1H NMR spectroscopic studies reveal multiple conformers of cyclic opioid peptide analogs

Peptides ◽  
1992 ◽  
pp. 253-254
Author(s):  
Brian J. Marsden ◽  
Brian C. Wilkes ◽  
Peter W. Schiller
Peptides 1994 ◽  
1995 ◽  
pp. 632-633 ◽  
Author(s):  
P. W. Schiller ◽  
G. Weltrowska ◽  
T. M.-D. Nguyen ◽  
C. Lemieux ◽  
N. N. Chung

1970 ◽  
Vol 43 (1) ◽  
pp. 123-130 ◽  
Author(s):  
M Zahurul Haque ◽  
M Abdullah As Saki ◽  
M Umar Ali ◽  
M Yusuff Ali

Arjun (Terminalia arjuna) is a source of many potent, biologically active compounds, planned all over Bangladesh. The chemical examinations of its fruits were taken up to isolate and identify active principles. For this purpose fresh fruits of Terminalia arjuna were extracted with rectified spirit. The extract was then triturated with petroleum ether (40-60°C), which was then subjected to column chromatographic separation followed by PTLC. Such separation led to the isolation of some new pure compounds, TA-1 to TA-5. The structures of compounds were characterized through spectroscopic studies (IR, 1H-NMR and 13C-NMR). Key words: Arjun, TA-1, TA-5, Spectroscopic studies DOI: 10.3329.bjsir.v43i1.863 Bangladesh J. Sci. Ind. Res. 43(1),123-130, 2008


2019 ◽  
Vol 35 (1) ◽  
pp. 186-192 ◽  
Author(s):  
Ahmed S. Al-Janabi ◽  
Adnan A. Al-Dulaimi ◽  
Hayfa M. Gergees ◽  
Mohammed H. Saleh

Treatment of the chelated palladium(II) complex, trans-[Pd(K2-Sac-CH2O)2].2H2O with one mole equivalent of the diammines (L-L), L-L = 2,2'-bipyridine (bipy),. ethylene diamine (en), 1,10-phenanthroline (phen), or N,N-dimethyl ethylene diammine (dmen) in EtOH solvent afforded mixed ligand complexes of the type [Pd(K1-Sac-CH2O)2(L-L)] in 82-93% yield. While treatment of trans-[Pd(K2-Sac-CH2O)2].2H2O with two mole equivalents of the monoamines (L), L=pyridine (py), 3-methylpyridine (3-mpy) or 3-aminopyridine (3-apy) in EtOH solvent gave trans-[Pd(K1-Sac-CH2O)2(L)2] complexes in 86-89% yield The prepared complexes were characterized by elemental CHN analysis, .conductivity measurements,. infrared and 1H nmr spectra.


2000 ◽  
Vol 146 (1) ◽  
pp. 49-57 ◽  
Author(s):  
Robert C. Long ◽  
Klearchos K. Papas ◽  
Athanassios Sambanis ◽  
Ioannis Constantinidis

1995 ◽  
Vol 8 (8) ◽  
pp. 1046-1053 ◽  
Author(s):  
Maria L. Anthony ◽  
Elaine Holmes ◽  
Peter C. R. McDowell ◽  
Tim J. B. Gray ◽  
Melanie Blackmore ◽  
...  

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