Possibilities of biocompatible material production using conform SPD technology

2017 ◽  
Vol 1 (88) ◽  
pp. 5-11 ◽  
Author(s):  
J. Palán ◽  
L. Maleček ◽  
J. Hodek ◽  
M. Zemko ◽  
J. Dzugan

Purpose: At present, materials research in the area of SPD (severe plastic deformation) processes is very intensive. Materials processed by these techniques show better mechanical properties and have finer grain when compared to the input feedstock. The refined microstructure may be ultrafine-grained or nanostructured, where the grain size becomes less than 100 nm. One of the materials used for such processes is CP (commercially pure) titanium of various grades, which is widely used for manufacturing dental implants. The article deals with one of the technologies available for the production of ultrafine-grained titanium: Conform technology. CP titanium processed by CONFORM technology exhibits improved mechanical properties and very favourable biocompatibility, due to its fine-grained structure. The article presents the current experience in the production of ultrafine CP titanium using this technology. The main objective of this article is describing the behaviour of CP titanium during forming in the Conform device and its subsequent use in dental implantology. Design/methodology/approach: In the present study, commercially pure Grade 2 titanium was processed using the CONFORM machine. The numerical simulation of the process was done using FEM method with DEFORMTM software. The evaluation was performed by simple tensile testing and transmission electron microscopy. The first conclusions were derived from the determined mechanical properties and based on analogies in available publications on a similar topic. Findings: This study confirmed that the SPD process improves mechanical properties and does not impair the ductility of the material. The CONFORM process enables the continuous production of ultrafine-grained or nanostructured materials. Research limitations/implications: At the present work, the results show the possible way of continuous production of ultrafine-grained or nanostructured materials. Nevertheless, the further optimization is needed in order to improve the final quality of wires and stabilize the process. As these factors will be solved, the technology will be ready for the industry. Practical implications: The article gives the practical information about the continuous production of ultrafine-grained pure titanium Grade 2 and the possibility of use this material for dental implants. Originality/value: The present paper gives information about the influence of the CONFORM technology on final mechanical and structural properties with the emphasis on technological aspects

2010 ◽  
Vol 667-669 ◽  
pp. 1165-1170 ◽  
Author(s):  
Alexander V. Polyakov ◽  
Dmitriy Gunderov ◽  
Georgy I. Raab

This work reports on the results of investigation of microstructure change of commercially pure titanium Grade 4 with the increase of the number of ECAP-Conform passes. There has been investigated influence of continuous equal-channel angular pressing by the scheme “Conform” (ECAP-C) on the structure and properties of commercially pure titanium Grade 4. It has been demonstrated that as a result of first two ECAP-C cycles titanium structure is strongly fragmented and deformation bands are formed. With the further increase of ECAP-C passes to 6 the band structure is transformed into ultrafine-grained (UFG) structure with the grain size of about 250 nm. The strength of titanium regularly grows with the increase of the number of ECAP-C passes, while ductility, which settles after first cycle on the level of 12%, is almost not changed with the further strain degree increase. As a result of the subsequent drawing of titanium after ECAP-C its strength additionally increases to 1300 MPa, with retention of ductility about 11%.


Author(s):  
L. R. Rezyapova ◽  
◽  
R. R. Valiev ◽  
E. I. Usmanov ◽  
R. Z. Valiev ◽  
...  

It is known that titanium and its alloys are one of the promising materials in the industry, especially in medicine, due to their excellent biocompatibility and corrosion resistance. The latest modern equipment and instruments used in traumatology, orthopedics, dentistry, etc. demand increasingly higher mechanical properties for materials. In comparison with commercially pure titanium, alloys do not have such high corrosion-resistant properties and biocompatibility. In this regard, improving the mechanical characteristics of a pure material is an urgent issue. The authors studied the effect of annealing on the structure and properties of commercially pure grade 4 titanium in the coarse-grained and ultrafine-grained states. The ultrafine-grained state was obtained using high-pressure torsion (HPT) under the pressure of 6 GPa at N=10 revolutions at room temperature. In the microstructure investigated using transmission electron microscopy, the authors could detect particles of precipitated phases after annealing, which had different morphologies. Deformation leads to an increase in the precipitated particles after annealing. The authors carried out an X-ray phase analysis, which showed the approximation of the lattice parameters of the α-phase after deformation and annealing at 700 °C to the values of the parameters of pure titanium. Thus, aging processes occur in the material, accompanied by the decomposition of the supersaturated solid solution and the release of particles of the second phase. The paper shows the results of titanium microhardness measurements in different states. The combined treatment, consisting of HPT at N=5 revolutions, annealing at 700 °C, and additional HPT deformation at N=5 revolutions, allowed obtaining the record strength for commercially pure grade 4 titanium.


Alloy Digest ◽  
2020 ◽  
Vol 69 (6) ◽  

Abstract UPM CP Titanium Grade 3 (UNS R50550) is an unalloyed commercially pure titanium that exhibits moderate strength (higher strength than that of Titanium Grade 2), along with excellent formability and corrosion resistance. It offers the highest ASME allowable design stress of any commercially pure grade of titanium, and can be used in continuous service up to 425 °C (800 °F) and in intermittent service up to 540 °C (1000 °F). This datasheet provides information on composition, physical properties, and elasticity. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Ti-167. Producer or source: United Performance Metals.


2015 ◽  
Vol 60 (3) ◽  
pp. 1895-1900 ◽  
Author(s):  
K. Dyja ◽  
W. Więckowski

Abstract An important factor in the possibility of obtaining correct drawn parts with the desired functional properties is the friction between the stamped sheet and the tool. The article discusses the impact of technological lubricants developed according to our own formulas, based on vegetable oils, on the stamping process taking into account the strain distributions in the drawn parts. Biodegradable lubricants based on rapeseed oil with an addition of stearic acid or boric acid were used. The results of the friction coefficient in a strip drawing test and the numerical analysis results of the stamping process of a spherical cap from sheet metal: aluminium 2024, commercially pure titanium Grade 2, steel 5604 in dry friction and lubrication conditions, are presented. Strain distributions and changes in the drawn part wall thickness were analysed.


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