solvent effect
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2022 ◽  
Author(s):  
Zaid Abdul Khalik ◽  
Zeyad Saleh ◽  
Mazin Ali

Abstract In this research paper, a method built on UV/VIS spectrofluorophotometer and spectrophotometer by finding the fluorescence of glycyrrhizic acid in licorice root. Glycyrrhizic acid is an imperative active component present in licorice (Glycyrrhiza uralensis Fisch). Solvent effect had been studied in different solvents like deionized water and methanol. The differences between them were explored by the glycyrrhizic acid absorption and emission spectra. Under work conditions, i.e. 100% methanol solvent, a liquid ratio concentration 10−2 to 10−5 g /mL and second solvent with same conditions 100% deionized water in the same concentrations ,was done. The effect of the solvent was significant by change the value for λmax. The result was validated for parameters confines for Ex (λ Excitation) in different solvents. The results of absorption spectra obey Beer-Lambert's law. Because of the same property of these solvents (protic), the absence of a significant difference in the absorption spectra are shown. From florescence spectra, the spectrum at concentration 10−4 is the best for both solvents..


2022 ◽  
Author(s):  
Chunfang Guo ◽  
Zhaolong Liu ◽  
Xiangye Li ◽  
Xuliang Han ◽  
Yueyun Li ◽  
...  

A mild and efficient method for direct C−H monofluoroalkylation of heteroarenes with easily accessible and inexpensive α-fluorocarboxylic acids has been developed. This silver-catalyzed reaction affords mono- and bis-monofluoroalkylated heteroarenes in...


Author(s):  
Qiang Gao ◽  
Peizhi Zhu ◽  
Hongkun Zhao ◽  
Ali Farajtabar ◽  
Abolghasem Jouyban ◽  
...  
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