precipitation synthesis
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2022 ◽  
Author(s):  
Mingmei Wu ◽  
Bojana Milićević ◽  
Yingyuan Chen ◽  
Junhao Li ◽  
Miroslav D Dramićanin ◽  
...  

We report an organic solvent-assisted (OSA) co-precipitation strategy for the production of Mn4+-activated K2TiF6 phosphor. The phosphor particle size was controlled through the selection of organic solvents with an alcohol...


Author(s):  
Sangki Hong ◽  
Ye Cheng ◽  
Shruti Hariyani ◽  
Jingzhe Li ◽  
Rachel M. Doughty ◽  
...  

Author(s):  
Feng Jiang ◽  
Li Yin ◽  
Guo Feng ◽  
Chao Wu ◽  
Jingang Tan ◽  
...  

Photochem ◽  
2021 ◽  
Vol 1 (3) ◽  
pp. 345-357
Author(s):  
Gopal Panthi ◽  
Mira Park

For the first time, heterostructures of electrospun carbon nanofibers decorated with Ag3PO4 nanoparticles (Ag3PO4/CNFs) were successfully fabricated by the combination of simple and versatile electrospinning technique followed by carbonization and incorporation of Ag3PO4 nanoparticles via colloidal and precipitation synthesis approaches. The as-fabricated heterostructures were characterized by FESEM with EDS, XRD, TEM with HRTEM, FTIR and UV-vis diffuse reflectance spectroscopy. Experimental results revealed that the heterostructure obtained by colloidal synthesis approach (Ag3PO4/CNFs-1) was decorated with small-sized (~20 nm) and uniformly distributed Ag3PO4 nanoparticles on the surface of CNFs without any evident agglomeration, while in the heterostructure obtained by the precipitation synthesis approach (Ag3PO4/CNFs-2), CNFs were decorated with agglomerated and bigger-sized Ag3PO4 nanoparticles. The visible-light-driven photocatalytic investigation signified that the Ag3PO4/CNFs-1 heterostructure can exhibit higher performance towards the photodegradation of MB dye solution compared to the Ag3PO4/CNFs-2 heterostructure, which could be attributed to the synergistic effect between the uniformity and small size of Ag3PO4 nanoparticles and CNFs that can serve as a conductivity network to prevent the recombination of charge carriers. Moreover, the mechanism of the photocatalytic activity as-prepared heterostructure is proposed.


2021 ◽  
Vol 133 ◽  
pp. 105970
Author(s):  
T. Thilagavathi ◽  
D. Venugopal ◽  
D. Thangaraju ◽  
R. Marnadu ◽  
Baskaran Palanivel ◽  
...  

2021 ◽  
Vol 2021 ◽  
pp. 1-10
Author(s):  
Bulcha Bekele ◽  
Anatol Degefa ◽  
Fikadu Tesgera ◽  
Leta Tesfaye Jule ◽  
R. Shanmugam ◽  
...  

Comparison of green and chemical precipitation method syntheses of zinc oxide nanoparticles (ZnO NPs) was performed, and antimicrobial properties were investigated. Avocado, mango, and papaya fruit extracts were carried out for the green synthesising methods, while the chemical precipitation method was chosen from chemical synthesis methods. Zinc nitrate was used as a salt precursor, whereas leaf extract was served as a reducing agent for green synthesising methods. In addition, sodium hydroxide, polyvinyl alcohol, and potassium hydroxide were used as reducing agents in the case of chemical precipitation synthesis methods. ZnO NPs were characterised by characterizing techniques such as Fourier transform infrared (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). The antimicrobial activities of prepared nanoparticles were evaluated on Bacillus subtilis (B. subtilis), Staphylococcus aureus (S. aureus), and Salmonella typhimurium (S. typhimurium). The particle sizes of the prepared samples which were evaluated by the Scherrer equation were in the range of 11-21 nm for green synthesis, while 30-40 nm for chemical precipitation synthesis methods. Small agglomerations were observed from SEM results of prepared ZnO NPs from both methods. Prepared ZnO NPs were showed strong antimicrobial properties. From the result, the inhibition zone was in the range of 15-24 mm for the green route and 7–15 mm for chemical precipitation methods, where the standard drugs have 25 mm of the zone of inhibition. A green synthesised method of preparing ZnO NPs gives promising antimicrobial properties compared to chemical synthesis and is also eco-friendly and safe compared to the chemical synthesis.


2021 ◽  
Vol 129 (9) ◽  
pp. 579-583
Author(s):  
Hideyuki HIRAZAWA ◽  
Reika MATSUMOTO ◽  
Masanori SAKAMOTO ◽  
Uyanga ENKHNARAN ◽  
Deleg SANGAA ◽  
...  

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