Surface Roughness of Ceramic-Resin Composites After Femtosecond Laser Irradiation, Sandblasting or Acid Etching and Their Bond Strength With and Without Silanization to a Resin Cement

2019 ◽  
Vol 44 (2) ◽  
pp. 156-167 ◽  
Author(s):  
Z Demirtag ◽  
AK Culhaoglu
Keyword(s):  
Surface Roughness ◽  
Femtosecond Laser ◽  
Bond Strength ◽  
Laser Irradiation ◽  
Hydrofluoric Acid ◽  
Failure Modes ◽  
Resin Cement ◽  
Femtosecond Laser Irradiation ◽  
Acid Etching ◽  
Resin Composites

SUMMARY Objectives: The aim of this study was to investigate the effects of femtosecond laser irradiation, sandblasting, or acid etching treatments on the surface roughness of ceramic-resin composites and also shear bond strength (SBS) with and without silanization to a resin cement. Methods: Samples of Vita Enamic (VE; Vita Zahnfabrik, Bad Säckingen, Germany) and Lava Ultimate (LU; 3M ESPE, Seefeld, Germany) were classified into control (no treatment), sandblasting, hydrofluoric acid, and femtosecond laser groups (n=30). Surface roughness was determined using two-dimensional contact profilometry. Surface topography was evaluated using a three-dimensional contact profilometer and a scanning electron microscope. Then groups were divided into two subgroups with similar surface roughness values, including control (C), control + silane (C-S), sandblasting (SB), sandblasting + silane (SB-S), hydrofluoric acid (HF), hydrofluoric acid + silane (HF-S), femtosecond laser (FS), and femtosecond laser + silane (FS-S) groups (n=15). Panavia F 2.0 resin cement was applied to the sample surfaces using an SDI SBS rig (SDI Limited, Bayswater, Australia). The SBS test was performed after water storage (24 h, 37°C) and thermocycles (2000 cycles, 5°C to 55°C), and failure modes were evaluated. Results: The highest surface roughness was observed in the FS group, and the highest SBS was observed in the FS-S group for both VE and LU (p<0.001). Silanization improved the SBS of VE significantly (p<0.001) in all surface treatments but did not improve that of LU except in the FS group (p=0.004). There was a significantly moderate negative correlation in the VE/SB group (p=0.012) and a moderate positive correlation in the VE/HF group (p=0.049). Conclusions: Femtosecond laser irradiation was found to be more effective than sandblasting or acid etching in increasing the surface roughness, and it was also the most effective surface treatment with silanization on the SBS of a resin cement to the ceramic-resin composites.

scholarly journals Surface treatment and adhesion approaches on polymer-infiltrated ceramic network

2021 ◽  
Vol 20 ◽  
pp. e211670
Author(s):  
Michele Mirian May ◽  
Camila da Silva Rodrigues ◽  
Juliane Bortolotto Da Rosa ◽  
Júlia Persio Herrmann ◽  
Liliana Gressler May
Keyword(s):  
Contact Angle ◽  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Failure Modes ◽  
Contact Angles ◽  
Resin Cement ◽  
Acid Etching ◽  
Single Bond ◽  
Universal Adhesive ◽  
Angle Data

Aim: To evaluate the effect of different surface treatments and adhesive approaches on the microshear bond strength of resin cement to a polymer-infiltrated ceramic network (PICN). Methods: PICN blocks were randomly assigned into 9 groups (n=10): CTRL: no treatment; HF: 5% hydrofluoric acid etching; HF-S: HF + silane; HF-S-A: HF-S + adhesive (Adper Single Bond 2); HF-UA: HF + universal adhesive (Single Bond Universal); SB: sandblasting with 50 μm Al2O3 particles; SB-S: SB + silane; SB-S-A: SB-S + adhesive; SB-UA: SB + universal adhesive. Resin cement microcylinders (Ø = 0.96 mm; height = 1 mm) (RelyX Ultimate) were built upon the PICN surface after roughness and contact angle measurements. Next, microshear bonding tests (μSBS) were performed (0.5 mm/min) after water storage (37ºC, 90 days) and thermocycling (12,000 cycles; 5ºC-55ºC). Failure modes were observed under stereomicroscope. Bond strength data were analyzed by two-way ANOVA/Tukey’s test and t-tests. Kruskal-Wallis/Dunn’s tests were conducted for roughness and contact angle data (α = 0.05). Results: A rougher surface and lower contact angles were observed for Sandblasting. HF-S (18.54 ± 2.03 MPa), SB-S (19.00 ± 1.66 MPa) and SB-UA (18.07 ± 2.36 MPa) provided the highest bond strength values, followed by the other treated groups. The CTRL group resulted in lower bond strength (7.18 ± 2.34 MPa). Conclusion: Hydrofluoric acid etching followed by silane application and sandblasting followed by silane or universal adhesive are useful clinical steps to enhance bonding to PICN. Adhesive applications after HF etching have no advantages in bonding to PICN.  

