The qualitative and quantitative analysis of insect hemolymph sugars by high performance thin-layer chromatography

1990 ◽  
Vol 95 (4) ◽  
pp. 539-544 ◽  
Author(s):  
Richard D. Fell
1975 ◽  
Vol 58 (1) ◽  
pp. 44-47 ◽  
Author(s):  
Wendell F Phillips ◽  
John E Trafton

Abstract A screening method for the estimation of possible residues of sulfonamides in poultry tissues is described. The method utilizes thin layer chromatography (TLC) to separate Bratton-Marshall positive reactants. In the absence of interference and the identification of 1 sulfonamide by TLC, the colorimctric method is recommended for quantitation. When interferences are present, TLC should be used for both qualitative and quantitative analysis. The screening method has a sensitivity of less than 0.05 ppm and a recovery of greater than 80%.


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