ChemInform Abstract: Hypervalent Iodine Mediated Solid State Transformations. An Efficient Synthetic Route to Diacylhydrazines (II).

ChemInform ◽  
2010 ◽  
Vol 32 (24) ◽  
pp. no-no
Author(s):  
K. Mogilaiah ◽  
R. Babu Rao
Keyword(s):  
Solid State ◽  
Hypervalent Iodine ◽  
Synthetic Route

Unprecedented Hexa- and Undecanuclear Frameworks of Two New Tin(IV) Oxo Clusters Resulting from Partial Debenzylation Reactions

2010 ◽  
Vol 65 (11) ◽  
pp. 1293-s1308 ◽  
Author(s):  
Laurent Plasseraud ◽  
Hélène Cattey ◽  
Philippe Richard
Keyword(s):  
Solid State ◽  
1H Nmr Spectroscopy ◽  
Trifluoromethanesulfonic Acid ◽  
Synthetic Route ◽  
State Structure ◽  
X Ray Diffraction ◽  
Neutral Cluster ◽  
Broad Resonance ◽  
X Ray ◽  
The Core

A new and facile synthetic route to the known neutral cluster ((PhCH2)2SnO)6[((PhCH2)2SnOH)2- (CO3)]2 (2) as well as its reactivity toward trifluoromethanesulfonic acid (HO3SCF3, TfOH) are reported. The solid-state structure of the new solvate 2·6C7H8 has been determined by single-crystal X-ray diffraction. The core of 2 can be described as a pair of coplanar pentanuclear [(PhCH2)2SnO]5 ladders bridged at their ends by two carbonate groups. Successive additions of TfOH to a suspension of 2 in CD3CN were monitored by 119Sn{1H} NMR spectroscopy showing the transformation of the fingerprint of 2 (δ = −244, −246, −306 ppm), via new upfield signals, to a final broad resonance located at δ = −474 ppm. Thereafter, two unprecedented ionic monobenzyltin(IV) oxo clusters, 3 and 4, resulting from a debenzylation reaction and exhibiting unusual hexa- and undecanuclear frameworks, respectively, have been isolated as single crystals.

A novel synthetic route to obtain RUB-15 phase by pseudo solid-state conversion

2016 ◽  
Vol 228 ◽  
pp. 116-122 ◽  
Author(s):  
Fethi Kooli ◽  
Yan Liu ◽  
Kais Hbaieb ◽  
Rawan Al-Faze
Keyword(s):  
Solid State ◽  
Synthetic Route

Titanium(III) alkoxides. A new synthetic route and solid state properties (CP/MAS 13C NMR, X-ray and IR)

1986 ◽  
Vol 120 (2) ◽  
pp. 197-203 ◽  
Author(s):  
Enrico Albizzati ◽  
Luigi Abis ◽  
Enrico Pettenati ◽  
Enzo Gianneti
Keyword(s):  
Solid State ◽  
13C Nmr ◽  
Synthetic Route ◽  
X Ray ◽  
Cp Mas 13C Nmr

Synthetic Route to Metal Nitrides: High-Pressure Solid-State Metathesis Reaction

2013 ◽  
Vol 52 (23) ◽  
pp. 13356-13362 ◽  
Author(s):  
Li Lei ◽  
Wenwen Yin ◽  
Xiaodong Jiang ◽  
Sen Lin ◽  
Duanwei He
Keyword(s):  
High Pressure ◽  
Solid State ◽  
Metal Nitrides ◽  
Synthetic Route ◽  
Metathesis Reaction

scholarly journals A bio-facilitated synthetic route for nano-structured complex electrode materials

2016 ◽  
Vol 18 (9) ◽  
pp. 2619-2624 ◽  
Author(s):  
Maryam Moradi ◽  
Jae Chul Kim ◽  
Jifa Qi ◽  
Kang Xu ◽  
Xin Li ◽  
...  
Keyword(s):  
Solid State ◽  
Energy Efficient ◽  
Electrode Materials ◽  
Inorganic Materials ◽  
State Solution ◽  
Solid State Reactions ◽  
Synthetic Route ◽  
Efficient Synthesis ◽  
Wide Range

Bio-facilitated solid state solution: we investigate an energy-efficient synthesis that merges the bio-templated technique and solid-state reactions to produce a wide range of nano-structured complex inorganic materials.

Thiol–ene click chemistry: a modular approach to solid-state triplet–triplet annihilation upconversion

2018 ◽  
Vol 6 (15) ◽  
pp. 3876-3881 ◽  
Author(s):  
Abagail K. Williams ◽  
Brad J. Davis ◽  
Erin R. Crater ◽  
Joseph R. Lott ◽  
Yoan C. Simon ◽  
...  
Keyword(s):  
Solid State ◽  
Click Chemistry ◽  
Modular Approach ◽  
Synthetic Route ◽  
On Demand ◽  
Host Materials ◽  
Triplet Triplet Annihilation

Thiol–ene click chemistry can be used as a facile cure-on-demand synthetic route to access robust host materials for solid-state upconversion.

Electrochemically activated solid synthesis: an alternative solid-state synthetic method

2018 ◽  
Vol 47 (41) ◽  
pp. 14604-14611 ◽  
Author(s):  
Junnan Liu ◽  
Henrik Lyder Andersen ◽  
Othman K. Al Bahri ◽  
Saroj Bhattacharyya ◽  
Aditya Rawal ◽  
...  
Keyword(s):  
Solid State ◽  
Synthetic Method ◽  
Thermal Treatments ◽  
Synthetic Route ◽  
Electrochemical Discharge ◽  
Solid Synthesis

Electrochemical discharge followed by thermal treatments leads to the generation of unconventional phases upon heating, an alternative synthetic route.

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