One-step controlled synthesis of anisotropic gold nanostructures with aniline as the reductant in aqueous solution

2007 ◽  
Vol 309 (2) ◽  
pp. 518-523 ◽  
Author(s):  
Zhirui Guo ◽  
Yu Zhang ◽  
Lan Huang ◽  
Meng Wang ◽  
Jing Wang ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Gold Nanostructures ◽  
Controlled Synthesis ◽  
One Step

Controlled Synthesis of Gold Nanostructures by a Thermal Approach

2008 ◽  
Vol 8 (7) ◽  
pp. 3465-3472 ◽  
Author(s):  
Min Zhou ◽  
Michael Bron ◽  
Wolfgang Schuhmann
Keyword(s):  
Aqueous Solution ◽  
Experimental Parameter ◽  
Thermal Reduction ◽  
Gold Nanostructures ◽  
Controlled Synthesis ◽  
Oh Groups ◽  
Generic Strategy ◽  
One Step ◽  
Different Shapes ◽  
Shape Controlled

Shape-controlled gold nanostructures were successfully synthesized in an aqueous solution by a one-step, non-templated thermal reduction method through heating of a poly(vinylpyrrolidone)/HAuCl4 aqueous solution. Poly(vinylpyrrolidone) (PVP) serves as both the stabilizing surfactant and reducing agent for the controlled synthesis of gold nanostructures with different shapes. Upon adjusting the chain-length and the concentration of the PVP, decahedral, icosahedral and platelike gold nanostructures with dominating distribution were fabricated, respectively, with the ratio of terminating OH groups at the polymer to Au ions as an important experimental parameter. The results suggest that the morphology of the gold nanostructures could be tuned by this method. The successful preparation of gold nanostructures exemplifies a very facile, effective, and generic strategy for fabrication of gold nanoparticles with various shapes.

A Simple Synthesis of the Anticancer Drug Altretamine

2020 ◽  
Vol 17 (8) ◽  
pp. 628-630
Author(s):  
Vu Binh Duong ◽  
Pham Van Hien ◽  
Tran Thai Ngoc ◽  
Phan Dinh Chau ◽  
Tran Khac Vu
Keyword(s):  
Aqueous Solution ◽  
Anticancer Drug ◽  
Potassium Hydroxide ◽  
Large Scale ◽  
Synthesis Method ◽  
Practical Method ◽  
Cyanuric Chloride ◽  
Simple Synthesis ◽  
High Yield ◽  
One Step

A simple and practical method for the synthesis on a large scale of altretamine (1), a wellknown antitumor drug, has been successfully developed. The synthesis method involves the conversion of cyanuric chloride (2) into altretamine (1) by dimethylamination of 2 with an aqueous solution of 40% dimethylamine and potassium hydroxide in 1, -dioxan 4in one step to give altretamine (1) in high yield.

One-step aqueous solution route toward depositing transparent carbon film onto different quartize substrate

2016 ◽  
Vol 185 ◽  
pp. 135-138 ◽  
Author(s):  
Yingjie Cao ◽  
Xiao Dai ◽  
Keqin Zhang ◽  
Hao Wang ◽  
Guifu Zou
Keyword(s):  
Aqueous Solution ◽  
Carbon Film ◽  
One Step ◽  
Solution Route

BiVO4hollow microplates: controlled synthesis and enhanced photocatalytic activity achieved through one-step boron doping and Co(OH)2loading

CrystEngComm ◽  
2017 ◽  
Vol 19 (42) ◽  
pp. 6305-6313 ◽  
Author(s):  
Abraham Adenle ◽  
De-Kun Ma ◽  
De-Peng Qu ◽  
Wei Chen ◽  
Shaoming Huang
Keyword(s):  
Photocatalytic Activity ◽  
Boron Doping ◽  
Controlled Synthesis ◽  
One Step

BiVO4hollow microplates co-modified by boron doping and Co(OH)2nanoparticle loading achieved enhanced photocatalytic activity.

scholarly journals Controlled synthesis of dendritic gold nanostructures by graphene oxide and their morphology-dependent performance for iron detection in coastal waters

RSC Advances ◽  
2017 ◽  
Vol 7 (26) ◽  
pp. 15833-15841 ◽  
Author(s):  
Haitao Han ◽  
Dawei Pan ◽  
Chenchen Wang ◽  
Rilong Zhu
Keyword(s):  
Graphene Oxide ◽  
Coastal Waters ◽  
Voltammetric Determination ◽  
Gold Nanostructures ◽  
Controlled Synthesis

Dendritic gold nanostructures were controllably synthesized by graphene oxide for voltammetric determination of Fe(iii) in coastal waters.

