Luminescence Dating in Fluvial Settings: Overcoming the Challenge of Partial Bleaching

Author(s):  
Rachel K. Smedley ◽  
Grace K. A. Skirrow
2011 ◽  
Vol 38 (3) ◽  
pp. 249-258 ◽  
Author(s):  
Reza Sohbati ◽  
Andrew Murray ◽  
Mayank Jain ◽  
Jan-Pieter Buylaert ◽  
Kristina Thomsen

Abstract There are many examples of buried rock surfaces whose age is of interest to geologists and archaeologists. Luminescence dating is a potential method which can be applied to dating such surfaces; as part of a research project which aims to develop such an approach, the degree of resetting of OSL signals in grains and slices from five different cobbles/boulders collected from a modern beach is investigated. All the rock surfaces are presumed to have been exposed to daylight for a prolonged period of time (weeks to years). Feldspar was identified as the preferred dosimeter because quartz extracts were insensitive. Dose recovery tests using solar simulator and IR diodes on both K-feldspar grains and solid slices taken from the inner parts of the rocks are discussed. Preheat plateau results using surface grains and slices show that significant thermal transfer in naturally bleached samples can be avoided by keeping preheat temperatures low. Equivalent doses from surface K-feldspar grains were highly scattered and much larger than expected (0.02 Gy to >100 Gy), while solid surface slices gave more reproducible small doses (mean = 0.17±0.02 Gy, n = 32). Neither crushing nor partial bleaching were found to be responsible for the large scattered doses from grains, nor did the inevitable contribution from Na-feldspar to the signal from solid slices explain the improved reproducibility in the slices. By modelling the increase of luminescence signal with distance into the rock surface, attenuation factors were derived for two samples. These indicate that, for instance, bleaching at a depth of 2 mm into these samples occurs at about ∼28% of the rate at the surface. We conclude that it should be possible to derive meaningful burial doses of >1 Gy from such cobbles; younger samples would probably require a correction for incomplete bleaching.


2021 ◽  
Author(s):  
Felix Martin Hofmann ◽  
Alexander Fülling ◽  
Frank Preusser

<p>During the last glaciation maximum, an ice cap and its more than 20 kilometres-long outlet glaciers covered the highest summit of the Black Forest, the Feldberg (1493 m above sea-level), and the surrounding region (Hofmann et al., 2020). This event is tentatively correlated with the global last glacial maximum (at ca. 22-19 ka). However, this hypothesis has never been tested by applying up-to-date geochronological techniques to glacial deposits or landforms. Due to the lack of significant topographic control, the climate probably mainly controlled the mass balance of the ice cap. Dating its last maximum extent may thus have important implications for the reconstruction of atmospheric circulations patterns during the Pleistocene. A last glaciation maximum out of phase with the Alps would strengthen the hypothesis that a meridional atmospheric circulation prevailed over Europe during the last glaciation maximum in the Alps (at ca. 25 ka).</p><p>We aim at filling this gap by re-investigating a well-preserved multi-ridged terminal moraine complex several kilometres north-west of the Feldberg. Since the beginning of the twentieth century, this landform is undisputedly assigned to the last glaciation maximum. As units of sorted sediments occur in two sections on one ridge of the terminal moraine complex, luminescence dating was deemed a suitable technique to infer the age of the landform.</p><p>Luminescence dating was applied to both feldspar and quartz for suitable comparison, as these dosimeters have different drawbacks. Since quartz from crystalline source areas often shows no or only a relatively weak luminescence signal, we anticipated that this also applies to the sampled sediments from the crystalline part of the Black Forest. Optically-stimulated luminescence (OSL) measurements revealed a bright signal in quartz as well as equivalent doses in the order of 200 Gy considerably below the saturation level. We did not observe any obvious signs for partial bleaching, but this possibility has to be confirmed via further OSL measurements, since the sampled sediments were not transported over large distances. Component analysis will also be performed.</p><p>Infrared-stimulated luminescence (IRSL) measurements on feldspar revealed higher preliminary luminescence ages. It is expected that anomalous fading and partial bleaching will be two major future challenges. To overcome the first problem, post-infrared IRSL dating will be applied. As resetting of this signal is more difficult when compared to IRSL and OSL signals, problems associated with incomplete bleaching may arise in future work.</p><p>Our preliminary quartz OSL ages tentatively suggest that the last glaciation maximum in the southern Black Forest preceded the last glaciation maxima in other formerly glaciated uplands in Central Europe and the global last glacial maximum. This result needs to be evaluated by luminescence dating of other ice-marginal landforms correlative with the last glaciation maximum. Other geochronological techniques, such as <sup>10</sup>Be cosmic-ray exposure dating, will also be applied to reveal their age.</p><p> </p><p><strong>Reference</strong></p><p>Hofmann, F. M., Rauscher, F., McCreary, W., Bischoff, J.-P., and Preusser, F.: Revisiting Late Pleistocene glacier dynamics north-west of the Feldberg, southern Black Forest, Germany, E&G Quaternary Science Journal, 69, 61–87, https://doi.org/10.5194/egqsj-69-61-2020, 2020.</p><p> </p><p> </p><p> </p>


Geochronology ◽  
2020 ◽  
Vol 2 (2) ◽  
pp. 305-323
Author(s):  
Daniela Mueller ◽  
Frank Preusser ◽  
Marius W. Buechi ◽  
Lukas Gegg ◽  
Gaudenz Deplazes

