In Situ Neutron Diffraction Study of Internal Stresses in 60% Mn-40% Cu Alloy Introduced by Ageing

2008 ◽  
Vol 137 ◽  
pp. 163-168
Author(s):  
S.G. Sheverev ◽  
G.V. Markova ◽  
V.V. Sumin
Keyword(s):  
Solid Solution ◽  
Neutron Diffraction ◽  
Diffraction Method ◽  
Neutron Diffraction Study ◽  
Internal Stresses ◽  
Ordered Structure ◽  
Cu Alloy ◽  
Decomposition Of Solid Solution ◽  
Neutron Diffraction Method

Spinodal decomposition of solid solution in the 60 at.% Mn - 40 at.% Cu alloy was observed at the temperatures of decomposition (380 – 420 °C) using the neutron diffraction method in situ. The contribution of residual stresses of third type introduced by further cooling of alloy and, correspondingly, martensitic tranformation is estimated. The relatively small value of stresses of third type introduced by martensitic transformation is revealed. Appearance of magnetic superstructural reflexes typical for antiferromagnetic ordered structure is noted.

Neutron diffraction study of the crystal structure of TlInSe2 at high pressure

2019 ◽  
Vol 33 (15) ◽  
pp. 1950149 ◽  
Author(s):  
N. T. Mamedov ◽  
S. H. Jabarov ◽  
D. P. Kozlenko ◽  
N. A. Ismayilova ◽  
M. Yu. Seyidov ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Neutron Diffraction ◽  
Tetragonal Phase ◽  
Unit Cell Volume ◽  
Diffraction Method ◽  
Lattice Parameter ◽  
Neutron Diffraction Study ◽  
Pressure Derivative ◽  
Neutron Diffraction Method

We have investigated the crystal structure of strongly anisotropic semiconductor TlInSe2 by neutron diffraction method under high pressure upto P = 3.3 GPa. It was shown that the tetragonal phase of TlInSe2 crystal (the space group I4/mcm) is stable in the whole investigated range of pressure. The lattice parameters dependence of the pressure and the unit cell volume are obtained, the linear coefficients of compressibility and the bulk moduli are calculated. At the low pressure, obtained value of compressibility for the lattice parameter a is k[Formula: see text] = 14.23 × 10[Formula: see text] GPa[Formula: see text] and for c is k[Formula: see text] = 5.93 × 10[Formula: see text] GPa[Formula: see text]. Obtained values for bulk modulus B0 and its pressure derivative B[Formula: see text] in tetragonal phase are 30(7) GPa and 4(1), respectively.

Determination of Internal Stresses During Pearlite Transformation of 0.8c–1.5Mn Steel Through In-Situ Neutron Diffraction

2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Internal Stresses

Residual Stress Evaluation of Ni Based Weld Metal Using Neutron Diffraction Method

2006 ◽  
Vol 524-525 ◽  
pp. 697-702 ◽  
Author(s):  
Shinobu Okido ◽  
Hiroshi Suzuki ◽  
K. Saito
Keyword(s):  
Residual Stress ◽  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Neutron Diffraction ◽  
Weld Metal ◽  
Diffraction Method ◽  
Fem Analysis ◽  
Butt Weld ◽  
Stress Evaluation ◽  
Neutron Diffraction Method

Residual stress generated in Type-316 austenitic stainless steel butt-weld jointed by Inconel-182 was measured using a neutron diffraction method and compared with values calculated using FEM analysis. The measured values of Type-316 austenitic stainless steel as base material agreed well with the calculated ones. The diffraction had high intensity and a sharp profile in the base metal. However, it was difficult to measure the residual stress at the weld metal due to very weak diffraction intensities. This phenomenon was caused by the texture in the weld material generated during the weld procedure. As a result, this texture induced an inaccurate evaluation of the residual stress. Procedures for residual stress evaluation to solve this textured material problem are discussed in this paper. As a method for stress evaluation, the measured strains obtained from a different diffraction plane with strong intensity were modified with the ratio of the individual elastic constant. The values of residual stress obtained using this method were almost the same as those of the standard method using Hooke’s law. Also, these residual stress values agreed roughly with those from the FEM analysis. This evaluation method is effective for measured samples with a strong texture like Ni-based weld metal.

Local Structure of the Amorphous Ni25Zr75-Alloy by Using the Isotope-Substitution Neutron Diffraction Method

1991 ◽  
Vol 46 (11) ◽  
pp. 951-954
Author(s):  
W.-M. Kuschke ◽  
P. Lamparter ◽  
S. Steeb
Keyword(s):  
Neutron Diffraction ◽  
Local Structure ◽  
Short Range ◽  
Short Range Order ◽  
Diffraction Method ◽  
Isotopic Substitution ◽  
Isotope Substitution ◽  
Coordination Numbers ◽  
Structure Factors ◽  
Neutron Diffraction Method

AbstractUsing neutron diffraction as well as the method of isotopic substitution the partial Bhatia-Thornton as well as the partial Faber-Ziman structure factors of amorphous Ni25Zr75 were determined. A compound forming tendency was found. The atomic distances, partial coordination numbers, and the chemical short range order parameter are evaluated.

In situ neutron diffraction study of fatigue behavior of CrFeCoNiMo0.2 high entropy alloy

2021 ◽  
Vol 139 ◽  
pp. 107371
Author(s):  
Haiyan He ◽  
Bing Wang ◽  
Dong Ma ◽  
Alexandru D. Stoica ◽  
Zhenduo Wu ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Diffraction Study ◽  
Fatigue Behavior ◽  
Neutron Diffraction Study ◽  
High Entropy Alloy ◽  
High Entropy ◽  
In Situ Neutron Diffraction

A neutron diffraction cell for studying lithium-insertion processes in electrode materials

1998 ◽  
Vol 31 (5) ◽  
pp. 823-825 ◽  
Author(s):  
Ö. Bergstöm ◽  
A. M. Andersson ◽  
K. Edström ◽  
T. Gustafsson
Keyword(s):  
Neutron Diffraction ◽  
Electrode Materials ◽  
Negative Electrode ◽  
Current Collector ◽  
Neutron Diffraction Study ◽  
Lithium Insertion ◽  
Lithium Electrode ◽  
Extraction Processes ◽  
Li Ion

An electrochemical cell has been constructed forin situneutron diffraction studies of lithium-insertion/extraction processes in electrode materials for Li-ion batteries. Its key components are a Pyrex tube, gold plated on its inside, which functions as a current collector, and a central lithium rod, which serves as the negative electrode. The device is demonstrated here for a neutron diffraction study of lithium extraction from LiMn2O4: a mechanical Celgard©separator soaked in the electrolyte surrounds the lithium electrode. The LiMn2O4powder, mixed with electrolyte, occupies the space between separator and current collector.

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