In this study, neutron time-of-flight single-crystal Laue diffraction analysis was carried out for synthetic hydrous ringwoodite. Hydrogen cations were found only in the sites in MgO6 octahedra in the ringwoodite structure, which compensated the reduced occupancies of both magnesium and silicon cations. The refined cation occupancies suggest that the most plausible hydration mechanism is that three hydrogen cations simultaneously occupy an MgO6 octahedron, whereas four such hydrogenated octahedra surround a vacant SiO4 tetrahedron.

Determination of exchange and crystal field effects in Sm alloys by polarized neutron diffraction

1979 ◽  
Vol 40 (C5) ◽  
pp. C5-180-C5-182 ◽  
Author(s):  
J. X. Boucherle ◽  
D. Givord ◽  
J. Laforest ◽  
J. Schweizer ◽  
F. Tasset
Keyword(s):  
Neutron Diffraction ◽  
Crystal Field ◽  
Field Effects ◽  
Polarized Neutron

A NEUTRON DIFFRACTION DETERMINATION OF SHORT RANGE ORDER IN A Ni63.7Zr36.3 GLASS

1985 ◽  
Vol 46 (C8) ◽  
pp. C8-87-C8-92 ◽  
Author(s):  
R. Bellissent ◽  
J. Bigot ◽  
Y. Calvayrac ◽  
S. Lefebvre ◽  
A. Quivy
Keyword(s):  
Neutron Diffraction ◽  
Short Range ◽  
Short Range Order ◽  
Range Order ◽  
Diffraction Determination

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

Determination of Internal Stresses During Pearlite Transformation of 0.8c–1.5Mn Steel Through In-Situ Neutron Diffraction

2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Internal Stresses

scholarly journals New high-pressure phases of Fe7N3 and Fe7C3 stable at Earth's core conditions: evidences for carbon–nitrogen isomorphism in Fe-compounds

RSC Advances ◽  
2019 ◽  
Vol 9 (7) ◽  
pp. 3577-3581 ◽  
Author(s):  
Nursultan Sagatov ◽  
Pavel N. Gavryushkin ◽  
Talgat M. Inerbaev ◽  
Konstantin D. Litasov
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Ab Initio ◽  
Structure Prediction ◽  
Harmonic Approximation ◽  
Crystal Structure Prediction ◽  
Earth’S Core ◽  
Earth's Core ◽  
Core Conditions

We carried out ab initio calculations on the crystal structure prediction and determination of P–T diagrams within the quasi-harmonic approximation for Fe7N3 and Fe7C3.

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