scholarly journals Microwave-Assisted Facile Synthesis and Crystal Structure of cis-9,10,11,15-Tetrahydro-9,10[3′,4′]-furanoanthracene-12,14-dione.

ChemInform ◽  
2006 ◽  
Vol 37 (34) ◽  
Author(s):  
Weerachai Phutdhawong ◽  
Duang Buddhasukh ◽  
Stephen G. Pyne ◽  
Apinpus Rujiwatra ◽  
Chaveng Pakawatchai
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted

scholarly journals Microwave‐Assisted Facile Synthesis and Crystal Structure of cis‐9,10,11,15‐Tetrahydro‐9,10[3′,4′]‐furanoanthracene‐12,14‐dione

2006 ◽  
Vol 36 (7) ◽  
pp. 881-883 ◽  
Author(s):  
Weerachai Phutdhawong ◽  
Duang Buddhasukh ◽  
Stephen G. Pyne ◽  
Apinpus Rujiwatra ◽  
Chaveng Pakawatchai
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted

Facile Synthesis and Crystal Structure of [(PhSO2 N)2 WVI Cl2 (CH3CN)2] - the Oxidative Imination of W(CO)6 by N,N-Dichlorophenylsulphonamide

1985 ◽  
Vol 40 (6) ◽  
pp. 736-739 ◽  
Author(s):  
Herbert W. Roesky ◽  
Jörg Sundermeyer, ◽  
Jürgen Schimkowiak ◽  
Peter G. Jones ◽  
Mathias Noltemeyer ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Good Yield ◽  
Polymeric Complex ◽  
Facile Synthesis ◽  
Triclinic Space Group ◽  
Synthesis And Crystal Structure ◽  
Tungsten Hexacarbonyl ◽  
Space Group

AbstractThe reaction of N,N-dichlorophenylsulphonamide with tungsten hexacarbonyl in refluxing CCl4 leads in good yield to the yellow polymeric complex [(PhSO2N)2WCl2]x, which may be converted to the octahedral nitrene complex [(PhSO2N)2WCl2(CH3CN)2] by recrystallisation from aceto­nitrile. Crystals of the acetonitrile complex are triclinic, space group P 1̅, a = 820.7(2), b = 1128.8(3), c = 1286.9(3) pm, α = 89.25(3), β = 89.54(3). γ = 72.67(2)°, Z = 2, R = 0.027 for 2527 unique observed reflections.

Microwave-Assisted Synthesis and Crystal Structure of Novel 2-Dichloromethyl-1,3-dioxolanes

Heterocycles ◽  
2013 ◽  
Vol 87 (2) ◽  
pp. 407 ◽  
Author(s):  
Ying Fu ◽  
Fei Ye ◽  
Ying Li ◽  
Shuang Gao ◽  
Li-Xia Zhao
Keyword(s):  
Crystal Structure ◽  
Microwave Assisted Synthesis ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted

scholarly journals Microwave-Assisted Synthesis and Crystal Structure of Oxo(diperoxo)(4,4'-di-tert-butyl-2,2'-bipyridine)-molybdenum(VI)

Molecules ◽  
2009 ◽  
Vol 14 (9) ◽  
pp. 3610-3620 ◽  
Author(s):  
Tatiana Amarante ◽  
Filipe Almeida Paz ◽  
Sandra Gago ◽  
Isabel Gonçalves ◽  
Martyn Pillinger ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Microwave Assisted Synthesis ◽  
Synthesis And Crystal Structure ◽  
Tert Butyl ◽  
Microwave Assisted

scholarly journals Green synthesis and crystal structure of 3-(benzothiazol-2-yl)thiophene

2017 ◽  
Vol 73 (11) ◽  
pp. 1647-1651 ◽  
Author(s):  
Linh Nguyen Ngoc ◽  
Trung Vu Quoc ◽  
Hoan Duong Quoc ◽  
Manh Vu Quoc ◽  
Luong Truong Minh ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Crystal Packing ◽  
High Yield ◽  
Dihedral Angles ◽  
Microwave Assisted Synthesis ◽  
Aromatic Rings ◽  
Synthesis And Crystal Structure ◽  
Microwave Assisted ◽  
Compound C ◽  
Whole Molecule Disorder

The title compound, C11H7NS2, was prepared in high yield (87%) using a solvent-free microwave-assisted synthesis. The structure shows whole-molecule disorder with occupancies for two orientations (A and B) of 0.4884 (10) and 0.5116 (10), respectively. The thiophene and benzothiazole rings are almost planar and make dihedral angles of 10.02 (18) and 12.54 (19)° for orientations A and B, respectively. Slipped π–π stacking between the aromatic rings, together with C—H...π, C—H...S and C—H...N interactions, result in a herringbone motif in the crystal packing.

Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane

2008 ◽  
Vol 634 (8) ◽  
pp. 1244-1246 ◽  
Author(s):  
Thomas M. Klapötke ◽  
Burkhard Krumm ◽  
Matthias Scherr ◽  
Gunnar Spieß ◽  
F. Xaver Steemann
Keyword(s):  
Crystal Structure ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure

BODIPY trimer with 1,3,5-triazine core: Facile synthesis and crystal structure

2021 ◽  
pp. A-H
Author(s):  
Chunhua Huang ◽  
Bin Shen ◽  
Kaili Wang ◽  
Xiaofei Sun
Keyword(s):  
Crystal Structure ◽  
Fluorescence Spectroscopy ◽  
Hirshfeld Surface ◽  
Spectroscopic Methods ◽  
X Ray Diffraction ◽  
Facile Synthesis ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Design And Synthesis ◽  
H Nmr

Trimerization reaction of 8-(4[Formula: see text]-cyanophenyl)-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (CN-BODIPY) led to the isolation of a new triazine-based BODIPY trimer 2,4,6-tris(8[Formula: see text]-phenyl-1[Formula: see text],3[Formula: see text],5[Formula: see text],7[Formula: see text]-tetramethyl-4[Formula: see text],4[Formula: see text]-difluoro-4[Formula: see text]-bora-3a[Formula: see text],4a[Formula: see text]-diaza-s-indacene)-1,3,5-triazine (1). This BODIPY trimer 1 have been characterized by a series of spectroscopic methods including MALDI-TOF mass, 1H NMR, electronic absorption, IR and fluorescence spectroscopy. In particular, the single crystals of 1 have be obtained by slow diffusion of methanol into the solution of this compound in CHCl3. The BODIPY trimer structure of 1 with a triazine core has been directly revealed on the basis of single crystal X-ray diffraction analysis with the intermolecular interactions investigated by Hirshfeld surface analysis. This work will be helpful for the design and synthesis of new multiple BODIPY derivatives with various application.

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