scholarly journals Effect of surface treatment on the shear bond strength of a resin-based cement to porcelain

2006 ◽  
Vol 17 (4) ◽  
pp. 290-295 ◽  
Author(s):  
Marcos Paulo Nagayassu ◽  
Luciana Keiko Shintome ◽  
Eduardo Shigueyuki Uemura ◽  
José Eduardo Junho de Araújo
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
In Vitro Study ◽  
Resin Cement ◽  
Vitro Study ◽  
Acid Etching ◽  
And Control

The purpose of this in vitro study was to evaluate the effect of different surface treatments on the shear bond strength of a resin-based cement to porcelain. Sixty pairs of 50% aluminous porcelain discs were fabricated. In each pair, one disc measured 6 mm in diameter X 3 mm thickness (A) and the other measured 3 mm in diameter X 3mm thickness (B). The specimens were randomly assigned to 6 groups (n=10 pairs of discs), according to the surface treatment: etching with 10% hydrofluoric acid for 2 or 4min (G1 and G2); 50-µm particle aluminum oxide sandblasting for 5 s (G3); sandblasting followed by etching for 2 or 4min (G4 and G5) and control - no treatment (G6). A silane agent was applied to the treated surface of both discs of each pair. Bistite II DC dual-cure resin cement was applied and the B discs were bonded to their respective A discs. Specimens were stored in distilled water at 37ºC for 24 h and were tested in shear strength at a crosshead speed of 2 mm/min. Means in MPa were: G1: 14.21 ± 4.68; G2: 8.92 ± 3.02; G3: 10.04 ± 2.37; G4: 12.74 ± 5.15; G5: 10.99 ± 3.35; G6: 6.09 ± 1.84. Data were compared by one-way ANOVA and Tukey's test at 5% significance level. Bond strength recorded after 2-min acid etching was significantly higher than 4-min etching (p<0.05) and control (p<0.05), but did not differ significantlyfrom sandblasting alone (p>0.05) or followed by etching for 2 or 4 min (p>0.05). Within the limitations of an in vitro study, it may be concluded that 2-min hydrofluoric acid etching produced a favorable micromechanical retention that enhanced resin cement bond strength to porcelain.

scholarly journals Fabrication of concave spherical microlenses on silicon by femtosecond laser irradiation and mixed acid etching

2014 ◽  
Vol 22 (12) ◽  
pp. 15245 ◽  
Author(s):  
An Pan ◽  
Bo Gao ◽  
Tao Chen ◽  
Jinhai Si ◽  
Cunxia Li ◽  
...  
Keyword(s):  
Femtosecond Laser ◽  
Laser Irradiation ◽  
Femtosecond Laser Irradiation ◽  
Acid Etching ◽  
Mixed Acid

The Effect of Aging and Surface treatments on Micro-shear Bond Strength of Resin Nano-Ceramic Material Using Two Resin Cements

2020 ◽  
Author(s):  
Ayman Mohammed Said
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Surface Treatments ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Mean Values ◽  
Adhesive Resin Cement

