Front Cover: Extraction of acetanilide herbicides in naked oat ( Avena nuda L .) by using ionic‐liquid‐based matrix solid‐phase dispersion‐foam flotation solid‐phase extraction

2019 ◽  
Vol 42 (22) ◽  
Author(s):  
Liyuan Zhang ◽  
Zhenchuan Ma ◽  
Changyuan Wang ◽  
Runzhong Yu ◽  
Dongjie Zhang
2015 ◽  
Vol 38 (10) ◽  
pp. 1733-1740 ◽  
Author(s):  
Liyuan Zhang ◽  
Bocheng Cao ◽  
Di Yao ◽  
Runzhong Yu ◽  
Changqing Yu ◽  
...  

Talanta ◽  
2007 ◽  
Vol 74 (1) ◽  
pp. 20-31 ◽  
Author(s):  
M.S. Dopico-García ◽  
P. Valentão ◽  
A. Jagodziñska ◽  
J. Klepczyñska ◽  
L. Guerra ◽  
...  

2015 ◽  
Vol 13 (1) ◽  
Author(s):  
Bozena Lozowicka ◽  
Ewa Rutkowska ◽  
Izabela Hrynko

AbstractLSE (liquid-solid extraction), MSPD (matrix solid phase dispersion) and QuEChERS (quick, easy, cheap, effective, rugged and safe) extractions followed by GC-μECD/NPD to determine 223 pesticide residues in tobacco simultaneously were developed and compared. The identities of ten model pesticides were confirmed by GC-MS/MS. The type and amount of dispersant (Florisil, silica gel and alumina), sample mass, cleanup adsorbent, and the eluent (hexane, acetone and acetonitrile) were optimized. Linearity, recovery, LOQ, LOD, and matrix effect were compared. Most recoveries were 71−120% (RSD < 18%). LOD and LOQ were much lower than the CORESTA GRLs. The best method was QuEChERS: acetonitrile extraction and dispersive solid-phase extraction using primary-secondary amine and graphitized carbon.


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