Microwave assisted synthesis and optimization of Aegle marmelos-g-poly(acrylamide): Release kinetics studies

2014 ◽  
Vol 65 ◽  
pp. 462-470 ◽  
Author(s):  
A. Setia ◽  
R. Kumar
Keyword(s):  
Release Kinetics ◽  
Microwave Assisted Synthesis ◽  
Aegle Marmelos ◽  
Microwave Assisted ◽  
Kinetics Studies ◽  
Poly Acrylamide

scholarly journals MASTIC-G-POLY (ACRYLAMIDE): MICROWAVE-ASSISTED SYNTHESIS AND CHARACTERISATION

2021 ◽  
pp. 228-234
Author(s):  
MOHIT KUMAR ◽  
SURAJPAL
Keyword(s):  
Design Space ◽  
Maximum Yield ◽  
Ceric Ammonium Nitrate ◽  
Microwave Assisted Synthesis ◽  
Box Behnken Design ◽  
Critical Quality Attributes ◽  
Grafting Efficiency ◽  
Microwave Assisted ◽  
Free Radical Initiator ◽  
Poly Acrylamide

Objective: The objective of the present investigation was the synthesis of grafted co-polymer gum mastic using acrylamide as the monomer. Methods: 3-factor 3-level response surface Box-Behnken design, which requires 15 runs including three replicates of the central run, was used for the synthesis of graft copolymers of mastic gum with acrylamide using ceric ammonium nitrate as the free radical initiator. The critical synthesis and process parameters; CSPP (A = concentration of monomer, B = concentration of initiator and C= Temperature) to generate design space and optimize formulation with an aim to obtain critical quality attributes (CQA, Y1 =% Yield, Y2 =% Grafting, Y3 =% grafting efficiency). Result: Formulation F14 having a maximum % yield of 75.89% with % grafting of 210% and % grafting efficiency 51.57% was selected as best. Conclusion: The microwave-assisted grafted mastic gum was prepared successfully and optimized by using Box Behnken design.

Microwave Assisted Synthesis of Cationic Amino Sugar Surfactants

2020 ◽  
Vol 57 (3) ◽  
pp. 265-272
Author(s):  
Priya S. Singh ◽  
Aizaz Shaikh ◽  
Aditi Deshmukh ◽  
Amit P. Pratap
Keyword(s):  
Amino Sugar ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted
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