The goal of this research is to obtain experimental information about combustion characteristics of the composite propellant containing various metallic fuels. The propellant formulations contained two fractions of ammonium perchlorate (64.6%), inert binder (19.7%) - butadiene rubber SKD plastized with transformer oil, and metal fuel (15.7% of aluminum ASD-4, ASD-6, Alex; boron; aluminum diboride; aluminum dodecaboride; some mixtures of above listed ingredients). Experimental information will be used further as a background to develop the physical and mathematical model of combustion process.