Use of thermogravimetric analysis-Fourier transform infrared spectroscopy in the study of the reaction mechanism of the preparation of Pb(Zr, Ti)O3 by the sol-gel method

1996 ◽  
Vol 10 (2) ◽  
pp. 291-299 ◽  
Author(s):  
R. Nouwen ◽  
J. Mullens ◽  
D. Franco ◽  
J. Yperman ◽  
L.C. Van Poucke
Keyword(s):  
Fourier Transform ◽  
Infrared Spectroscopy ◽  
Reaction Mechanism ◽  
Thermogravimetric Analysis ◽  
Fourier Transform Infrared Spectroscopy ◽  
Sol Gel ◽  
Fourier Transform Infrared ◽  
Gel Method ◽  
Sol Gel Method

Production and characterization of boron nitride-doped nanofiber mats created through electrospinning

2016 ◽  
Vol 47 (6) ◽  
pp. 993-1005 ◽  
Author(s):  
Yasemin Cakmak ◽  
M Fatih Canbolat ◽  
Enes Cakmak ◽  
Mehmet Dayik
Keyword(s):  
Thermal Stability ◽  
Fourier Transform ◽  
Infrared Spectroscopy ◽  
Thermogravimetric Analysis ◽  
Boron Nitride ◽  
Fourier Transform Infrared Spectroscopy ◽  
Fourier Transform Infrared ◽  
Electrospinning Method ◽  
The Fourier Transform ◽  
Nanofiber Mats

The aim of this study was to produce advanced nanofiber mats by adding boron nitride to poly (ɛ-caprolactone) polymer using an electrospinning method and to characterize the resultant structures. Pure poly (ɛ-caprolactone) nanofiber mats and boron nitride-doped nanofiber mats prepared at different concentrations were compared. The morphological structures of the nanofiber mats were examined under a scanning electron microscope, spectroscopic analyses were conducted using Fourier transform infrared spectroscopy, and thermal stability was analyzed using a thermogravimetric analysis method. Successful electrospinning of boron nitride-doped nanofibers at lower voltages was achieved. The thermogravimetric analysis test found that the thermal stability of boron nitride-doped nanofiber mats is higher than that of pure nanofibers, which suggests that the produced composite material could be preferable in applications involving insulation and high temperature. On the other hand, the Fourier transform infrared spectroscopy results indicated that no chemical reaction occurred between boron nitride and the poly (ɛ-caprolactone) nanofibers.

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