Crack identification and evaluation in BEoL stacks of two different samples utilizing acoustic emission testing and nano X-ray computed tomography

2021 ◽  
Vol 121 ◽  
pp. 114137
Author(s):  
Jendrik Silomon ◽  
Jürgen Gluch ◽  
André Clausner ◽  
Jens Paul ◽  
Ehrenfried Zschech
Minerals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 539 ◽  
Author(s):  
Yu Wang ◽  
Changhong Li ◽  
Zhiqiang Hou ◽  
Xuefeng Yi ◽  
Xiaoming Wei

Cemented waste rock backfill (CWRB), which is a mixture of tailings, waste rock, cement, and water, is subjected to combination actions in underground mining operations and has been widely used in deep resource mining. While the strength requirement and macroscopic deformation behaviors of CWRB have been well studied, the mesoscopic damage evolution mechanisms are still not well understood. In this work, a CWRB sample with a waste rock proportion of 30% was studied with a uniaxial compression test under tomographic monitoring, using a 450 kV industrial X-ray computed tomography (CT). Clear CT images, CT value analysis, crack identification, and extraction reveal that CWRB damage evolution is extremely inhomogeneous and affected by the waste rock size, shape, and distribution. Furthermore, the crack initiation, propagation, and coalescence behaviors are limited to the existing waste rocks. When deformation grows to a certain extent, the cracks demonstrate an interlocking phenomenon and their propagation paths are affected by the waste rocks, which may improve the ability to resist compressive deformation. Volumetric dilatancy caused by the damage and cracking behavior has closed a link with the meso-structural changes, which are controlled by the interactions between the waste rocks and the cemented tailing paste.


2010 ◽  
Vol 24 (12) ◽  
pp. 2347-2352 ◽  
Author(s):  
Tetsuya Suzuki ◽  
Hidehiko Ogata ◽  
Ryuichi Takada ◽  
Masao Aoki ◽  
Masayasu Ohtsu

Materials ◽  
2019 ◽  
Vol 12 (16) ◽  
pp. 2569 ◽  
Author(s):  
Kaige Wu ◽  
Kaita Ito ◽  
Ippei Shinozaki ◽  
Pornthep Chivavibul ◽  
Manabu Enoki

An accurate evaluation of stress corrosion cracking (SCC) in 13Cr martensitic stainless steel (MSS) is still missing due to the lack of an in-situ insight into the process evolution and full characterization of the corrosion morphology. In this work, two main regimes involved in the SCC progression, including localized corrosion and cracking, were comparatively studied using in-situ acoustic emission (AE) monitoring and three-dimensional (3D) X-ray computed tomography (XCT) scanning. The stress corrosion tests were conducted with u-bent smooth specimens subjected to a single droplet of 1 μL 1% neutral NaCl solution. Localized corrosion and cracking evolution were controlled in tempered and quenched steel specimens, respectively. From XCT scanning, localized corrosion was featured by an irregular corrosion pit with deposited corrosion products containing cracks. The single dominant SCC crack was observed to initiate from corrosion pit and propagate with a 3D tortuous and discontinuous morphology. AE signals were detected in both cases. Correlated with in-situ observations and clustering analysis, source identification of AE signals was proposed. AE signals during localized corrosion were assessed to be mainly from cracking within the deposited corrosion products. Comparatively, hydrogen-bubble evolution, plastic deformation, and crack-branches coalescence were proposed as the AE sources of cracking evolution.


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