scholarly journals Observations of breakage for transversely isotropic shale using acoustic emission and X-ray computed tomography: Effect of bedding orientation, pre-existing weaknesses, and pore water

Author(s):  
Guanyi Lu ◽  
Dustin Crandall ◽  
Andrew P. Bunger
2010 ◽  
Vol 24 (12) ◽  
pp. 2347-2352 ◽  
Author(s):  
Tetsuya Suzuki ◽  
Hidehiko Ogata ◽  
Ryuichi Takada ◽  
Masao Aoki ◽  
Masayasu Ohtsu

Materials ◽  
2019 ◽  
Vol 12 (16) ◽  
pp. 2569 ◽  
Author(s):  
Kaige Wu ◽  
Kaita Ito ◽  
Ippei Shinozaki ◽  
Pornthep Chivavibul ◽  
Manabu Enoki

An accurate evaluation of stress corrosion cracking (SCC) in 13Cr martensitic stainless steel (MSS) is still missing due to the lack of an in-situ insight into the process evolution and full characterization of the corrosion morphology. In this work, two main regimes involved in the SCC progression, including localized corrosion and cracking, were comparatively studied using in-situ acoustic emission (AE) monitoring and three-dimensional (3D) X-ray computed tomography (XCT) scanning. The stress corrosion tests were conducted with u-bent smooth specimens subjected to a single droplet of 1 μL 1% neutral NaCl solution. Localized corrosion and cracking evolution were controlled in tempered and quenched steel specimens, respectively. From XCT scanning, localized corrosion was featured by an irregular corrosion pit with deposited corrosion products containing cracks. The single dominant SCC crack was observed to initiate from corrosion pit and propagate with a 3D tortuous and discontinuous morphology. AE signals were detected in both cases. Correlated with in-situ observations and clustering analysis, source identification of AE signals was proposed. AE signals during localized corrosion were assessed to be mainly from cracking within the deposited corrosion products. Comparatively, hydrogen-bubble evolution, plastic deformation, and crack-branches coalescence were proposed as the AE sources of cracking evolution.


2021 ◽  
Author(s):  
Weina Yuan ◽  
Wen Fan

Abstract The macroscopic properties of loess are significantly controlled by its microstructure. Quantitative analysis of loess microstructure is essential for modeling the microstructure and further incorporating the microstructural effects into geotechnical practice. However, loess has a multi-scale microstructure ranging from nanometer to millimeter scales, and researches at the particle resolution are still inadequate. This study systematically investigates the micrometer-scale microstructure of loess from Jingyang, China, via X-ray computed tomography and the image segmentation method that was explored for loess. The statistical analyses of three-dimensional (3D) microstructure reveal that the particle size follows the Weibull distribution, and the distributions of pore and pore throat sizes obey the gamma distribution. Most particles are blade-shaped, with a peak length ratio of (1.53–1.64):1.28:1. The particles are oriented in the polar directions but not azimuthally, in a spherical coordinate system, exhibiting a transversely isotropic structure. The quantitative microstructures of the loess and paleosol samples were slightly different irrespective of the large aggregates developed in paleosol sample. Moreover, the representative elementary volume obtained through porosity is also applicable for the analysis of microstructural parameters such as size distribution, shape factor, orientation angle, and pore connectivity. Besides, the two-dimensional (2D) distributions of the particle, pore, and pore throat sizes agree with the 3D distributions, except that the former were marginally smaller. However, the 2D sectional analysis of shape, arrangement, and pore connectivity cannot adequately represent the 3D characteristics.


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