Purpose: To evaluate the effect of aging and different surface treatments on micro-shear bond strength of two resin cements to resin nano-ceramic composite blocks using an in-vitro study. Materials and methods: Blocks of resin nano-ceramic (Lava Ultimate, 3M, St Paul, Minnesota, USA) were used to prepare eight plates having the following dimensions: (14mm × 12mm × 2mm). After plates preparation they were assigned to two main groups according to the surface treatment applied, either hydrofluoric acid etching and silane or sandblasting and silane. Scanning electron microscope (SEM) was used to analyze the surface topography of the Lava-Ultimate plates before and after application of surface treatments. Two resin cements were used; dual cured adhesive resin cement (Bifix QM, VOCO, Cuxhafen, Germany) and dual cured self-adhesive resin cement (Bifix SE, VOCO, Cuxhafen, Germany) to create a five resin micro-cylinders received on each lava ultimate plate. Ten specimens from each subgroup were tested after 24 hours and the other ten specimens were tested after aging in saline for 6 months. Micro-shear bond strength test was applied until failure. . Multi-factorial ANOVA test and One-way ANOVA followed by pair-wise Tukey’s post-hoc tests were used to analyze the data. Results: Both resin cements showed statistically significant decrease on bond strength after aging. Before aging, both surface treatments with adhesive resin cement showed statistically significant higher micro-shear bond strength mean values than with self-adhesive resin cement. After aging sandblasting showed a statistically significant higher micro-shear bond strength mean values with adhesive resin cement, while hydrofluoric acid etching revealed a statistically non-significant higher values with adhesive resin cement than self-adhesive resin cement. Conclusion: For both surface treatments and resin cements aging had a detrimental effect on micro- shear bond strength.

Fabrication of through holes in silicon carbide using femtosecond laser irradiation and acid etching

2014 ◽  
Vol 289 ◽  
pp. 529-532 ◽  
Author(s):  
Vanthanh Khuat ◽  
Yuncan Ma ◽  
Jinhai Si ◽  
Tao Chen ◽  
Feng Chen ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Femtosecond Laser ◽  
Laser Irradiation ◽  
Femtosecond Laser Irradiation ◽  
Acid Etching

Uniform nano-ripples on the sidewall of silicon carbide micro-hole fabricated by femtosecond laser irradiation and acid etching

2014 ◽  
Vol 104 (24) ◽  
pp. 241907 ◽  
Author(s):  
Vanthanh Khuat ◽  
Tao Chen ◽  
Bo Gao ◽  
Jinhai Si ◽  
Yuncan Ma ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Femtosecond Laser ◽  
Laser Irradiation ◽  
Femtosecond Laser Irradiation ◽  
Acid Etching ◽  
Micro Hole

scholarly journals Bond and topography evaluation of a Y-TZP ceramic with a superficial low-fusing porcelain glass layer after different hydrofluoric acid etching protocols

2018 ◽  
Vol 47 (6) ◽  
pp. 348-353
Author(s):  
Arthur Chaves SIMÕES ◽  
Jean Soares MIRANDA ◽  
Rodrigo Othávio de Assunção e SOUZA ◽  
Estevão Tomomitsu KIMPARA ◽  
Fabíola Pessôa Pereira LEITE
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Statistical Tests ◽  
Adhesive Bond ◽  
Surface Treatments ◽  
Resin Cement ◽  
Acid Etching ◽  
Glass Layer ◽  
Ceramic Surface ◽  
Adhesive Failure

Abstract Introduction Despite being one of the most studied ceramics today, zirconia still does not have a well-defined adhesion protocol. Objective Evaluate the influence of different etching times and hydrofluoric acid (HF) concentrations on the zirconia surface and bond strength between a vitrified Y-TZP ceramic and a resin cement. Materials and method The zirconia surface treatments were: sandblasting with silica-coated alumina (Co); glaze application + 5% HF etching for 5s (G5-5s), 10s (G5-10s) or 20s (G5-20s); glaze application + 10% HF etching for 5s (G10-5s), 10 (G10-10s) or 20s (G10-20s) . Then, cement cylinders (3.3 × 3.3 mm) were built up for shear bond test on all specimens. The specimens were subjected to 6000 thermal cycling before the test. Fractures were analyzed by stereomicroscope. Data were statistically analyzed by Kruskal-Wallis and Dunn statistical tests (5%). Extra samples of each group were made to obtain profilometry and scanning electron microscopy (SEM). Result Zirconia-cement bond strength was affected by the ceramic surface treatments (p = 0.001). G10-5s (2.71 MPa) recorded the highest bond strength values, followed by the Co (2.05 MPa) while G5 groups had the lowest bond value. Adhesive failure of the samples predominated. The image analysis revealed G5 groups seem to have a lower roughness when compared to groups treated by 10% HF. The creation of pores in the low-fusing porcelain glass layer surface occurred only when 10% HF was used. Conclusion The low-fusing porcelain glass layer application was able to overcome the sandblasting and obtain a greater adhesive bond to the resinous cement, however, only when 10% HF was used for an interval of 5 seconds.

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