Microstructural Evolution and Deformation Behavior of Stainless Steel in Semi-Solid State

Author(s):  
Jing Yuan Li ◽  
Sumio Sugiyama ◽  
Jun Yanagimoto
2006 ◽  
Vol 116-117 ◽  
pp. 681-685 ◽  
Author(s):  
Jing Yuan Li ◽  
Sumio Sugiyama ◽  
Jun Yanagimoto

Thixoforming or Semi-Solid Metal Forming offers many advantages in comparison with casting and conventional forging. The purpose of the present study is to provide the basic microstructure and deformation data for austenitic and ferritic stainless steel under mushy state. As well known, the stainless steels solidify in different modes according to the different chemical compositions. In this paper, microstructural evolution of austenitic stainless steel type 304 which solidifies in FA mode ( L → L +δ → L +δ +γ →δ +γ →γ ),austenitic stainless steel type 310S which solidifies in A mode ( L → L +γ →γ ), and ferritic stainless steel type 430 which solidifies in F mode ( L → L +δ →δ )are investigated during partial remelting by way of SIMA (Strain Induced Melted Activation). The results show that A and F mode of stainless steels melt directly at the grain boundary without phase transformation during reheating. A banded structure, originating from the primary dendritic segregation of the original ingots, is observed in type 310S steel during further heating. On the other hand, a perfect globular and insegregative two-phase semi-solid structure L +δ can be obtained while heated beyond the banded three-phase L +δ +γ semi-solid state in FA mode austenitic stainless steel type 304. This spheroidization can be attributed to the peritectic reaction occurred in the L +δ +γ semi-solid state. In addition, simple compression tests of these alloys in semi-solid state for varied combination of deformation rate and deformation temperature are conducted to examine the deformation behavior of stainless steel. Flow stress curves exhibit abrupt change in various alloys, even though in the same alloy such as type 304, various flow stresses are observed according to the difference in inner microstructure or morphology. Stress of type 310S steel shows the most reduction as the deformation temperature increasing at the same strain rate condition. The Liquid is centralized to periphery by the compression force in all deformed test pieces. Fracture, observed in all alloys except type 304 steel in globular L +δ semi-solid state, should be resulted from the lack of liquid in L +δ +γ state of type 304 steel and solidification crack in type 310S and type 430 steel. Deformation of solid particles occurs only in L +δ +γ state of type 304 steel. Last in this paper, various deformation mechanisms are proposed for various microstructures.


2009 ◽  
Vol 506 (1-2) ◽  
pp. 8-15 ◽  
Author(s):  
Zude Zhao ◽  
Qiang Chen ◽  
Yanbin Wang ◽  
Dayu Shu

1998 ◽  
Vol 46 (18) ◽  
pp. 6351-6360 ◽  
Author(s):  
H Iwasaki ◽  
T Mori ◽  
M Mabuchi ◽  
K Higashi

2015 ◽  
Vol 651-653 ◽  
pp. 1545-1550 ◽  
Author(s):  
Alfredo Hernández ◽  
J. Federico Chávez ◽  
Raquel E. Hernández

A rheocasting prototype for the semi-solid processing of Al-Si alloys was designed and assembled at laboratory scale, this is the first attempt for the development of S2P equipment in Mexico. This work describes the simplified method of mechanical stirring and the calculation of the theoretical parameters for the operation of the experimental device in order to provide shear rate into the slurry by a stainless steel impeller inside a crucible made of hot work steel. Moreover, a vertical pressure die-rheocasting system it is applied with the semi-solid alloy flowing counter the position of the injector during the displacement of the crucible in order to fill the mold. New design is applied in this rheocasting equipment.The semi-solid state with thixotropic behavior is produced in the stirred AlSi7Mg alloy; this condition allows the non-dendritic morphology because the intensively stirring at the beginning of the solidification produces the trimming of dendrites, growing so the primary solid (α) in globular shape surrounded by eutectic microstructure. Preliminary microstructural characterization was performed.


2005 ◽  
Vol 54 (4-5) ◽  
pp. 423-430 ◽  
Author(s):  
Yalin Lu ◽  
Miaoquan Li ◽  
Weichao Huang ◽  
Haitao Jiang

2021 ◽  
Vol 143 (5) ◽  
Author(s):  
Paul S. Korinko

Abstract Microstructure development is examined for a specialized spot weld that is used as a solid-state closure process for austenitic stainless steel tubing, referred to as pinch welding. In order to elucidate the microstructural evolution of the weld, a series of test welds were made at nominal conditions using tubing and production like components. These pinch welds normally terminate after twelve cycles of a 60 Hz AC weld process. In this study, production tubes were welded from one to twelve cycles and the microstructure and weld variables after each individual weld cycle number were characterized using radiography and optical metallography. Two electrochemical etchants were used to highlight different microstructural features. The study revealed that: (1) this type pinch weld is largely complete after about six cycles of 60 Hz AC current, half the weld time utilized; (2) the resistance, deformation, and closure length approach “steady-state” conditions after six cycles; and (3) both oxalic and nitric acid electrolytic etchants are useful for highlighting specific microstructural attributes of type 304 L stainless steel. Finally, two distinct microstructural regions can be identified for these welds: the edge of the weld, which is driven by concentrated deformation, recrystallization, and grain growth, and the center region, which is more typical of forge welding and micro-asperity breakdown followed by diffusion and grain-growth.


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