scholarly journals Degree of conversion of two dentin bonding agents with and without a desensitizing agent using fourier transform infrared spectroscopy: An in vitro study

2011 ◽  
Vol 14 (3) ◽  
pp. 302 ◽  
Author(s):  
Vidhya Sampath ◽  
Mahalaxmi Sekar ◽  
Poornima Jose ◽  
Srinivasulu Sakhamuri ◽  
Kavitha Sanjeev
2018 ◽  
Vol 777 ◽  
pp. 577-581
Author(s):  
Wassana Wichai ◽  
Kanin Nimcharoensuk ◽  
Niwat Anuwongnukroh ◽  
Surachai Dechkunakorn ◽  
Pitchaya Roongrujimek

Introduction: The aim of this in-vitro study was to analyze the polymerization ability of 3 light-cured orthodontic adhesives by determining the degree of conversion (DC). Materials and Methods: Fourier transform infrared spectroscopy (FTIR) was used to evaluate the DC after polymerization immediately, 1 day, 7 days, and 30 days. The adhesives investigated were Transbond XT (3M Unitek, USA), Grengloo (Ormco Corp., USA), and Green Glue (Hangzhou Biomaterials, China). Twelve stainless steel brackets (n=4) were used and the adhesives were cured with Bluephase G2 (Ivoclar Vivadent, Liechtenstein). The data were analyzed by Kruskal-Wallis test for comparing materials and Friedman test for comparing the time periods. Results: The DC values were significantly different among the materials and among the time periods. The highest DC in each period was obtained for Grengloo and the lowest DC was observed for Transbond XT. Thus, there were significant differences between the DC values of Grengloo and Transbond XT in each period. Among the time periods, DC% at T1 (Immediately) and T3 of the material were significantly different. The DC values of all adhesives increased extremely from immediately following curing to 1 day and then slightly increased from 1 day to 7 days. Conclusions: Grengloo showed the highest levels of DC at all tested periods. The percentage values of DC largely increased from immediately following curing to 1 day. This concluded that monomers in orthodontic adhesives kept converting even after completion of photoactivation.


2020 ◽  
Vol 19 ◽  
pp. e200656
Author(s):  
Virgínia Angélica Silva ◽  
Sávio Morato de Lacerda Gontijo ◽  
Alexandre Gatti ◽  
Luiz Thadeu de Abreu Poletto ◽  
Hugo Henriques Alvim

Composites have been proven to have a cytotoxiceffect on a variety of tissues and cells. Aim: The aim of thisstudy was to analyse the degree of conversion of resinsand its correlation with the cell viability in primary gingivalfibroblasts. Methods: Resin-based silorane (Filtek P90)and conventional methacrylate resins (Filtek Z100, FiltekZ250 and Filtek Z350XT) were used to evaluate cell viabilityand the degree of conversion. The resins were light-cured bya LED for 20 and 40 seconds. The degree of conversion wasanalysed by Fourier transform infrared spectroscopy. Cellularmetabolism was evaluated after 24 hours by the MTT assay(n = 6) using the storage solution of composite resin foreither 24 hours or 12 days. Variance analysis (ANOVA) witha Bonferroni correction (p < 0.05) was performed to comparethe groups. Results: The composite Filtek P90 showed ahigher degree of conversion when polymerised for 40 or20 seconds, while the composites Filtek Z100, Filtek Z250 andFiltek Z350XT showed similar degree of conversion. Only theFiltek Z100 resin was cytotoxic. Conclusion: We found nostatistically significant correlation between cell viability andthe degree of conversion.


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