Electron Beam Physical Vapor Deposition (EBPVD)

Author(s):  
Mélanie Auffan ◽  
Catherine Santaella ◽  
Alain Thiéry ◽  
Christine Paillès ◽  
Jérôme Rose ◽  
...  
2006 ◽  
Vol 522-523 ◽  
pp. 267-276 ◽  
Author(s):  
Kunihiko Wada ◽  
Yutaka Ishiwata ◽  
Norio Yamaguchi ◽  
Hideaki Matsubara

Several kinds of thermal barrier coatings (TBCs) deposited by electron beam physical vapor deposition (EB-PVD) were produced as a function of electron beam power in order to evaluate their strain tolerance. The deposition temperatures were changed from 1210 K to 1303 K depending on EB power. In order to evaluate strain tolerances of the EB-PVD/TBCs, a uniaxial compressive spallation test was newly proposed in this study. In addition, the microstructures of the layers were observed with SEM and Young’s moduli were measured by a nanoindentation test. The strain tolerance in as-deposited samples decreased with an increase in deposition temperature. In the sample deposited at 1210 and 1268 K, high-temperature aging treatment at 1273 K for 10 h remarkably promoted the reduction of the strain tolerance. The growth of thermally grown oxide (TGO) layer generated at the interface between topcoat and bondcoat layers was the principal reason for this strain tolerance reduction. We observed TGO-layer growth even in the as-deposited sample. Although the thickness of the initial TGO layer in the sample deposited at high temperature was thicker, the growth rate during aging treatment was smaller than those of the other specimens. This result suggests that we can improve the oxidation resistance of TBC systems by controlling the processing parameters in the EB-PVD process.


2006 ◽  
Vol 38 (6) ◽  
pp. 651-658 ◽  
Author(s):  
O. N. Gerasimchuk ◽  
G. A. Sergienko ◽  
V. I. Bondarchuk ◽  
A. V. Terukov ◽  
Yu. S. Nalimov ◽  
...  

2014 ◽  
Vol 788 ◽  
pp. 652-656
Author(s):  
Xiu Lin ◽  
Guang Ping Song ◽  
Hua Song Gou ◽  
Yi Jie Zhao ◽  
Yang Chen ◽  
...  

Freestanding FeCrAl-Y2O3 amorphous/crystalline composite coating with a thickness of about 200μm has been produced from electron-beam physical vapor deposition of FeCrAl and yttria materials with a substrate temperature of 500 oC around. The microstructure was composed of columnar grains near the substrate side and an amorphous top layer. Local crystallization occurred during room temperature preservation. It is inferred that the crystallization activation energy of the material is very low.


2019 ◽  
Vol 813 ◽  
pp. 165-170
Author(s):  
Maria P. Nikolova ◽  
Stefan Valkov ◽  
Stoyan Parshorov ◽  
Emil Yankov ◽  
Peter Petrov

The aim of the present study was to characterize two kinds of TiN/TiO2 coatings in terms of topography, composition, and electrochemical stability after immersion in simulated body fluid (SBF). Micropatterning of the substrate (Ti-5Al-4V alloy) was done by using electron beam modification (EBM) by scanning electron beam while nanostructured TiN/TiO2 films were deposited over EBM Ti5Al4V substrates using two physical vapor deposition techniques: 1) magnetron sputtering, and 2) cathodic arc and glow-discharge methods. When immersed for 7 and 14 days in SBF at static conditions (37±0.05 °C, pH 7.4), Ca/P ratio of the apatite deposits increased from approximately 1.5 up to near stoichiometric (1.67), respectively. After the initial decrease, the pH of the solution during soaking increased gradually reaching values close to 7.7 for both coatings. However, the weight gain of the samples with Arc coatings after the immersion period in SBF was nearly three times more than those with magnetron deposited coating. The electrochemical potentiodynamic tests performed in SBF indicated a shift in the corrosion potentials towards nobler direction after 7 and 14 days of immersion compared to non-immersed samples, whereas the corrosion current density was slightly increased.


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