Characterization of the Role of Post-Build Heat Treatment on the Localized Corrosion Susceptibility of Laser Powder Bed Fused Inconel 718 Parts

Author(s):  
Joshua P. James

Abstract As more industries look toward additively manufactured (AM) components to combat lead times, re-design, cost of complexity, etc., those industries are faced with re-evaluating the performance of AM-based materials as compared to their well-documented wrought or machined counterparts. A particular alloy of interest to many industries including aerospace and energy/power generation is Inconel 718 due to its resistance to oxidation and high temperature degradation [1]. Additively manufactured Inconel 718 parts typically receive a series of post-build heat treatments prior to deployment. If not properly controlled, these post-build treatments may introduce secondary precipitates and other inhomogeneities that will affect the parts’ mechanical properties and susceptibility to corrosion. This is specifically true of susceptibility to localized corrosion mechanisms that may lead to crack initiation, accelerated crack growth and ultimately premature failure. By utilizing electrochemical parameter testing to analyze for localized breakdown potentials, this work investigates the variation in tolerance to localized corrosion that results from common post-build heat treatment steps and the secondary phase precipitation that can ensue in Inconel 718 AM parts.

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 266
Author(s):  
Wakshum M. Tucho ◽  
Vidar Hansen

The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is, however, not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. Despite this, the highest hardness obtained after aging for ST temperatures (970–1250 °C) is at 1100 °C/1 as we have ascertained in our previous studies. The unreleased residual stresses in the retained lattice defects potentially affect other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the hardness after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16, or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43–49%. The high density of annealing twins evolved during 3 h of ST and only slightly varies for longer ST.


Author(s):  
Wakshum Tucho ◽  
Vidar Hansen

The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is however not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. In spite this, the highest hardness obtained after aging for ST temperatures (970 - 1250 °C) is at 1100 °C/1h [1]. The unreleased residual stresses in the retained lattice defects are potentially affecting other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the strength after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16 or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43 – 49 %, depending on hold time. A high density of annealing twins evolved during 3 h of ST and the quantity only slightly varies for longer ST.


2019 ◽  
Vol 35 (6) ◽  
pp. 1153-1164 ◽  
Author(s):  
Le Zhou ◽  
Abhishek Mehta ◽  
Brandon McWilliams ◽  
Kyu Cho ◽  
Yongho Sohn

Materials ◽  
2019 ◽  
Vol 12 (11) ◽  
pp. 1742 ◽  
Author(s):  
Marina Cabrini ◽  
Sergio Lorenzi ◽  
Cristian Testa ◽  
Fabio Brevi ◽  
Sara Biamino ◽  
...  

The effect of microstructure on the susceptibility to selective corrosion of Alloy 625 produced by laser powder bed fusion (LPBF) process was investigated through intergranular corrosion tests according to ASTM G28 standard. The effect of heat treatment on selective corrosion susceptibility was also evaluated. The behavior was compared to commercial hot-worked, heat treated Grade 1 Alloy 625. The morphology of attack after boiling ferric sulfate-sulfuric acid test according to ASTM G28 standard is less penetrating for LPBF 625 alloy compared to hot-worked and heat-treated alloy both in as-built condition and after heat treatment. The different attack morphology can be ascribed to the oversaturation of the alloying elements in the nickel austenitic matrix obtained due to the very high cooling rate. On as-built specimens, a shallow selective attack of the border of the melt pools was observed, which disappeared after the heat treatment. The results confirmed similar intergranular corrosion susceptibility, but different corrosion morphologies were detected. The results are discussed in relation to the unique microstructures of LPBF manufactured alloys.


Materialia ◽  
2021 ◽  
pp. 101272
Author(s):  
R. Jayaraj ◽  
Punit Kumar ◽  
Hang Li Seet ◽  
Sharon M.L. Nai ◽  
Pei Wang ◽  
...  

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