ChemInform Abstract: In situ Hydrothermal Synthesis of Tetrazole Coordination Polymers with Interesting Physical Properties

ChemInform ◽  
2008 ◽  
Vol 39 (18) ◽  
Author(s):  
Hong Zhao ◽  
Zhi-Rong Qu ◽  
Heng-Yun Ye ◽  
Ren-Gen Xiong
2013 ◽  
Vol 648 ◽  
pp. 139-142
Author(s):  
Fei Liu ◽  
Ting Li ◽  
Xiao Dan Wang ◽  
Jian Xin Cao

The ultra-light calcium silicate material was reinforced with the method of xonotlite whisker in-situ growth via hydrothermal synthesis. Effects of different hydrothermal temperatures and reaction times on the microstructure and physical properties of the reinforcement were studied in this paper. The results indicated that the hydrothermal temperatures and times posed great impacts on microstructure of the reinforcement. The increase of hydrothermal temperature and time was beneficial to the growth of xonotlite crystal. The effect of buffer and transfer action of the xonotlite whiskers was the key to reinforcing the ultra-light calcium silicate material.


Crystals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 617
Author(s):  
Yaodan Zhang ◽  
Zhijun Li ◽  
Yuanren Xiu ◽  
Chunjiang Li ◽  
Baosen Zhang ◽  
...  

Frazil particles, ice crystals or slushy granules that form in turbulent water, change the freezing properties of ice to create “frazil ice”. To understand the microstructural characteristics of these particles and the physical properties of frazil ice in greater depth, an in situ sampler was designed to collect frazil particles in the Yellow River. The ice crystal microstructural characteristics of the frazil particles (morphology, size, air bubble, and sediment) were observed under a microscope, and their nucleation mechanism was analyzed according to its microstructure. The physical properties of frazil ice (ice crystal microstructure, air bubble, ice density, and sediment content) were also observed. The results showed that these microstructures of frazil particles can be divided into four types: granular, dendritic, needle-like, and serrated. The size of the measured frazil particles ranged from 0.1 to 25 mm. Compared with columnar ice, the crystal microstructure of frazil ice is irregular, with a mean crystal diameter less than 5 mm extending in all directions. The crystal grain size and ice density of frazil ice are smaller than columnar ice, but the bubble and sediment content are larger.


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