Energy Dispersive Diffraction in a Diamond Anvil High Pressure Cell using Synchrotron and Conventional X-Radiation

1984 ◽  
pp. 331-337 ◽  
Author(s):  
David R. Black ◽  
Carmen S. Menoni ◽  
Ian L. Spain
1983 ◽  
Vol 27 ◽  
pp. 331-337
Author(s):  
David R. Black ◽  
Carmen S. Menoni ◽  
Ian L. Spain

A wide range of structural studies have been carried out in high pressure diamond anvil cells using x-rays. The most common experimental geometry is shown in Fig. 1a. The incident x-ray beam passes axially through the first diamond and enters the sample, typically 100-300 μm in diameter and 20-100 μm thick; the diffracted x-rays exit via the second diamond. Energy-dispersive detection techniques (EDXRD) have been used. However the intensity of diffracted radiation from the sample is weak, so that typical exposure times with a conventional, fixed anode, x-ray source are typically one to several days.Accordingly, higher intensity radiation from synchrotron sources has been used for these experiments.


2016 ◽  
Vol 13 (8/9) ◽  
pp. 604 ◽  
Author(s):  
V.D. Blank ◽  
B.A. Kulnitskiy ◽  
I.A. Perezhogin ◽  
E.V. Tyukalova ◽  
V.N. Denisov ◽  
...  

1986 ◽  
Vol 57 (11) ◽  
pp. 2795-2797 ◽  
Author(s):  
Dinesh Patel ◽  
Todd E. Crumbaker ◽  
James R. Sites ◽  
Ian L. Spain

Nature ◽  
1980 ◽  
Vol 288 (5787) ◽  
pp. 155-157 ◽  
Author(s):  
A. Lacam ◽  
M. Madon ◽  
J. P. Poirier

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