Controlled synthesis of Fe3O4 nanosheets via one-step pyrolysis of EDTA ferric sodium salt

2010 ◽  
Vol 504 (2) ◽  
pp. L46-L50 ◽  
Author(s):  
Lingyun Chen ◽  
Chenglan Zhao ◽  
Yang Zhou ◽  
Hui Peng ◽  
Yiyang Zheng
Keyword(s):  
Sodium Salt ◽  
Controlled Synthesis ◽  
Ferric Sodium ◽  
One Step

Tobacco stalk-derived carbon prepared by one-step molten salt carbonization for supercapacitor

2021 ◽  
pp. 2151021
Author(s):  
Yuxuan Liu ◽  
Xinhua Cheng ◽  
Shenghui Zhang
Keyword(s):  
Aqueous Solution ◽  
Energy Density ◽  
Porous Structure ◽  
Molten Salt ◽  
Electrode System ◽  
Rate Performance ◽  
Heteroatom Doping ◽  
Hierarchically Porous Structure ◽  
One Step ◽  
Tobacco Stalk

High-performance capacitive carbon materials, derived from tobacco stalk, were prepared by a one-step carbonization process in molten carbonate. Owing to the high specific surface area (SSA) (1165.9 m2 g[Formula: see text] and heteroatom doping by the activation effect of molten salt medium for 3 h, the as-obtained carbon material with hierarchically porous structure exhibits an ideal capacitive property with delivering specific capacitances of 219.8, 188.0, 176.4, and 168.4 F g[Formula: see text] at 0.2, 0.5, 1, and 2 A g[Formula: see text], respectively, acceptable rate performance with 76.6% capacitance retention in range of 0.2–2 A g[Formula: see text], and good cyclic stability with 93% capacitance retention after 3000 charge–discharge cycles at 1 A g[Formula: see text], as well as energy density of 30.5 Wh kg[Formula: see text] at 0.2 A g[Formula: see text] and power density of 989.6 W kg[Formula: see text] at 2 A g[Formula: see text] in 1 mol L[Formula: see text] H2SO4 aqueous solution using a three-electrode system. Moreover, it delivers specific capacitances of 143.3, 140.2, 137.4, and 134.3 F g[Formula: see text] at 0.2, 0.5, 1, and 2 A g[Formula: see text], respectively, and excellent rate performance with 93.7% capacitance retention in range of 0.2–2 A g[Formula: see text], as well as energy density of 4.9 Wh kg[Formula: see text] at 0.2 A g[Formula: see text] and power density of 488.6 W kg[Formula: see text] at 2 A g[Formula: see text] in 6 mol L[Formula: see text] KOH aqueous solution using a symmetrical two-electrode system. The correlation between hierarchically porous structure with heteroatom doping and capacitive performance is also discussed.

One-step preparation of polyimide-inlaid amine-rich porous organic block copolymer for efficient removal of chlorophenols from aqueous solution

2019 ◽  
Vol 78 ◽  
pp. 215-229 ◽  
Author(s):  
Yanyang Liu ◽  
Haijian Ou ◽  
Shangqing Li ◽  
Qingliang You ◽  
Huixian Liu ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Block Copolymer ◽  
Efficient Removal ◽  
One Step

Controlled synthesis of CeVO4 hierarchical hollow microspheres with tunable hollowness and their efficient photocatalytic activity

CrystEngComm ◽  
2018 ◽  
Vol 20 (31) ◽  
pp. 4499-4505 ◽  
Author(s):  
Jinjin Ding ◽  
Xuan Liu ◽  
Miao Wang ◽  
Quan Liu ◽  
Tongming Sun ◽  
...  
Keyword(s):  
Photocatalytic Activity ◽  
Hollow Microspheres ◽  
Controlled Synthesis ◽  
One Step ◽  
Hydrothermal Approach

CeVO4 hierarchical hollow microspheres assembled from nanoscaled building units (nanoparticles, nanocubes and nanoflakes) were synthesized by a one-step hydrothermal approach using l-Asp as the morphology-directing agent.

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