Green synthesis of gold nanoparticles by Allium sativum extract and their assessment as SERS substrate

2013 ◽  
Vol 16 (1) ◽  
Author(s):  
Cristina Coman ◽  
Loredana Florina Leopold ◽  
Olivia Dumitriţa Rugină ◽  
Lucian Barbu-Tudoran ◽  
Nicolae Leopold ◽  
...  
Author(s):  
Yoki Yulizar ◽  
Harits Atika Ariyanta ◽  
Lingga Abduracman

Gold nanoparticles (AuNPs) have been successfully prepared by green synthesis method using aqueous extract of garlic with the Latin name of Allium sativum L. (ASL) as a reducing and stabilizing agents. Identification of active compounds in aqueous ASL extract was conducted by phytochemical analysis and Fourier transform infrared (FTIR) spectroscopy, while the synthesized AuNPs were characterized using UV-Vis spectrophotometer and transmission electron microscopy-selected area electron diffraction (TEM-SAED). The AuNPs formation was optimized at aqueous ASL extract concentration of 0.05%, HAuCl4 concentration of 2.0×10-4 M, and pH of 3.6. The optimized AuNPs was characterized   using TEM, and has a spherical shape with particle size of 15±3 nm. The particles were also stable up until one month. The synthesized AuNPs has been studied its interaction with melamine, and showed the optimum pH of interaction at 3.6. Copyright © 2017 BCREC GROUP. All rights reservedReceived: 13rd November 2016; Revised: 3rd January 2017; Accepted: 10th February 2017How to Cite: Yulizar, Y., Ariyanta, H.A., Abdurrachman, L. (2017). Green Synthesis of Gold Nanoparticles using Aqueous Garlic (Allium sativum L.) Extract, and Its Interaction Study with Melamine. Bulletin of Chemical Reaction Engineering & Catalysis, 12 (2): 212-218 (doi:10.9767/bcrec.12.2.770.212-218)Permalink/DOI: http://dx.doi.org/10.9767/bcrec.12.2.770.212-218 


Catalysts ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 347
Author(s):  
Beomjin Kim ◽  
Woo Chang Song ◽  
Sun Young Park ◽  
Geuntae Park

The green synthesis of inorganic nanoparticles (NPs) using bio-materials has attained enormous attention in recent years due to its simple, eco-friendly, low-cost and non-toxic nature. In this work, silver nanoparticles (AgNPs) and gold nanoparticles (AuNPs) were synthesized by the marine algae extract, Sargassum serratifolium (SS). The characteristic studies of bio-synthesized SS-AgNPs and SS-AuNPs were carried out by using ultraviolet–visible (UV–Vis) absorption spectroscopy, dynamic light scattering (DLS), high-resolution transmission electron microscope (HR-TEM), selected area electron diffraction (SAED), energy-dispersive X-ray spectroscopy (EDX), X-ray powder diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR). Phytochemicals in the algae extract, such as meroterpenoids, acted as a capping agent for the NPs’ growth. The synthesized Ag and Au NPs were found to have important catalytic activity for the degradation of organic dyes, including methylene blue, rhodamine B and methyl orange. The reduction of dyes by SS-AgNPs and -AuNPs followed the pseudo-first order kinetics.


2019 ◽  
Vol 12 (8) ◽  
pp. 2310-2319 ◽  
Author(s):  
Nazar Ul Islam ◽  
Kamran Jalil ◽  
Muhammad Shahid ◽  
Naveed Muhammad ◽  
Abdur Rauf

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