Investigation of formation mechanism of Ti3SiC2 by self-propagating high-temperature synthesis

2013 ◽  
Vol 41 ◽  
pp. 152-161 ◽  
Author(s):  
Fanai Meng ◽  
Baoyan Liang ◽  
Mingzhi Wang
Keyword(s):  
High Temperature ◽  
Formation Mechanism ◽  
Temperature Synthesis ◽  
High Temperature Synthesis

Effect of Mg on the Synthesis of TiB2 Powder by a Self-Propagating High-Temperature Synthesis Technique

2013 ◽  
Vol 347-350 ◽  
pp. 1144-1147
Author(s):  
Su Li ◽  
Jun Shou Li ◽  
Fang Zhao ◽  
Ming Hui Ye
Keyword(s):  
High Temperature ◽  
Combustion Synthesis ◽  
Formation Mechanism ◽  
Molar Ratio ◽  
Synthesis Reaction ◽  
Hexagonal Crystal ◽  
Temperature Synthesis ◽  
High Temperature Synthesis ◽  
Higher Temperature ◽  
Combustion Synthesis Reaction

Micro-nanoTiB2 ceramic was prepared through increasing the molar ratio of Mg and leaching with suitable acid by the combustion synthesis reaction of Mg, TiO2 and B2O3, which could get higher temperature and purer product. The Samples were investigated by XRD and SEM, and the results showed the diameter of the TiB2 was 200 nm ~ 300 nm and the shape of the TiB2 was irregular hexagonal crystal. The diameter of the TiB2 was decreased with the increase of Mg powder. The formation mechanism of TiB2 has been studied.

Development of SHS-Si3N4 in LSCPM

2007 ◽  
Vol 280-283 ◽  
pp. 1191-1196 ◽  
Author(s):  
Chang Chun Ge ◽  
Wei Ping Shen ◽  
Fei Wang
Keyword(s):  
High Temperature ◽  
Process Control ◽  
Formation Mechanism ◽  
The Self ◽  
Temperature Synthesis ◽  
High Temperature Synthesis ◽  
The World ◽  
Solid System

Since 1990, Ge and his earlier and present groups in LSCPM have made great efforts to investigate the Self-propagating High-temperature Synthesis (SHS) of Si-N2 gas-solid system including the SHS process control and its thermodynamics, structural macrokinetics and formation mechanism of SHS-Si3N4. In this presentation, some results that were firstly reported in the world are reviewed and new progress in recent years is reported.

Formation mechanism of Ti2AlC under the self-propagating high-temperature synthesis (SHS) mode

2012 ◽  
Vol 47 (5) ◽  
pp. 1164-1168 ◽  
Author(s):  
Shinobu Hashimoto ◽  
Noriko Nishina ◽  
Kiyoshi Hirao ◽  
You Zhou ◽  
Hideki Hyuga ◽  
...  
Keyword(s):  
High Temperature ◽  
Formation Mechanism ◽  
The Self ◽  
Temperature Synthesis ◽  
High Temperature Synthesis

Investigation of formation mechanism of Ti3SiC2 by high pressure and high-temperature synthesis

2018 ◽  
Vol 38 (4) ◽  
pp. 440-447 ◽  
Author(s):  
Xuhai Li ◽  
Liang Xu ◽  
Qingyun Chen ◽  
Xiuxia Cao ◽  
Lixin Liu ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Formation Mechanism ◽  
Temperature Synthesis ◽  
High Temperature Synthesis

Study on Phase Stability during Pressure-Less Sintering Process of Slag α-Sialon Powder and Properties of As-Sintered Materials

2013 ◽  
Vol 746 ◽  
pp. 97-100 ◽  
Author(s):  
He Zhang ◽  
Yao Deng ◽  
Ying Zhang ◽  
Jiu Xin Jiang
Keyword(s):  
High Temperature ◽  
Formation Mechanism ◽  
Phase Stability ◽  
Sintering Process ◽  
Temperature Synthesis ◽  
High Temperature Synthesis ◽  
Unit Cells ◽  
Different Temperatures ◽  
Sialon Powder ◽  
Sintered Materials

The pressure-less sintering of slag α-Sialon powder, derived from slag wastes by self-propagating high-temperature synthesis technology, was carried out and the phase assemblages of slag α-Sialon sintered at different temperatures were studied. The results showed that the formation of β-Sialon phase did occur during the pressure-less sintering and was restrained to some extent via mass diffusion of Ca2+/Mg2+ added in embedded powder in samples. α-Sialon phase with two different unit cells was detected in samples sintered at 1700°C and above, and the formation mechanism was also discussed.

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