Improvement in the Thermal Shock Resistance of Zirconia Ceramic by the Addition of Aluminium Titanate

2011 ◽  
Vol 194-196 ◽  
pp. 1724-1727 ◽  
Author(s):  
Heng Yong Wei ◽  
Li Xue Yu ◽  
Zhi Fa Wang ◽  
Jing Long Bu ◽  
Shu Long Ma ◽  
...  
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Sem Analysis ◽  
Precipitation Method ◽  
Zirconia Ceramic ◽  
Aluminum Titanate ◽  
Sintering Properties ◽  
Shock Resistance ◽  
Co Precipitation

ZrO2-Al2TiO5 composite materials with high bending strength and good thermal shock resistance expansion were prepared using partially stabilized zirconia (Y-PSZ) powders coated with Al2TiO5 by co-precipitation method. The effects of Al2TiO5 content on the sintering properties, phase composition, microstructure and thermal shock resistance of the zirconia ceramic were investigated．The results show that the apparent porosity of the samples decreased and their bending strength increased with the content of aluminum titanate increasing from 0 to 8 wt%. The samples with 5 and 8 wt% aluminum titanate addtion have excellent thermal shock resistance. The results showed that the addtion of aluminum titanate could enhance the mechanical strength and improve the thermal shock resistance of zirconia ceramic. The XRD and SEM analysis results indicated that the propriety improvement is relative with the change of the microstructure and the increase of tetragonal ZrO2 phase in the composites.

Effect of Molar Ratio of Al2O3 to Fe2O3 on the Sintering and Thermal Shock Resistance of Al2O3-Fe2O3 Composite

2011 ◽  
Vol 194-196 ◽  
pp. 1745-1748
Author(s):  
Zhi Fa Wang ◽  
Jian Sheng Wang ◽  
Yue Jun Chen ◽  
Li Xue Yu ◽  
Jing Long Bu ◽  
...  
Keyword(s):  
Composite Materials ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Raw Materials ◽  
Sem Analysis ◽  
Molar Ratio ◽  
Alumina Powder ◽  
Linear Change ◽  
Shock Resistance

The Al2O3-Fe2O3 composite was prepared at 1550°C for 3h with alumina powder and ferric oxide powder as raw materials and with magnesia powder as additive. The effect of molar ratio of Al2O3 to Fe2O3 on the sintering and thermal shock resistance of the composite materials was studied. The results showed that the apparent porosity and bulk density of the samples both decreased with the molar ratio of Al2O3 to Fe2O3 increase, as a result, the linear change ratio and bending strength both increased. When the molar ratio of Al2O3 to Fe2O3 equals to 3, the sample exhibits excellent thermal shock resistance. The XRD and SEM analysis results indicated that the mechanical and thermal proprieties are relative to the microstructure and crystal phases of the composite materials.

Study of Thermal Shock Resistance of Sagger Plate Used in Floppy Magnets Sintering

2007 ◽  
Vol 280-283 ◽  
pp. 1667-1670 ◽  
Author(s):  
Feng Cao ◽  
Xing Rong Wu ◽  
Rainer Telle
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Rapid Development ◽  
Particle Surface ◽  
Sem Analysis ◽  
Sintering Process ◽  
Kiln Furniture ◽  
Dense Structure ◽  
Zircon Powder ◽  
Shock Resistance

The rapid development of magnetic materials has witnessed a sustained consumption increase in corundum-mullite kiln furniture application, yet a comparatively short duration of them. In this view, the thermal shock resistance of sagger plate in floppy magnets sintering turns out a factor of critical importance. This paper makes a study concerning the influence of factors including the size of critical electro-melted mullite particles, the electro-melted corundum or mullite as medium particles and the addition of upon the thermal shock resistance. The result shows that, with critical particles of 2 mm, the sheet of about 10mm thickness is characterized by better performance in modulus of rapture and thermal shock resistance. The latter proves to be more outstanding in samples rather than mullite. When zircon powder is added in a two-hour sintering process at the temperature of 1550°C, a remarkable improvement is made by the sample in terms of its thermal shock resistance. SEM analysis shows the existence of micropores in the section of samples with corundum as medium particles, whereas the glasses phase in that of mullite sample, resulting in a dense structure. Finally, zircon powder added makes for the improvement of thermal shock resistance due to the formation of baddeleyite on the particle surface of the corundum.

scholarly journals High Temperature Bending Strength and Thermal Shock Resistance of Carbon-Ceramics Composites

TANSO ◽  
1985 ◽  
Vol 1985 (120) ◽  
pp. 21-27 ◽  
Author(s):  
Kenji Miyazaki ◽  
Hisayoshi Yoshida ◽  
Kazuo Kobayashi
Keyword(s):  
High Temperature ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Shock Resistance

Development of Aluminum Titanate-Mullite Composite Having High Thermal Shock Resistance

1986 ◽  
Vol 69 (10) ◽  
pp. C-226-C-227 ◽  
Author(s):  
Hiroyuki Morishima ◽  
Zenji Kato ◽  
Keizo Uematsu ◽  
Katsukazu Saito ◽  
Toyohiko Yano ◽  
...  
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Aluminum Titanate ◽  
Shock Resistance ◽  
High Thermal Shock Resistance

Study on Thermal Shock Resistance of Nano-CeO2–Y2O3 Co-Stabilized ZrO2 (CYSZ) Ceramic Powders Thermal Barrier Coating of Aircraft Engine

