scholarly journals Test Methods for Fibre/Matrix Adhesion in Cellulose Fibre-Reinforced Thermoplastic Composite Materials: A Critical Review

2020 ◽  
Vol 8 (2) ◽  
pp. 68-129
Author(s):  
J. Müssig ◽  
N. Graupner
Keyword(s):  
Composite Materials ◽  
Cellulose Fibre ◽  
Test Methods ◽  
Test Method ◽  
Thermoplastic Composite ◽  
Thermoplastic Composites ◽  
Cellulose Fibres ◽  
Reinforced Polymers ◽  
Matrix Adhesion ◽  
Fibre Matrix

Due to the increasing discussion about sustainable and CO2-reduced materials, the demand for cellulose-based fibres as a reinforcing component in thermoplastic composites has increased considerably. Knowledge about the possibilities of modifying fibres for improved adhesion to the plastic matrix is essential in this context. The fibre/matrix adhesion in cellulose fibre-reinforced polymers is of considerable importance for the design of composite materials. Unfortunately, there are no standards for many essential methods to determine fibre/matrix adhesion. In this review article, various methods for measuring the interfacial shear strength between fibres and matrix, as an indirect characterisation of adhesion, are presented. Additionally, a brief overview of different methods for surface modification of cellulose fibres to improve the adhesion to a thermoplastic matrix is given. This review focuses on the fact that the parameters for the production of test specimens as well as the test method itself can vary considerably from study to study. Because of this, the comparison of data from different publications is not always possible. Therefore, in this article, the main influencing factors and differences in the methods are presented and discussed. Based on a systematic review and a clear description and discussion of the methods, the reader is given a broad basis for a better understanding of characteristic values for fibre/matrix adhesion.

scholarly journals Mechanical Properties of Compression Moulded Aggregate-Reinforced Thermoplastic Composite Scrap

2021 ◽  
Vol 5 (11) ◽  
pp. 299
Author(s):  
Julien Moothoo ◽  
Mahadev Bar ◽  
Pierre Ouagne
Keyword(s):  
Mechanical Properties ◽  
Tensile Properties ◽  
Test Method ◽  
Thermoplastic Composite ◽  
Recycled Aggregate ◽  
Thermoplastic Composites ◽  
Mechanical Recycling ◽  
Compression Moulding ◽  
Grain Sizes ◽  
Recycled Composites

Recycling of thermoplastic composites has drawn a considerable attention in the recent years. However, the main issue with recycled composites is their inferior mechanical properties compared to the virgin ones. In this present study, an alternative route to the traditional mechanical recycling technique of thermoplastic composites has been investigated with the view to increase mechanical properties of the recycled parts. In this regard, the glass/polypropylene laminate offcuts are cut in different grain sizes and processed in bulk form, using compression moulding. Further, the effect of different grain sizes (i.e., different lengths, widths and thicknesses) and other process-related parameters (such as mould coverage) on the tensile properties of recycled aggregate-reinforced composites have been investigated. The tensile properties of all composite samples are tested according to ISO 527-4 test method and the significance of test results is evaluated according to Student’s t-test and Fisher’s F-test respectively. It is observed that the tensile moduli of the recycled panels are close to the equivalent quasi-isotropic continuous fibre-reinforced reference laminate while there is a noteworthy difference in the strengths of the recycled composites. At this stage, the manufactured recycled composites show potential for stiffness-driven application.

Enhanced Infrared Heating of Thermoplastic Composite Sheets for Thermoforming Processes

2021 ◽  
Vol 36 (1) ◽  
pp. 35-43
Author(s):  
M. Längauer ◽  
G. Zitzenbacher ◽  
C. Burgstaller ◽  
C. Hochenauer
Keyword(s):  
Steady State ◽  
Composite Materials ◽  
Mechanical Performance ◽  
Heating Time ◽  
Thermoplastic Composite ◽  
Infrared Heating ◽  
Thermoplastic Composites ◽  
Steady State Condition ◽  
Reflector System ◽  
Heating Station

