Atom probe tomography analysis of nanostructure evolution in Ni-Cr-Mo low alloy steel under neutron irradiation

2017 ◽  
Vol 31 (8) ◽  
pp. 3675-3678
Author(s):  
Gyeong-Geun Lee ◽  
Hyung-Ha Jin ◽  
Kunok Chang ◽  
Sangyeob Lim ◽  
Min-Chul Kim ◽  
...  
The Analyst ◽  
2021 ◽  
Vol 146 (1) ◽  
pp. 69-74
Author(s):  
Elizabeth Kautz ◽  
John Cliff ◽  
Timothy Lach ◽  
Dallas Reilly ◽  
Arun Devaraj

235U enrichment in a metallic nuclear fuel was measured via NanoSIMS and APT, allowing for a direct comparison of enrichment across length scales and resolutions.


2015 ◽  
Vol 21 (S3) ◽  
pp. 843-844 ◽  
Author(s):  
F. A. Laiginhas ◽  
A. Perez-Huerta ◽  
R. L. Martens ◽  
T. J. Prosa ◽  
D. Reinhard

2012 ◽  
Vol 18 (S2) ◽  
pp. 928-929 ◽  
Author(s):  
D.J. Larson ◽  
D.A. Reinhard ◽  
T.J. Prosa ◽  
D. Olson ◽  
D. Lawrence ◽  
...  

Extended abstract of a paper presented at Microscopy and Microanalysis 2012 in Phoenix, Arizona, USA, July 29 – August 2, 2012.


Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4095
Author(s):  
Shenbao Jin ◽  
Haokai Su ◽  
Gang Sha

The stoichiometry of titanium carbide (TiCx) particles is important in determining particle properties. Spherical TiCx powders with particle sizes of 1–5 μm were produced by self-propagating high-temperature synthesis (SHS) in 30 wt.% Al–, 30 wt.% Cu–, and 30 wt.% Fe–Ti–C systems, respectively. To measure the compositions of the carbide powders, atom probe tomography (APT) tip specimens were carefully prepared by using a focus ion-beam milling method. APT analysis revealed that the TiCx particles formed in Al–, Cu–, and Fe–Ti–C systems are highly substoichiometric. The results are consistent with observations of the TiCx particles with a high content of oxygen and a certain amount of secondary metallic elements (Al, Cu, and Fe).


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