2019 ◽  
Vol 14 (11) ◽  
pp. 1597-1605
Author(s):  
Yang Lyu ◽  
Xuan Shao ◽  
Wen-Xue Wang ◽  
Hui Tang
Keyword(s):  
Thermal Shock ◽  
Thermal Barrier Coating ◽  
Thermal Shock Resistance ◽  
Ceramic Coatings ◽  
Precipitation Method ◽  
Thermal Barrier ◽  
Ceramic Powders ◽  
Alloy Matrix ◽  
Barrier Coating ◽  
Shock Resistance

In this paper, nano-CeO2–Y2O3 co-stabilized ZrO2 ceramic powders (CYSZ) were firstly prepared by co-precipitation method, and CYSZ powder was spray-granulated, followed by thermal plasma spraying of nano-CYSZ thermal barrier coating on 35Cr2Ni4 MoA alloy matrix. After XRD and SEM analysis, the five CYSZ ceramic coatings (CeO2 content 0, 1, 5, 10, 15 mol%) prepared were tetragonal phase structures before and after the thermal shock experiment, and the thickness of CYSZ ceramic coating was about 200 μm. Adding appropriate amount of nano CeO2 promoted the formation of micro-cracks in the coating, released the coating stress, slowed down the thermal shock damage process, and prevented the transformation from t-ZrO2 to m-ZrO2. The AFM morphology showed that the coating surface grains grow vertically after thermal shock cycle, which indicated that the entry of Ce4+ into ZrO2 lattice resulted in lattice distortion and made the grains more stable. When the content of CeO2 is 1 mol%, the thermal shock resistance excellent is 84 times. Therefore, the addition of CeO2 can effectively improve the thermal shock resistance performance of CYSZ thermal barrier coating, meeting the requirements of high temperature working conditions of aeroengine and hot-end components.

Influence of Additives on Performance of Silicon Carbide Refractory

2012 ◽  
Vol 538-541 ◽  
pp. 2277-2280
Author(s):  
You Fu Guo ◽  
Ming Yue Zheng ◽  
Jing Long Bu ◽  
Yue Jun Chen ◽  
Li Xue Yu ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Thermal Expansion ◽  
Bulk Density ◽  
Thermal Shock ◽  
Silica Fume ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Carbide Refractory ◽  
Shock Resistance ◽  
Silicon Carbide Refractory

Silicon carbide with diffierent granularity was used as raw material, quartz, silica fume, aluminum powder or alumina was used as additive with dosages of 1% (in mass, similarly hereinafter), 3% and 5%. Silicon carbide refractory material was prepared in oxidizing atmosphere at 1400 °C for 3 h. Performence of samples were researched by measurements of apparent porosity, bulk density, bending strength at room temperature, thermal shock resistance and thermal expansion rate, and analyzed by SEM. The results showed that samples added silica fume have low thermal expansion rate and apparent porosity, high bending strength and bulk density, good thermal shock resistance, compact texture as well. It can be deduced that 5% silica fume plays the excellent role to improve integrated performance of silicon carbide refractory material.

Microstructure and Thermal Shock Behaviour of Alumina Composite Ceramic for Heat Transmission Pipeline

2014 ◽  
Vol 692 ◽  
pp. 217-223 ◽  
Author(s):  
Xiao Hong Xu ◽  
Xiao Yang Xu ◽  
Jian Feng Wu ◽  
Yang Zhou ◽  
De Zhi He
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Raw Materials ◽  
Composite Ceramic ◽  
Alumina Powder ◽  
Monoclinic Zirconia ◽  
Heat Transmission ◽  
Transmission Pipeline ◽  
Shock Resistance

Al2O3 composite ceramics materials used for heat transmission pipeline were prepared by pressureless sintering in air. Calcined bauxite, talc and commercial alumina powder were used as the main raw materials, partially stabilized zirconia was also added to improve the thermal shock resistance of the samples. The effects of composition and sintering temperature on density, phase composition, microstructure and thermal shock behavior of samples were evaluated. It shows that the B2 sample which was sintered at 1400 °C for 2 h has optimal properties with porosity 0.4%, bulk density 3.2 g•cm-3.The bending strength increases 19.46 MPa after 30 times thermal shock cycles from 1100 °C to room temperature. The main phases of B2 are corundum and spinel, meanwhile, a small amount of monoclinic zirconia and α-quartz are also detected according to XRD pattern. Microstructure analysis reveals that spinel crystals are interlocked by prismatic corundum crystals, bright white beaded monoclinic zirconia particles are distributed uniformly, and it is beneficial to improve the thermal shock resistance of sample.

Effect of MgTi2O5 Addition on Thermal Shock Resistance of Al2TiO5

2007 ◽  
Vol 280-283 ◽  
pp. 1187-1190 ◽  
Author(s):  
Qiang Shen ◽  
Yong Hu ◽  
Chuan Bin Wang ◽  
Ming Zhong Li ◽  
Lian Meng Zhang
Keyword(s):  
Solid Solution ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Experimental Results ◽  
Aluminum Titanate ◽  
Shock Resistance

In the present paper, magnesium dititanate (MgTi2O5, M2T) was introduced into aluminum titanate (Al2TiO5, AT) to form AT-M2T solid solution so that the thermal shock resistance of Al2TiO5 could be kept still good while without any decomposition. The effect of MgTi2O5 addition on thermal shock resistance of Al2TiO5 was investigated. The experimental results showed that the thermal shock resistance of Al2TiO5 began to decrease when a little amount of MgTi2O5 was added and then rose with the continuous addition of MgTi2O5, even overrunning that of pure Al2TiO5 when 30mol% MgTi2O5 was contained. It was found that fine solid solution was formed between Al2TiO5 and MgTi2O5, which enhanced the thermal shock resistance of Al2TiO5.

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