Boosting C3-alcohol electrooxidations by co-fueling with formic acid: A real-time quantitative nuclear magnetic resonance spectroelectrochemical study

Author(s):  
Ye Feng ◽  
Xin-Yi Hou ◽  
Li-Fei Ji ◽  
Shuo-Hui Cao ◽  
Wen-Long Jiang ◽  
...  
Talanta ◽  
2014 ◽  
Vol 125 ◽  
pp. 94-101 ◽  
Author(s):  
Ting Huang ◽  
Wei Zhang ◽  
Xinhua Dai ◽  
Xiaoguang Zhang ◽  
Can Quan ◽  
...  

2019 ◽  
Vol 141 (51) ◽  
pp. 20209-20214 ◽  
Author(s):  
James Eills ◽  
Eleonora Cavallari ◽  
Carla Carrera ◽  
Dmitry Budker ◽  
Silvio Aime ◽  
...  

Molecules ◽  
2020 ◽  
Vol 25 (20) ◽  
pp. 4675
Author(s):  
Ninad Mehendale ◽  
Felix Jenne ◽  
Chandrakant Joshi ◽  
Swati Sharma ◽  
Shyam Kumar Masakapalli ◽  
...  

We present a Nuclear Magnetic Resonance (NMR) compatible platform for the automated real-time monitoring of biochemical reactions using a flow shuttling configuration. This platform requires a working sample volume of ∼11 mL and it can circulate samples with a flow rate of 28 mL/min, which makes it suitable to be used for real-time monitoring of biochemical reactions. Another advantage of the proposed low-cost platform is the high spectral resolution. As a proof of concept, we acquire 1H NMR spectra of waste orange peel, bioprocessed using Trichoderma reesei fungus, and demonstrate the real-time measurement capability of the platform. The measurement is performed over more than 60 h, with a spectrum acquired every 7 min, such that over 510 data points are collected without user intervention. The designed system offers high resolution, automation, low user intervention, and, therefore, time-efficient measurement per sample.


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