Electrospray ionization tandem mass spectrometry for the simultaneous determination of opiates and cocaine in human hair

2011 ◽  
Vol 704 (1-2) ◽  
pp. 123-132 ◽  
Author(s):  
Martha Míguez-Framil ◽  
Antonio Moreda-Piñeiro ◽  
Pilar Bermejo-Barrera ◽  
José Ángel Cocho ◽  
María Jesús Tabernero ◽  
...  
2013 ◽  
Vol 96 (1) ◽  
pp. 110-115 ◽  
Author(s):  
Hui Gao ◽  
Minli Yang ◽  
Minglin Wang ◽  
Yansheng Zhao ◽  
Ya Cao ◽  
...  

Abstract A method combining SPE with HPLC/electrospray ionization-MS/MS was developed for simultaneous determination of 30 synthetic food additives, including synthetic colorants, preservatives, and sweeteners in soft drinks. All targets were efficiently separated using the optimized chromatographic and MS conditions and parameters in a single run within 18 min. The LOD of the analytes ranged from 0.01 to 20 μg/kg, and the method was validated with recoveries in the 80.8 to 106.4% range. This multisynthetic additive method was found to be accurate and reliable and will be useful to ensure the safety of food products, such as the labeling and proper use of synthetic food additives in soft drinks.


Talanta ◽  
2013 ◽  
Vol 117 ◽  
pp. 235-241 ◽  
Author(s):  
Ángel Antelo-Domínguez ◽  
José Ángel Cocho ◽  
María Jesús Tabernero ◽  
Ana María Bermejo ◽  
Pilar Bermejo-Barrera ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document