Ultra(high)-pressure liquid chromatography–electrospray ionization-time-of-flight-ion mobility-high definition mass spectrometry for the rapid identification and structural characterization of flavonoid glycosides from cauliflower waste

2014 ◽  
Vol 1323 ◽  
pp. 39-48 ◽  
Author(s):  
Gerard Bryan Gonzales ◽  
Katleen Raes ◽  
Sofie Coelus ◽  
Karin Struijs ◽  
Guy Smagghe ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
High Pressure ◽  
Liquid Chromatography ◽  
Ion Mobility ◽  
Rapid Identification ◽  
Flavonoid Glycosides ◽  
High Definition ◽  
Ionization Time ◽  
Ultra High Pressure

scholarly journals Ion Mobility–Mass Spectrometry for Bioanalysis

Separations ◽  
2021 ◽  
Vol 8 (3) ◽  
pp. 33
Author(s):  
Xavier Garcia ◽  
Maria del Mar Sabaté ◽  
Jorge Aubets ◽  
Josep Maria Jansat ◽  
Sonia Sentellas
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Ion Mobility Spectrometry ◽  
Ion Mobility ◽  
Biological Samples ◽  
Ion Mobility Mass Spectrometry ◽  
Exogenous Compounds ◽  
Analytical Separation

This paper aims to cover the main strategies based on ion mobility spectrometry (IMS) for the analysis of biological samples. The determination of endogenous and exogenous compounds in such samples is important for the understanding of the health status of individuals. For this reason, the development of new approaches that can be complementary to the ones already established (mainly based on liquid chromatography coupled to mass spectrometry) is welcomed. In this regard, ion mobility spectrometry has appeared in the analytical scenario as a powerful technique for the separation and characterization of compounds based on their mobility. IMS has been used in several areas taking advantage of its orthogonality with other analytical separation techniques, such as liquid chromatography, gas chromatography, capillary electrophoresis, or supercritical fluid chromatography. Bioanalysis is not one of the areas where IMS has been more extensively applied. However, over the last years, the interest in using this approach for the analysis of biological samples has clearly increased. This paper introduces the reader to the principles controlling the separation in IMS and reviews recent applications using this technique in the field of bioanalysis.

scholarly journals Fast log P determination by ultra-high-pressure liquid chromatography coupled with UV and mass spectrometry detections

2009 ◽  
Vol 394 (7) ◽  
pp. 1919-1930 ◽  
Author(s):  
Yveline Henchoz ◽  
Davy Guillarme ◽  
Sophie Martel ◽  
Serge Rudaz ◽  
Jean-Luc Veuthey ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
High Pressure ◽  
Liquid Chromatography ◽  
High Pressure Liquid Chromatography ◽  
Log P ◽  
Ultra High Pressure
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