Synthesis of a poly(sulfobetaine-co-polyhedral oligomeric silsesquioxane) hybrid monolith via an in-situ ring opening quaternization for use in hydrophilic interaction capillary liquid chromatography

2020 ◽  
Vol 187 (2) ◽  
Author(s):  
Wangming Tan ◽  
Ye Chen ◽  
Xiyue Xiong ◽  
Si Huang ◽  
Zhengfa Fang ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Ring Opening ◽  
Polyhedral Oligomeric Silsesquioxane ◽  
Capillary Liquid Chromatography ◽  
Hydrophilic Interaction ◽  
Oligomeric Silsesquioxane ◽  
Capillary Liquid

Facile one-pot preparation of an imidazolium embedded C8 hybrid monolith using polyhedral oligomeric silsesquioxane for capillary liquid chromatography

RSC Advances ◽  
2015 ◽  
Vol 5 (111) ◽  
pp. 91436-91440 ◽  
Author(s):  
Niu Zhang ◽  
Lu Zhang ◽  
Xiaoqiang Qiao ◽  
Yongli Wang ◽  
Hongyuan Yan ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Monolithic Column ◽  
Polyhedral Oligomeric Silsesquioxane ◽  
Capillary Liquid Chromatography ◽  
One Pot ◽  
Oligomeric Silsesquioxane ◽  
Capillary Liquid ◽  
Hybrid Monolithic Column

In this study, a novel imidazolium embedded C8 hybrid monolithic column based on polyhedral oligomeric silsesquioxane (POSS) was developed.

Preparation of polyhedral oligomeric silsesquioxane based hybrid monoliths by thiol-ene click chemistry for capillary liquid chromatography

The Analyst ◽  
2015 ◽  
Vol 140 (1) ◽  
pp. 265-271 ◽  
Author(s):  
Shufen Shen ◽  
Fanggui Ye ◽  
Cong Zhang ◽  
Yuhao Xiong ◽  
Linjing Su ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Click Chemistry ◽  
Click Reaction ◽  
Polyhedral Oligomeric Silsesquioxane ◽  
Capillary Liquid Chromatography ◽  
System P ◽  
Oligomeric Silsesquioxane ◽  
Capillary Liquid ◽  
Organic Silica ◽  
Silica Hybrid

A facile organic–silica hybrid monolith was prepared by a thiol-ene click reaction of polyhedral oligomeric silsesquioxane methacryl substituted (POSS-MA) with 1,4-bis(mercaptoacetoxy) butane (BMAB) using toluene and dodecanol as a porogenic system.

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