Application of QbD Elements in the Development and Scale-Up of a Commercial Filtration Process

Author(s):  
Feroz Jameel
Keyword(s):  
Scale Up ◽  
2021 ◽  
Vol 3 (4) ◽  
Author(s):  
Alexandre Gonçalves Andrade ◽  
Maycon Athayde

AbstractThe present study presents the effect of pH reduction in iron ore slurry for an iron ore filtration process. A reduction on moisture content and increase on filters throughput was proposed by the pH modification. The experimental procedure included bench scale tests and industrial scale up of the observed results. Additionally, Langelier’s saturation index was applied to determine the optimum pH range for the filtration operation. The calcium carbonate deposition test was developed and evaluated in the present study. A comprehensive evaluation at different pH ranges was performed leading to identify the calcium carbonate deposition critical point.


Author(s):  
L.E. Murr ◽  
J.S. Dunning ◽  
S. Shankar

Aluminum additions to conventional 18Cr-8Ni austenitic stainless steel compositions impart excellent resistance to high sulfur environments. However, problems are typically encountered with aluminum additions above about 1% due to embrittlement caused by aluminum in solid solution and the precipitation of NiAl. Consequently, little use has been made of aluminum alloy additions to stainless steels for use in sulfur or H2S environments in the chemical industry, energy conversion or generation, and mineral processing, for example.A research program at the Albany Research Center has concentrated on the development of a wrought alloy composition with as low a chromium content as possible, with the idea of developing a low-chromium substitute for 310 stainless steel (25Cr-20Ni) which is often used in high-sulfur environments. On the basis of workability and microstructural studies involving optical metallography on 100g button ingots soaked at 700°C and air-cooled, a low-alloy composition Fe-12Cr-5Ni-4Al (in wt %) was selected for scale up and property evaluation.


Planta Medica ◽  
2012 ◽  
Vol 78 (11) ◽  
Author(s):  
RS Barboza ◽  
BR Rocha ◽  
AC Siani ◽  
LMM Valente ◽  
JL Mazzei
Keyword(s):  

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