Effect of the ZrO2 concentration on the crystallization behavior and the mechanical properties of high-strength MgO–Al2O3–SiO2 glass–ceramics

2016 ◽  
Vol 52 (4) ◽  
pp. 1955-1968 ◽  
Author(s):  
Sabrina Seidel ◽  
Marc Dittmer ◽  
Wolfgang Wisniewski ◽  
Wolfram Höland ◽  
Christian Rüssel
2010 ◽  
Vol 177 ◽  
pp. 447-450 ◽  
Author(s):  
Xin Zhang ◽  
Yi Wen Hu ◽  
Yin Wu ◽  
Wen Jie Si

The purpose of this study was to evaluate the crystal phase formation behavior and its influence on the mechanical properties of LiO2-SiO2-P2O5 glass-ceramics system. High temperature XRD was used to analyze the crystal phase formation in situ. The crystalline phases in the material both before and after heat-treatment were also analyzed. The flexural strength was measured by three-point bending test according to ISO 6872:2008(E). The SEM analysis showed that the high strength of the glass-ceramics is attributed to the continuous interlocking microstructure with fine lithium disilicate crystallines.


2017 ◽  
Vol 130 ◽  
pp. 347-360 ◽  
Author(s):  
Gisele G. Santos ◽  
Francisco C. Serbena ◽  
Vladimir M. Fokin ◽  
Edgar D. Zanotto

2010 ◽  
Vol 92 ◽  
pp. 131-137 ◽  
Author(s):  
Qiu Hua Yuan ◽  
Pei Xin Zhang ◽  
Li Gao ◽  
Hai Lin Peng ◽  
Xiang Zhong Ren ◽  
...  

The crystallization behavior of MgO-Al2O3-SiO2 glass-ceramics by sol-gel technology was investigated by using x-ray diffraction (XRD), differential thermal analysis (DTA), Scanning electron microscopy (SEM). The results showed that: (1)α-cordierite phase was precipitated when the green body was calcined at 1050°C, and α-cordierite of high purity and stability could be formed at 1100°C; (2) Adding an appropriate amount of low melting point glass powder into the green body may provide liquid-phase environment during the sintering process, which will help enhance the tightness density of glass-ceramic, and thus improve its flexural strength.


2005 ◽  
Vol 351 (2) ◽  
pp. 149-157 ◽  
Author(s):  
Emilija Tkalcec ◽  
Stanislav Kurajica ◽  
Hrvoje Ivankovic

2007 ◽  
Vol 336-338 ◽  
pp. 1590-1592
Author(s):  
Xiao Dong Li ◽  
Jie Mo Tian ◽  
Chen Wang ◽  
Li Min Dong ◽  
Qing Feng Zan

Crystallization behavior of ZrO2-ZnO-Al2O3-SiO2 glass has been studied by differential thermal analysis, X-ray diffraction analysis and scanning electronic microscope. ZrO2 doped in the glass induces the phase separation effectively. The crystal phases obtained are gahnite (ZnAl2O4) and a small amount of ZrO2 phase. SEM photographs show that the crystal phases distribute uniformly in the glass ceramics and the grain sizes of glass ceramics after different heat treatment are less than 60nm.


2010 ◽  
Vol 502 (2) ◽  
pp. 387-391 ◽  
Author(s):  
Hsing-I Hsiang ◽  
Li-Then Mei ◽  
Chi-Shiung Hsi ◽  
Wen-Chang Liao ◽  
Fu-Su Yen

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