Fibre/matrix adhesion of cellulose fibres in PLA, PP and MAPP: A critical review of pull-out test, microbond test and single fibre fragmentation test results

2014 ◽  
Vol 63 ◽  
pp. 133-148 ◽  
Author(s):  
Nina Graupner ◽  
Joraine Rößler ◽  
Gerhard Ziegmann ◽  
Jörg Müssig
Keyword(s):  
Critical Review ◽  
Single Fibre ◽  
Test Results ◽  
Cellulose Fibres ◽  
Matrix Adhesion ◽  
Fragmentation Test ◽  
Pull Out ◽  
Microbond Test ◽  
Fibre Matrix

An Energy-Based interpretation of Interfacial Adhesion from Single Fibre Composite Fragmentation Testing

1993 ◽  
Vol 2 (5) ◽  
pp. 096369359300200 ◽  
Author(s):  
H.D. Wagner ◽  
S. Ling
Keyword(s):  
Interfacial Adhesion ◽  
Mechanical Characteristics ◽  
Interfacial Shear Strength ◽  
Fibre Composite ◽  
Stress Transfer ◽  
Single Fibre ◽  
Transfer Length ◽  
Fragmentation Test ◽  
Energy Balance Approach ◽  
Fibre Matrix

An energy balance approach is proposed for the single fibre composite (or fragmentation) test, by which the degree of fibre-matrix bonding is quantified by means of the interfacial energy, rather than the interfacial shear strength, as a function of the fibre geometrical and mechanical characteristics, the stress transfer length, and the debonding length. The validity of the approach is discussed using E-glass fibres embedded in epoxy, both in the dry state and in the presence of hot distilled water.

scholarly journals Micromechanical Tests on Natural Fibre Composites with Enzymatically Enhanced Fibre–Matrix Adhesion

2021 ◽  
Vol 4 (1) ◽  
Author(s):  
Hanna M. Brodowsky ◽  
Anne Hennig
Keyword(s):  
Shear Strength ◽  
Single Fibre ◽  
Natural Fibre ◽  
Interfacial Shear ◽  
Frictional Stress ◽  
Reinforced Composites ◽  
Fragmentation Test ◽  
Fibre Pullout ◽  
Fibre Matrix ◽  
Fibre Reinforced Composites

Abstract Natural fibre–reinforced composites are more sustainable than other composites with respect to the raw materials. Their properties are attractive due to high specific properties, and especially so wherever high damping is valued. As the interphase between fibre and matrix is the region of highest stresses, a strong bond between fibre and matrix is essential for any composites’ properties. The present study compares two methods of determining the interfacial shear stress in natural fibre–reinforced composites: the single fibre fragmentation test and the single fibre pullout test. The studied composites are flax fibre reinforced epoxy. For a variety of fibre–matrix interaction, the fibres are treated with a laccase enzyme and dopamine, which is known to improve the fibre–matrix shear strength. In the observed samples, single fibre fragmentation test data, i.e. of fracture mode and fragment length, scatter when compared to pullout data. In single fibre pullout tests, the local interfacial shear strength showed a 30% increase in the laccase-treated samples, compared to the control samples. The method also permitted an evaluation of the frictional stress occurring after surface failure.

scholarly journals Electrolytic Surface Treatment for Improved Adhesion between Carbon Fibre and Polycarbonate

Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2253 ◽  
Author(s):  
Jan Henk Kamps ◽  
Luke Henderson ◽  
Christina Scheffler ◽  
Ruud van der Heijden ◽  
Frank Simon ◽  
...  
Keyword(s):  
Carbon Fibre ◽  
Surface Treatment ◽  
Photoelectron Spectroscopy ◽  
Surface Characteristics ◽  
Fibre Surface ◽  
Single Fibre ◽  
Optimum Level ◽  
Pull Out ◽  
Force Displacement ◽  
Fibre Matrix

To achieve good mechanical properties of carbon fibre-reinforced polycarbonate composites, the fibre-matrix adhesion must be dialled to an optimum level. The electrolytic surface treatment of carbon fibres during their production is one of the possible means of adapting the surface characteristics of the fibres. The production of a range of tailored fibres with varying surface treatments (adjusting the current, potential, and conductivity) was followed by contact angle, inverse gas chromatography and X-ray photoelectron spectroscopy measurements, which revealed a significant increase in polarity and hydroxyl, carboxyl, and nitrile groups on the fibre surface. Accordingly, an increase in the fibre-matrix interaction indicated by a higher interfacial shear strength was observed with the single fibre pull-out force-displacement curves. The statistical analysis identified the correlation between the process settings, fibre surface characteristics, and the performance of the fibres during single fibre pull-out testing.

scholarly journals Test Methods for Fibre/Matrix Adhesion in Cellulose Fibre-Reinforced Thermoplastic Composite Materials: A Critical Review

2020 ◽  
Vol 8 (2) ◽  
pp. 68-129
Author(s):  
J. Müssig ◽  
N. Graupner
Keyword(s):  
Composite Materials ◽  
Cellulose Fibre ◽  
Test Methods ◽  
Test Method ◽  
Thermoplastic Composite ◽  
Thermoplastic Composites ◽  
Cellulose Fibres ◽  
Reinforced Polymers ◽  
Matrix Adhesion ◽  
Fibre Matrix

Due to the increasing discussion about sustainable and CO2-reduced materials, the demand for cellulose-based fibres as a reinforcing component in thermoplastic composites has increased considerably. Knowledge about the possibilities of modifying fibres for improved adhesion to the plastic matrix is essential in this context. The fibre/matrix adhesion in cellulose fibre-reinforced polymers is of considerable importance for the design of composite materials. Unfortunately, there are no standards for many essential methods to determine fibre/matrix adhesion. In this review article, various methods for measuring the interfacial shear strength between fibres and matrix, as an indirect characterisation of adhesion, are presented. Additionally, a brief overview of different methods for surface modification of cellulose fibres to improve the adhesion to a thermoplastic matrix is given. This review focuses on the fact that the parameters for the production of test specimens as well as the test method itself can vary considerably from study to study. Because of this, the comparison of data from different publications is not always possible. Therefore, in this article, the main influencing factors and differences in the methods are presented and discussed. Based on a systematic review and a clear description and discussion of the methods, the reader is given a broad basis for a better understanding of characteristic values for fibre/matrix adhesion.

scholarly journals Analytical Fracture Mechanics Analysis of the Pull-Out Test Including the Effects of Friction and Thermal Stresses

2000 ◽  
Vol 9 (6) ◽  
pp. 096369350000900 ◽  
Author(s):  
John A. Nairn
Keyword(s):  
Energy Release Rate ◽  
Energy Release ◽  
Release Rate ◽  
Thermal Stresses ◽  
Interfacial Crack ◽  
Single Fibre ◽  
Finite Elements Analysis ◽  
Accurate Analysis ◽  
Pull Out ◽  
Microbond Test

The energy release rate for propagation of a debond in a single-fibre pull out test was derived analytically. The key finding was that an accurate analysis can be derived by a global energy analysis that includes effects of residual stresses and interfacial friction but does not need to include the details of the stress state at the interfacial crack tip. By comparison to finite elements analysis, it was verified that the analytical results are very accurate provided the debond tip is not too close to either end of the specimen. By casting the results in terms of net-specimen stress, it was possible to derive a general energy release rate result that applies to both the pull-out test and the related microbond test. The energy release rate expressions can be used to determine interfacial fracture toughness from single-fibre pull-out tests or microbond tests.

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