scholarly journals Effect of calcination temperature on Microstructures, magnetic properties, and microwave absorption on BaFe11.6Mg0.2Al0.2O19 synthesized from natural iron sand

2019 ◽  
Vol 13 ◽  
pp. 100393 ◽  
Author(s):  
Martha Rianna ◽  
Timbangen Sembiring ◽  
Marhaposan Situmorang ◽  
Candra Kurniawan ◽  
Anggito P. Tetuko ◽  
...  
2020 ◽  
Vol 855 ◽  
pp. 255-260
Author(s):  
Mukhtar Effendi ◽  
Efi Solihah ◽  
Candra Kurniawan ◽  
Wahyu Tri Cahyanto ◽  
Wahyu Widanarto

The synthesize of Nd3+-strontium hexaferrite magnetic material by the solid-state reaction method has been successfully carried out. This study aims to determine the effect of Nd3+ on the structure, magnetic properties, and microwave absorption capability of the material. Preparation of (1-x)SrO:xNd2O3:6Fe2O3 where x = 0, 10, 20, and 30 mol% using basic material in the form of SrCO3 powder, Nd2O3 powder and Fe3O4 from natural iron sand. The characterization includes the X-Ray Diffraction (XRD) examination to determine the crystal structure, the Scanning Electron Microscope (SEM) for exploring the surface morphology, Vibrating Sample Magnetometer (VSM) for the magnetic properties investigation of material, and Vector Network Analyzer (VNA) for microwave absorption capability analysis. The XRD results show that the addition of Nd3+ doping increases the number of SrNdFeO4 phases. The phase has a tetragonal crystal system that has cell parameters a = b = 3.846 Å, and c = 12.594 Å. The magnetic properties of the material showed that the addition of Nd3+ decreased the saturation and remanence magnetization values, whereas the value of the coercivity field increased. Meanwhile, the best microwave absorption occurs in samples with the addition of Nd3+ as much as 0.3 mol, which results in a reflection loss value of -18.9 dB with a frequency bandwidth of 3.9 GHz.


2019 ◽  
Vol 256 ◽  
pp. 126612 ◽  
Author(s):  
Martha Rianna ◽  
Marhaposan Situmorang ◽  
Candra Kurniawan ◽  
Anggito P. Tetuko ◽  
Eko Arief Setiadi ◽  
...  

Author(s):  
Jinxiang Guo ◽  
Zhaofei Tong ◽  
Qihua Liang ◽  
Fangyu Gan ◽  
Lepeng Wei ◽  
...  

2020 ◽  
Vol 20 (5) ◽  
pp. 2998-3003
Author(s):  
Jia Liu ◽  
Zhou Wang ◽  
Yanyan Wang

A novel type of magnetic Fe2O3/Fe3O4 heterogeneous microparticles with ellipsoidal macropores was prepared via the ethanol-water reflux and rapid combustion process. The experimental results showed that the volume of absolute ethyl alcohol and the calcination temperature were the key factors to the grain sizes and the magnetic properties, the calcination temperature largely affected the saturation magnetization and the grain size of Fe2O3/Fe3O4 heterogeneous microparticles, and the amount of absolute ethyl alcohol also tremendously affected the saturation magnetization, however, the amount of absolute ethyl alcohol affected little on the grain size. Fe2O3/Fe3O4 heterogeneous microparticles calcined at 200 °C for 1 h with absolute ethyl alcohol of 20 mL had the largest saturation magnetization of 90.1 Am2/kg.


1999 ◽  
Vol 13 (02) ◽  
pp. 59-69
Author(s):  
K. SUGAWARA ◽  
N. OHYA ◽  
N. ARAI ◽  
S. ICHIMURA ◽  
K. YAMAMOTO ◽  
...  

Several samples of K 3 C 60 have been made by the calcination of C 60 powder plus K flakes in evacuated quartz tubes at temperatures between 100°C and 700°C for 24 hours. The non-resonant microwave absorption (NRMA) measurements have been done below T c for these samples. From the linewidths and intensities of the NRMA signals, the superconducting properties (T c superconducting volume fraction and vortex size) have been studied as a function of the calcination temperature.


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