Effect of Powder Particle Size on the Grain Size of the Sintered Material

1968 ◽  
pp. 284-294 ◽  
Author(s):  
H. H. Hausner ◽  
R. King
Author(s):  
Olugbenga Ogunbiyi ◽  
Tamba Jamiru ◽  
Rotimi Sadiku ◽  
Oluwagbenga Adesina ◽  
Olanrewaju Seun Adesina ◽  
...  

This study aims to investigate the effects of powder particle size on the densification and microhardness properties of spark plasma sintered superalloy. Three particles size ranges of nickel were used in this study, namely, (3-44, 45-106 and 106-150 μm), and this is the matrix in the IN738LC superalloy composition (powder), used in the study. The effects of the particle size were examined at a specific applied temperature and pressure. The transitioning stages during the sintering process of the green powders to the formation of the sintered alloy were analyzed and given as the particle rearrangement stage, the localized deformation stage and the neck formation/grain growth stage. There was the formation of γ, γ' and a solid solution within the microstructure of the sintered alloys. The effect of particle size was more pronounced on the grain sizes obtained, while the phases formed is the same for the three alloys. The results indicate that the nickel particle size (>60% of the total composition) has a significant influence on the densification, porosity, grain size and hardness properties of the IN738LC sintered alloy. Finer nickel particle size resulted in a sintered product with smaller grain size (9 µm), reduced percentage porosity (3.9%), increased relative density (96.1%) and increased hardness properties (371 Hv).


2014 ◽  
Vol 936 ◽  
pp. 1694-1700
Author(s):  
Zhi Wei Li ◽  
Kai Yong Jiang ◽  
Fei Wang ◽  
Ji Liang Zhang

This paper mainly introduces the mechanism of microwave heating: electric conduction loss, eddy current loss and arc discharge. The microwave heating behavior of 316 stainless steel powder body which made by gel casting was investigated in the paper. Experiments on different microwave power, powder particle size, and the content of auxiliary heating material showed that the smaller the powder particle size, the larger microwave power and auxiliary heating materials help 316 stainless steel body for sintering.


2014 ◽  
Vol 46 (3) ◽  
pp. 365-375
Author(s):  
N. Labus ◽  
S. Mentus ◽  
Z.Z. Djuric ◽  
M.V. Nikolic

The influence of air and nitrogen atmosphere during heating on TiO2 nano and micro sized powders as well as sintered polycrystalline specimens was analyzed. Sintering of TiO2 nano and micro powders in air atmosphere was monitored in a dilatometer. Non compacted nano and micro powders were analyzed separately in air and nitrogen atmospheres during heating using thermo gravimetric (TG) and differential thermal analysis (DTA). The anatase to rutile phase transition temperature interval is influenced by the powder particle size and atmosphere change. At lower temperatures for nano TiO2 powder a second order phase transition was detected by both thermal techniques. Polycrystalline specimens obtained by sintering from nano powders were reheated in the dilatometer in nitrogen and air atmosphere, and their shrinkage is found to be different. Powder particle size influence, as well as the air and nitrogen atmosphere influence was discussed.


2016 ◽  
Vol 43 (2) ◽  
pp. 0203007
Author(s):  
闫岸如 Yan Anru ◽  
杨恬恬 Yang Tiantian ◽  
王燕灵 Wang Yanling ◽  
马志红 Ma Zhihong ◽  
杜云 Du Yun ◽  
...  

2020 ◽  
Vol 989 ◽  
pp. 816-820
Author(s):  
Roman Sergeevich Khmyrov ◽  
R.R. Ableyeva ◽  
Tatiana Vasilievna Tarasova ◽  
A.V. Gusarov

Mass transfer in the laser-interaction zone at selective laser melting influences the quality of the obtained material. Powder particles displacement during the formation of the single bead is experimentally studied. The so-called denudated zone was visualized by metallography. It was determined that increasing the powder particle size leads to widening the denudated zone. This can signify that the adhesion forces between powder particles prevail over the friction forces.


2020 ◽  
Vol 364 ◽  
pp. 115-122 ◽  
Author(s):  
Annika Linke ◽  
Jörg Hinrichs ◽  
Reinhard Kohlus

2010 ◽  
Vol 434-435 ◽  
pp. 335-339
Author(s):  
Han Wang ◽  
Xiao Hui Wang ◽  
Shao Peng Zhang ◽  
Long Tu Li ◽  
Zhao Hui Huang

In this paper, the effect of gel-calcination on piezoelectric property in (1-x) BiScO3-xPbTiO3 with the composition of x=0.635 is investigated. According to previous work, the heating rate of 200°C/h and holding for 210min having been taken as the basic processing condition. The BSPT powders were obtained from the same sol solution but calcined at different temperatures, and then the powders were used to prepare BSPT ceramics. The result shows that for the bulk ceramics with higher relative density ( higher than 95%), with the increasing calcining temperature of the gel (from 420°C to 500°C), the piezoelectric coefficient d33 of ceramic specimens first increases to maximum of 636pC/N at 450°C, then shows a fluctuation. In this work how the powder activity and the grain size affect (which was leaded by powder particle size) piezoelectric properties of BSPT ceramics are discussed.


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