Raman Spectroscopic Characterization of Carbon Nanofibers Obtained by Using Metal Chloride as Catalyst Precursor

2007 ◽  
Vol 561-565 ◽  
pp. 1387-1390
Author(s):  
Fei Li ◽  
Xiao Ping Zou ◽  
Jin Cheng ◽  
Hong Dan Zhang ◽  
Peng Fei Ren ◽  
...  

Carbon nanofibers have been obtained by the interaction of ethanol with metal chloride over copper plate. Different metal chloride was used as the catalyst precursor. The products were characterized by the Raman spectroscopy for the degree of graphitization. The relative intensities and the amount of amorphous carbon were estimated. The results indicate that the catalyst precursor has effects on the degree of graphitization of carbon nanofibers.

1999 ◽  
Vol 14 (12) ◽  
pp. 4474-4477 ◽  
Author(s):  
M. Endo ◽  
K. Nishimura ◽  
Y. A. Kim ◽  
K. Hakamada ◽  
T. Matushita ◽  
...  

Variations of the properties of submicron vapor-grown carbon fibers (VGCFs) and nanofibers, with diameters around 0.1–0.2 μm and 80–100 nm, respectively, are observed by Raman spectroscopy as a function of heat-treatment temperature. The microstructural evolution strongly depends on the original properties of the material, such that the main transition temperatures associated with the onset for establishing two-dimensional graphene ordering are defined below 1500 °C for the nanofibers and 2000 °C for the submicron VGCFs, respectively. The relative intensities (ID/IG) of the as-grown phase for submicron VGCFs and nanofibers are 3.44 and 1.35, while those for the corresponding graphitized samples are 0.393 and 0.497, respectively.


2007 ◽  
Vol 26-28 ◽  
pp. 809-812
Author(s):  
Fei Li ◽  
Xiao Ping Zou ◽  
Jin Cheng ◽  
Hong Dan Zhang ◽  
Peng Fei Ren ◽  
...  

Catalytic grown carbon nanofibers have been obtained from decomposition of ethanol over copper plate. Ferric chloride of different concentration was employed as the catalyst precursor. Scanning electron microscopy has shown that different morphologies of carbon nanofibers can be obtained by using different concentration of catalyst precursor solution. The results from the Raman spectroscopic characterization have also demonstrated that the graphitization of carbon nanofibers can be tailored by control of the concentration of catalyst precursor solution. When the information from these characterization are combined with that of the associated morphologies of the carbon nanofibers, it is possible to synthesize perfect carbon nanofibers.


Author(s):  
A. A. Vladimirova ◽  
A. A. Kamnev ◽  
A. V. Tugarova

In the biomass of A. thiophilum BV-S grown in the presence of 7 mM Na2SO4, Raman spectroscopy showed a peak at 348 cm–1 (Se–S bond) in addition to a peak at 250 cm–1 (amorphous modification of Se).


2016 ◽  
Vol 88 (15) ◽  
pp. 7683-7688 ◽  
Author(s):  
Inês P. Santos ◽  
Peter J. Caspers ◽  
Tom C. Bakker Schut ◽  
Remco van Doorn ◽  
Vincent Noordhoek Hegt ◽  
...  

The Analyst ◽  
2014 ◽  
Vol 139 (21) ◽  
pp. 5379-5386 ◽  
Author(s):  
Shiyamala Duraipandian ◽  
Jianhua Mo ◽  
Wei Zheng ◽  
Zhiwei Huang

NIR Raman spectroscopic characterization of cervical precarcinogenic transformation.


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