Abstract. Luminescence dating has become a pillar of the understanding of Pleistocene glacial advances in the northern foreland of the Swiss Alps. However, both quartz and feldspar from the region are equally challenging as dosimeters with anomalous fading and partial bleaching being some of the obstacles to overcome for the establishment of decisive chronologies. In this study, luminescence properties of coarse- and fine-grained quartz, feldspar, and polymineral fractions of eight samples from a palaeovalley, Rinikerfeld in northern Switzerland, are systematically assessed. Standard performance tests are conducted on all four fractions. Deconvolution of luminescence signals of the quartz fractions is implemented and shows the dominance of stable fast components. Reader-specific low preheat temperatures are investigated on the infrared stimulated luminescence (IRSL) signal of feldspar. Thermal stability of this signal is found for low preheats, and thermal quenching could be excluded for higher preheats. However, anomalous fading is observed in the feldspar and polymineral IRSL signals and two correction approaches are applied. For one approach, fading corrected coarse-grained feldspar ages are consistent with those derived from quartz. In general, coarse-grained quartz and feldspar, as well as the fine-grained polymineral fraction of one sample, are in chrono-stratigraphic agreement and present negligible evidence for partial bleaching. However, ages derived from fine-grained quartz are found to underestimate those of the coarse-grained quartz fractions. Hence, the impact of alpha efficiency and water content on the dose rate and thus the ages are assessed. A finite explanation for the observed discrepancies remains lacking, but this systematic investigation of different luminescence signals allows for the establishment of a chronology for the palaeovalley fill dating back to at least Marine Isotope Stage 6 (MIS 6).


Author(s):  
Tengis S ◽  
Saran S ◽  
Munkhbayar L ◽  
Bemmann J

We investigated the potential of the optically stimulated luminescence (OSL) method to date young (<1000 years) samples collected in the Orkhon Valley Cultural Landscape, Mongolia. Quartz showed an infrared signal; therefore the post-IR OSL method was applied to small aliquots which are considered proxies for single grain measurements. Statistical analysis of the dose distribution produced CAM De of 5.14±0.10 Gy and over dispersion of 47.5%, and MAM De of 3.7±0.6 Gy. Since no partial bleaching was suspected, the analysis of signal composition was done and the fast quartz post-IR OSL lead to De of 4.9±0.2 Gy. Based on the quartz fast component and CAM De we propose the new chronology of ancient construction at 785±80 AD, rather than 906-1125 AD as suggested by archaeological evidence. However, the MAM age is in good agreement with independent age control for construction of the ramparts suggesting the date of reconstruction, collapse or reuse for the square walled enclosure MOR3 during 1090±80AD.


2012 ◽  
Vol 12 (7) ◽  
pp. 2177-2192 ◽  
Author(s):  
D. Brill ◽  
N. Klasen ◽  
K. Jankaew ◽  
H. Brückner ◽  
D. Kelletat ◽  
...  

Abstract. The Holocene beach-ridge plain of Phra Thong Island (Ko Phra Thong, SW Thailand) provides sedimentary evidence of several palaeotsunamis, in addition to the deposit of the 2004 Indian Ocean tsunami. Due to poor preservation conditions, these palaeoevent layers are restricted to swales. Correlation across beach ridges, which is important e.g. to reconstruct inundation distances, remains a major challenge. A primary tool for establishing a precisely confined correlation of the sand sheets is the use of chronological data. Since the application of radiocarbon dating is limited by the scarcity of appropriate material, this study utilised optically stimulated luminescence (OSL) dating of tsunamigenic quartz grains. Generally, the sediments showed favourable luminescence properties regarding signal intensity, dose recovery and thermal stability. Disturbances of the OSL signal due to partial bleaching were corrected using the minimum age model. At least three palaeoevents – being 490–550, 925–1035 and 1740–2000 yr old – were distinguished by dating the discontinuous sand sheets at four different sites. Besides this chronological framework, the OSL data provide the opportunity to correlate the discontinuous sand sheets between spatially separated sites within the same swale as well as across ridges. This allows for first estimates of inundation distances for the palaeotsunamis documented on Phra Thong Island. Furthermore, the two younger events overlap in age with contemporaneous tsunami and earthquake evidence from other coasts bordering the Indian Ocean.


2020 ◽  
Author(s):  
Daniela Mueller ◽  
Frank Preusser ◽  
Marius W. Buechi ◽  
Lukas Gegg ◽  
Gaudenz Deplazes

Abstract. Luminescence dating has become a pillar of the understanding of Pleistocene glacial advances in the northern foreland of the Swiss Alps. However, both quartz and feldspar from the region are equally challenging as dosimeters with anomalous fading, partial bleaching and unstable components being some of the obstacles to overcome. In this study, luminescence properties of coarse- and fine-grained quartz, feldspar and polymineral fractions of eight samples from a palaeovalley, Rinikerfeld, in northern Switzerland are assessed and found appropriate for dating. While anomalous fading of the IRSL signal of the feldspar and polymineral fraction is observed, fading corrected coarse-grained feldspar ages are consistent with those derived from quartz. In general, coarse-grained quartz and feldspar as well as the fine-grained polymineral fractions are in agreement and present negligible evidence for partial bleaching. However, ages derived from fine-grained quartz are found to underestimate those of the coarse-grained quartz fractions. Impact of total dose rate on finite ages was assessed but age underestimation is likely due to grain size dependent luminescence properties. The top six samples indicate sedimentation of at least 16.6 m during Marine Isotope Stage 6 with a rapid transition from a lacustrine environment to a landscape dominated by colluvial deposits. For the two lowest samples, no finite ages are derived.


2017 ◽  
Author(s):  
Yesong Han ◽  
◽  
Jiafu Zhang ◽  
Zhijiu Cui ◽  
Gengnian Liu
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