Abstract Thermoforming of thermoplastic composites attracts increasing attention in the community due to the mechanical performance of these materials and their recyclability. Yet there are still difficulties concerning the uniformity of the heating and overheating of parts prior to forming. The need for higher energy efficiencies opens new opportunities for research in this field. This is why this study presents a novel experimental method to classify the efficiency of infrared heaters in combination with different thermoplastic composite materials. In order to evaluate this, different organic sheets are heated in a laboratory scale heating station until a steady state condition is reached. This station mimics the heating stage of an industrial composite thermoforming device and allows sheets to slide on top of the pre-heated radiator at a known distance. By applying thermodynamic balances, the efficiency of chosen parameters and setups is tested. The tests show that long heating times are required and the efficiency of the heating is low. Furthermore, the efficiency is strongly dependent on the distance of the heater to the sheet, the heater temperature and also the number of heating elements. Yet, using a full reflector system proves to have a huge effect and the heating time can be decreased by almost 50%.

Review of material test standardization status for the material qualification of laminated thermosetting composite structures

2020 ◽  
pp. 073168442095810
Author(s):  
Sang Yoon Park ◽  
Won Jong Choi
Keyword(s):  
Composite Materials ◽  
Material Properties ◽  
Composite Structures ◽  
Failure Modes ◽  
Laminated Composite ◽  
Test Methods ◽  
Test Method ◽  
Experimental Comparison ◽  
Laminated Composite Materials ◽  
Design Values

This paper presents a review of recent literature related to the static mechanical testing of thermoset-based carbon fiber reinforced composites and introduces a material qualification methodology to generate statistically-based allowable design values for aerospace application. Although most test methods have been found to be effective in determining the specific material properties by incorporating them into the material qualification and quality control provisions, a full validation to clarify the behavior of thermoset-based laminated composite materials is currently lacking, particularly with regard to the characterization of compressive, in-plane, interlaminar shear, and damage tolerance properties. The present study obtains information on the different types of test method that can be employed within the same material properties, and makes an in-depth experimental comparison based on the past literatures. A discussion on the scope of theoretical analysis involves a description of how the proposed test method can be adequate for obtaining more accurate material properties. This discussion is directly applicable to the assessment of material nonlinearity and the geometrical effect of specimens. Finally, the resulting failure modes and the effect of each material property are studied to aid the understanding of the load distribution and behavior of laminated composite materials.

The Pseudomonas fluorescens SBW25 wrinkly spreader biofilm requires attachment factor, cellulose fibre and LPS interactions to maintain strength and integrity

Microbiology ◽  
2005 ◽  
Vol 151 (9) ◽  
pp. 2829-2839 ◽  
Author(s):  
Andrew J. Spiers ◽  
Paul B. Rainey
Keyword(s):  
Pseudomonas Fluorescens ◽  
Insertion Site ◽  
Cellulose Fibre ◽  
Cellulose Fibres ◽  
Pseudomonas Fluorescens Sbw25 ◽  
Increased Strength ◽  
Biofilm Development ◽  
Air Liquid Interface ◽  
Attachment Factor ◽  
Fibre Matrix

The wrinkly spreader (WS) isolate of Pseudomonas fluorescens SBW25 forms a substantial biofilm at the air–liquid interface. The biofilm is composed of an extracellular partially acetylated cellulose-fibre matrix, and previous mutagenesis of WS with mini-Tn5 had identified both the regulatory and cellulose-biosynthetic operons. One uncharacterized WS mutant, WS-5, still expressed cellulose but produced very weak biofilms. In this work, the mini-Tn5 insertion site in WS-5 has been identified as being immediately upstream of the tol-pal operon. Like Tol-Pal mutants of other Gram-negative bacteria, WS-5 showed a ‘leaky-membrane’ phenotype, including the serendipitous ability to utilize sucrose, increased uptake of the hydrophilic dye propidium iodide, and the loss of lipopolysaccharide (LPS) expression. WS-5 cells were altered in relative hydrophobicity, and showed poorer recruitment and maintenance in the biofilm than WS. The WS-5 biofilm was also less sensitive to chemical interference during development. However, growth rate, cellulose expression and attachment were not significantly different between WS and WS-5. Finally, WS-5 biofilms could be partially complemented with WS-4, a biofilm- and attachment-deficient mutant that expressed LPS, resulting in a mixed biofilm with significantly increased strength. These findings show that a major component of the WS air–liquid biofilm strength results from the interactions between LPS and the cellulose matrix of the biofilm – and that in the WS biofilm, cellulose fibres, attachment factor and LPS are required for biofilm development, strength and integrity.

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